A multiclass, multiresidue analytical method for pesticides in water
Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into gro...
Ausführliche Beschreibung
Autor*in: |
Thompson, John F. [verfasserIn] |
---|
Format: |
Artikel |
---|---|
Sprache: |
Englisch |
Erschienen: |
1977 |
---|
Schlagwörter: |
---|
Anmerkung: |
© Springer-Verlag New York Inc. 1977 |
---|
Übergeordnetes Werk: |
Enthalten in: Archives of environmental contamination and toxicology - Springer-Verlag, 1973, 6(1977), 1 vom: Dez., Seite 143-157 |
---|---|
Übergeordnetes Werk: |
volume:6 ; year:1977 ; number:1 ; month:12 ; pages:143-157 |
Links: |
---|
DOI / URN: |
10.1007/BF02097757 |
---|
Katalog-ID: |
OLC2070673901 |
---|
LEADER | 01000caa a22002652 4500 | ||
---|---|---|---|
001 | OLC2070673901 | ||
003 | DE-627 | ||
005 | 20230324031515.0 | ||
007 | tu | ||
008 | 200819s1977 xx ||||| 00| ||eng c | ||
024 | 7 | |a 10.1007/BF02097757 |2 doi | |
035 | |a (DE-627)OLC2070673901 | ||
035 | |a (DE-He213)BF02097757-p | ||
040 | |a DE-627 |b ger |c DE-627 |e rakwb | ||
041 | |a eng | ||
082 | 0 | 4 | |a 333.7 |a 610 |q VZ |
100 | 1 | |a Thompson, John F. |e verfasserin |4 aut | |
245 | 1 | 0 | |a A multiclass, multiresidue analytical method for pesticides in water |
264 | 1 | |c 1977 | |
336 | |a Text |b txt |2 rdacontent | ||
337 | |a ohne Hilfsmittel zu benutzen |b n |2 rdamedia | ||
338 | |a Band |b nc |2 rdacarrier | ||
500 | |a © Springer-Verlag New York Inc. 1977 | ||
520 | |a Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. | ||
650 | 4 | |a Methylene Chloride | |
650 | 4 | |a Solvent System | |
650 | 4 | |a Carbamate | |
650 | 4 | |a Parent Compound | |
650 | 4 | |a Electron Capture | |
700 | 1 | |a Reid, Stuart J. |4 aut | |
700 | 1 | |a Kantor, Edward J. |4 aut | |
773 | 0 | 8 | |i Enthalten in |t Archives of environmental contamination and toxicology |d Springer-Verlag, 1973 |g 6(1977), 1 vom: Dez., Seite 143-157 |w (DE-627)129397725 |w (DE-600)185986-9 |w (DE-576)01478100X |x 0090-4341 |7 nnns |
773 | 1 | 8 | |g volume:6 |g year:1977 |g number:1 |g month:12 |g pages:143-157 |
856 | 4 | 1 | |u https://doi.org/10.1007/BF02097757 |z lizenzpflichtig |3 Volltext |
912 | |a GBV_USEFLAG_A | ||
912 | |a SYSFLAG_A | ||
912 | |a GBV_OLC | ||
912 | |a SSG-OLC-UMW | ||
912 | |a GBV_ILN_11 | ||
912 | |a GBV_ILN_21 | ||
912 | |a GBV_ILN_22 | ||
912 | |a GBV_ILN_70 | ||
912 | |a GBV_ILN_252 | ||
912 | |a GBV_ILN_601 | ||
912 | |a GBV_ILN_2018 | ||
912 | |a GBV_ILN_4012 | ||
912 | |a GBV_ILN_4035 | ||
912 | |a GBV_ILN_4103 | ||
912 | |a GBV_ILN_4219 | ||
912 | |a GBV_ILN_4313 | ||
912 | |a GBV_ILN_4319 | ||
951 | |a AR | ||
952 | |d 6 |j 1977 |e 1 |c 12 |h 143-157 |
author_variant |
j f t jf jft s j r sj sjr e j k ej ejk |
---|---|
matchkey_str |
article:00904341:1977----::mlilsmlieiuaayiamtofr |
hierarchy_sort_str |
1977 |
publishDate |
1977 |
allfields |
10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
spelling |
10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
allfields_unstemmed |
10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
allfieldsGer |
10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
allfieldsSound |
10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
language |
English |
source |
Enthalten in Archives of environmental contamination and toxicology 6(1977), 1 vom: Dez., Seite 143-157 volume:6 year:1977 number:1 month:12 pages:143-157 |
sourceStr |
Enthalten in Archives of environmental contamination and toxicology 6(1977), 1 vom: Dez., Seite 143-157 volume:6 year:1977 number:1 month:12 pages:143-157 |
format_phy_str_mv |
Article |
institution |
findex.gbv.de |
topic_facet |
Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture |
dewey-raw |
333.7 |
isfreeaccess_bool |
false |
container_title |
Archives of environmental contamination and toxicology |
authorswithroles_txt_mv |
Thompson, John F. @@aut@@ Reid, Stuart J. @@aut@@ Kantor, Edward J. @@aut@@ |
publishDateDaySort_date |
1977-12-01T00:00:00Z |
hierarchy_top_id |
129397725 |
dewey-sort |
3333.7 |
id |
OLC2070673901 |
language_de |
englisch |
fullrecord |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2070673901</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230324031515.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s1977 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/BF02097757</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2070673901</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)BF02097757-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">333.7</subfield><subfield code="a">610</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Thompson, John F.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">A multiclass, multiresidue analytical method for pesticides in water</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1977</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Springer-Verlag New York Inc. 1977</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Methylene Chloride</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Solvent System</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Carbamate</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Parent Compound</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Electron Capture</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Reid, Stuart J.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Kantor, Edward J.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Archives of environmental contamination and toxicology</subfield><subfield code="d">Springer-Verlag, 1973</subfield><subfield code="g">6(1977), 1 vom: Dez., Seite 143-157</subfield><subfield code="w">(DE-627)129397725</subfield><subfield code="w">(DE-600)185986-9</subfield><subfield code="w">(DE-576)01478100X</subfield><subfield code="x">0090-4341</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:6</subfield><subfield code="g">year:1977</subfield><subfield code="g">number:1</subfield><subfield code="g">month:12</subfield><subfield code="g">pages:143-157</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/BF02097757</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-UMW</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_11</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_21</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_22</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_252</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_601</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2018</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4012</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4035</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4103</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4313</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4319</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">6</subfield><subfield code="j">1977</subfield><subfield code="e">1</subfield><subfield code="c">12</subfield><subfield code="h">143-157</subfield></datafield></record></collection>
|
author |
Thompson, John F. |
spellingShingle |
Thompson, John F. ddc 333.7 misc Methylene Chloride misc Solvent System misc Carbamate misc Parent Compound misc Electron Capture A multiclass, multiresidue analytical method for pesticides in water |
authorStr |
Thompson, John F. |
ppnlink_with_tag_str_mv |
@@773@@(DE-627)129397725 |
format |
Article |
dewey-ones |
333 - Economics of land & energy 610 - Medicine & health |
delete_txt_mv |
keep |
author_role |
aut aut aut |
collection |
OLC |
remote_str |
false |
illustrated |
Not Illustrated |
issn |
0090-4341 |
topic_title |
333.7 610 VZ A multiclass, multiresidue analytical method for pesticides in water Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture |
topic |
ddc 333.7 misc Methylene Chloride misc Solvent System misc Carbamate misc Parent Compound misc Electron Capture |
topic_unstemmed |
ddc 333.7 misc Methylene Chloride misc Solvent System misc Carbamate misc Parent Compound misc Electron Capture |
topic_browse |
ddc 333.7 misc Methylene Chloride misc Solvent System misc Carbamate misc Parent Compound misc Electron Capture |
format_facet |
Aufsätze Gedruckte Aufsätze |
format_main_str_mv |
Text Zeitschrift/Artikel |
carriertype_str_mv |
nc |
hierarchy_parent_title |
Archives of environmental contamination and toxicology |
hierarchy_parent_id |
129397725 |
dewey-tens |
330 - Economics 610 - Medicine & health |
hierarchy_top_title |
Archives of environmental contamination and toxicology |
isfreeaccess_txt |
false |
familylinks_str_mv |
(DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X |
title |
A multiclass, multiresidue analytical method for pesticides in water |
ctrlnum |
(DE-627)OLC2070673901 (DE-He213)BF02097757-p |
title_full |
A multiclass, multiresidue analytical method for pesticides in water |
author_sort |
Thompson, John F. |
journal |
Archives of environmental contamination and toxicology |
journalStr |
Archives of environmental contamination and toxicology |
lang_code |
eng |
isOA_bool |
false |
dewey-hundreds |
300 - Social sciences 600 - Technology |
recordtype |
marc |
publishDateSort |
1977 |
contenttype_str_mv |
txt |
container_start_page |
143 |
author_browse |
Thompson, John F. Reid, Stuart J. Kantor, Edward J. |
container_volume |
6 |
class |
333.7 610 VZ |
format_se |
Aufsätze |
author-letter |
Thompson, John F. |
doi_str_mv |
10.1007/BF02097757 |
dewey-full |
333.7 610 |
title_sort |
a multiclass, multiresidue analytical method for pesticides in water |
title_auth |
A multiclass, multiresidue analytical method for pesticides in water |
abstract |
Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. © Springer-Verlag New York Inc. 1977 |
abstractGer |
Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. © Springer-Verlag New York Inc. 1977 |
abstract_unstemmed |
Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. © Springer-Verlag New York Inc. 1977 |
collection_details |
GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 |
container_issue |
1 |
title_short |
A multiclass, multiresidue analytical method for pesticides in water |
url |
https://doi.org/10.1007/BF02097757 |
remote_bool |
false |
author2 |
Reid, Stuart J. Kantor, Edward J. |
author2Str |
Reid, Stuart J. Kantor, Edward J. |
ppnlink |
129397725 |
mediatype_str_mv |
n |
isOA_txt |
false |
hochschulschrift_bool |
false |
doi_str |
10.1007/BF02097757 |
up_date |
2024-07-04T01:58:58.157Z |
_version_ |
1803611891993411584 |
fullrecord_marcxml |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2070673901</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230324031515.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s1977 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/BF02097757</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2070673901</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)BF02097757-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">333.7</subfield><subfield code="a">610</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Thompson, John F.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">A multiclass, multiresidue analytical method for pesticides in water</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1977</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Springer-Verlag New York Inc. 1977</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Methylene Chloride</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Solvent System</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Carbamate</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Parent Compound</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Electron Capture</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Reid, Stuart J.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Kantor, Edward J.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Archives of environmental contamination and toxicology</subfield><subfield code="d">Springer-Verlag, 1973</subfield><subfield code="g">6(1977), 1 vom: Dez., Seite 143-157</subfield><subfield code="w">(DE-627)129397725</subfield><subfield code="w">(DE-600)185986-9</subfield><subfield code="w">(DE-576)01478100X</subfield><subfield code="x">0090-4341</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:6</subfield><subfield code="g">year:1977</subfield><subfield code="g">number:1</subfield><subfield code="g">month:12</subfield><subfield code="g">pages:143-157</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/BF02097757</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-UMW</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_11</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_21</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_22</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_252</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_601</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2018</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4012</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4035</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4103</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4313</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4319</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">6</subfield><subfield code="j">1977</subfield><subfield code="e">1</subfield><subfield code="c">12</subfield><subfield code="h">143-157</subfield></datafield></record></collection>
|
score |
7.399131 |