Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C
Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates w...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Fabbrizio, Alessandro [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2013 |
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| Schlagwörter: |
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| Systematik: |
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| Anmerkung: |
© The Author(s) 2013 |
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| Übergeordnetes Werk: |
Enthalten in: Contributions to mineralogy and petrology - Springer Berlin Heidelberg, 1966, 166(2013), 2 vom: 19. Juni, Seite 639-653 |
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| Übergeordnetes Werk: |
volume:166 ; year:2013 ; number:2 ; day:19 ; month:06 ; pages:639-653 |
| Links: |
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| DOI / URN: |
10.1007/s00410-013-0902-5 |
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| Katalog-ID: |
OLC2070532534 |
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| 245 | 1 | 0 | |a Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C |
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| 520 | |a Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. | ||
| 650 | 4 | |a Halogens | |
| 650 | 4 | |a Trace element partitioning | |
| 650 | 4 | |a Mantle | |
| 650 | 4 | |a Defects | |
| 650 | 4 | |a TEM | |
| 700 | 1 | |a Stalder, Roland |4 aut | |
| 700 | 1 | |a Hametner, Kathrin |4 aut | |
| 700 | 1 | |a Günther, Detlef |4 aut | |
| 700 | 1 | |a Marquardt, Katharina |4 aut | |
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10.1007/s00410-013-0902-5 doi (DE-627)OLC2070532534 (DE-He213)s00410-013-0902-5-p DE-627 ger DE-627 rakwb eng 550 VZ 13 ssgn TE 1000 VZ rvk Fabbrizio, Alessandro verfasserin aut Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2013 Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. Halogens Trace element partitioning Mantle Defects TEM Stalder, Roland aut Hametner, Kathrin aut Günther, Detlef aut Marquardt, Katharina aut Enthalten in Contributions to mineralogy and petrology Springer Berlin Heidelberg, 1966 166(2013), 2 vom: 19. Juni, Seite 639-653 (DE-627)129068721 (DE-600)1616-0 (DE-576)014400367 0010-7999 nnns volume:166 year:2013 number:2 day:19 month:06 pages:639-653 https://doi.org/10.1007/s00410-013-0902-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 GBV_ILN_381 GBV_ILN_2018 GBV_ILN_2027 GBV_ILN_4277 GBV_ILN_4323 TE 1000 AR 166 2013 2 19 06 639-653 |
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10.1007/s00410-013-0902-5 doi (DE-627)OLC2070532534 (DE-He213)s00410-013-0902-5-p DE-627 ger DE-627 rakwb eng 550 VZ 13 ssgn TE 1000 VZ rvk Fabbrizio, Alessandro verfasserin aut Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2013 Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. Halogens Trace element partitioning Mantle Defects TEM Stalder, Roland aut Hametner, Kathrin aut Günther, Detlef aut Marquardt, Katharina aut Enthalten in Contributions to mineralogy and petrology Springer Berlin Heidelberg, 1966 166(2013), 2 vom: 19. Juni, Seite 639-653 (DE-627)129068721 (DE-600)1616-0 (DE-576)014400367 0010-7999 nnns volume:166 year:2013 number:2 day:19 month:06 pages:639-653 https://doi.org/10.1007/s00410-013-0902-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 GBV_ILN_381 GBV_ILN_2018 GBV_ILN_2027 GBV_ILN_4277 GBV_ILN_4323 TE 1000 AR 166 2013 2 19 06 639-653 |
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10.1007/s00410-013-0902-5 doi (DE-627)OLC2070532534 (DE-He213)s00410-013-0902-5-p DE-627 ger DE-627 rakwb eng 550 VZ 13 ssgn TE 1000 VZ rvk Fabbrizio, Alessandro verfasserin aut Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2013 Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. Halogens Trace element partitioning Mantle Defects TEM Stalder, Roland aut Hametner, Kathrin aut Günther, Detlef aut Marquardt, Katharina aut Enthalten in Contributions to mineralogy and petrology Springer Berlin Heidelberg, 1966 166(2013), 2 vom: 19. Juni, Seite 639-653 (DE-627)129068721 (DE-600)1616-0 (DE-576)014400367 0010-7999 nnns volume:166 year:2013 number:2 day:19 month:06 pages:639-653 https://doi.org/10.1007/s00410-013-0902-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 GBV_ILN_381 GBV_ILN_2018 GBV_ILN_2027 GBV_ILN_4277 GBV_ILN_4323 TE 1000 AR 166 2013 2 19 06 639-653 |
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10.1007/s00410-013-0902-5 doi (DE-627)OLC2070532534 (DE-He213)s00410-013-0902-5-p DE-627 ger DE-627 rakwb eng 550 VZ 13 ssgn TE 1000 VZ rvk Fabbrizio, Alessandro verfasserin aut Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2013 Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. Halogens Trace element partitioning Mantle Defects TEM Stalder, Roland aut Hametner, Kathrin aut Günther, Detlef aut Marquardt, Katharina aut Enthalten in Contributions to mineralogy and petrology Springer Berlin Heidelberg, 1966 166(2013), 2 vom: 19. Juni, Seite 639-653 (DE-627)129068721 (DE-600)1616-0 (DE-576)014400367 0010-7999 nnns volume:166 year:2013 number:2 day:19 month:06 pages:639-653 https://doi.org/10.1007/s00410-013-0902-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 GBV_ILN_381 GBV_ILN_2018 GBV_ILN_2027 GBV_ILN_4277 GBV_ILN_4323 TE 1000 AR 166 2013 2 19 06 639-653 |
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10.1007/s00410-013-0902-5 doi (DE-627)OLC2070532534 (DE-He213)s00410-013-0902-5-p DE-627 ger DE-627 rakwb eng 550 VZ 13 ssgn TE 1000 VZ rvk Fabbrizio, Alessandro verfasserin aut Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2013 Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. Halogens Trace element partitioning Mantle Defects TEM Stalder, Roland aut Hametner, Kathrin aut Günther, Detlef aut Marquardt, Katharina aut Enthalten in Contributions to mineralogy and petrology Springer Berlin Heidelberg, 1966 166(2013), 2 vom: 19. Juni, Seite 639-653 (DE-627)129068721 (DE-600)1616-0 (DE-576)014400367 0010-7999 nnns volume:166 year:2013 number:2 day:19 month:06 pages:639-653 https://doi.org/10.1007/s00410-013-0902-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 GBV_ILN_381 GBV_ILN_2018 GBV_ILN_2027 GBV_ILN_4277 GBV_ILN_4323 TE 1000 AR 166 2013 2 19 06 639-653 |
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Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. 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Fabbrizio, Alessandro |
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550 VZ 13 ssgn TE 1000 VZ rvk Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C Halogens Trace element partitioning Mantle Defects TEM |
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Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C |
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Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C |
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experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 gpa and 900–1,300 °c |
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Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C |
| abstract |
Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. © The Author(s) 2013 |
| abstractGer |
Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. © The Author(s) 2013 |
| abstract_unstemmed |
Abstract We present new partition coefficients for various trace elements including Cl between olivine, pyroxenes, amphibole and coexisting chlorine-bearing aqueous fluid in a series of high-pressure experiments at 2 GPa between 900 and 1,300 °C in natural and synthetic systems. Diamond aggregates were added to the experimental capsule set-up in order to separate the fluid from the solid residue and enable in situ analysis of the quenched solute by LA–ICP–MS. The chlorine and fluorine contents in mantle minerals were measured by electron microprobe, and the nature of OH defects was investigated by infrared spectroscopy. Furthermore, a fluorine-rich olivine from one selected sample was investigated by TEM. Results reveal average Cl concentrations in olivine and pyroxenes around 20 ppm and up to 900 ppm F in olivine, making olivine an important repository of halogens in the mantle. Chlorine is always incompatible with Cl partition coefficients DClolivine/fluid varying between $ 10^{−5} $ and $ 10^{−3} $, whereas DClorthopyroxene/fluid and DClclinopyroxene/fluid are ~$ 10^{−4} $ and DClamphibole/fluid is ~5 × $ 10^{−3} $. Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. The presence of planar defects could not be proved by TEM investigations, but dislocations in the olivine lattice were observed and are suggested to be an important site for halogen incorporation in olivine. © The Author(s) 2013 |
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Experimental partitioning of halogens and other trace elements between olivine, pyroxenes, amphibole and aqueous fluid at 2 GPa and 900–1,300 °C |
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Furthermore, partitioning results for incompatible trace element show that compatibilities of trace elements are generally ordered as Damph/fluid ≈ Dcpx/fluid > Dopx/fluid > Dol/fluid but that Dmineral/fluid for Li and P is very similar for all observed silicate phases. Infrared spectra of olivine synthesized in a F-free Ti-bearing system show absorption bands at 3,525 and ~3,570 $ cm^{−1} $. In F ± $ TiO_{2} $-bearing systems, additional absorption bands appear at ~3,535, ~3,595, 3,640 and 3,670 $ cm^{−1} $. Absorption bands at ~3,530 and ~3,570 $ cm^{−1} $, previously assigned to humite-like point defects, profit from low synthesis temperatures and the presence of F. 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Juni, Seite 639-653</subfield><subfield code="w">(DE-627)129068721</subfield><subfield code="w">(DE-600)1616-0</subfield><subfield code="w">(DE-576)014400367</subfield><subfield code="x">0010-7999</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:166</subfield><subfield code="g">year:2013</subfield><subfield code="g">number:2</subfield><subfield code="g">day:19</subfield><subfield code="g">month:06</subfield><subfield code="g">pages:639-653</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/s00410-013-0902-5</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-GEO</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OPC-GGO</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_30</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_40</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_381</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2018</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2027</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4277</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4323</subfield></datafield><datafield tag="936" ind1="r" ind2="v"><subfield code="a">TE 1000</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">166</subfield><subfield code="j">2013</subfield><subfield code="e">2</subfield><subfield code="b">19</subfield><subfield code="c">06</subfield><subfield code="h">639-653</subfield></datafield></record></collection>
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