A multiclass, multiresidue analytical method for pesticides in water
Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into gro...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Thompson, John F. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
1977 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer-Verlag New York Inc. 1977 |
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| Übergeordnetes Werk: |
Enthalten in: Archives of environmental contamination and toxicology - Springer-Verlag, 1973, 6(1977), 1 vom: Dez., Seite 143-157 |
|---|---|
| Übergeordnetes Werk: |
volume:6 ; year:1977 ; number:1 ; month:12 ; pages:143-157 |
| Links: |
|---|
| DOI / URN: |
10.1007/BF02097757 |
|---|
| Katalog-ID: |
OLC2070673901 |
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| 520 | |a Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. | ||
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10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
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10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
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10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
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10.1007/BF02097757 doi (DE-627)OLC2070673901 (DE-He213)BF02097757-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Thompson, John F. verfasserin aut A multiclass, multiresidue analytical method for pesticides in water 1977 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc. 1977 Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. Methylene Chloride Solvent System Carbamate Parent Compound Electron Capture Reid, Stuart J. aut Kantor, Edward J. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 6(1977), 1 vom: Dez., Seite 143-157 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:6 year:1977 number:1 month:12 pages:143-157 https://doi.org/10.1007/BF02097757 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_70 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4313 GBV_ILN_4319 AR 6 1977 1 12 143-157 |
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A multiclass, multiresidue analytical method for pesticides in water |
| abstract |
Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. © Springer-Verlag New York Inc. 1977 |
| abstractGer |
Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. © Springer-Verlag New York Inc. 1977 |
| abstract_unstemmed |
Abstract A procedure is reported for the multiclass, multiresidue analysis of pesticides in water. Compounds are extracted from water with methylene chloride, and the extract is concentrated by an evaporative technique utilizing reduced pressure and low temperature. Compounds are segregated into groups using a column of partially deactivated silica gel and sequential elution with four different solvent systems. Carbamate residues, converted to their 2,4-dinitrophenyl ether derivatives, are gas chromatographedvia electron capture detection as are the parent compounds of the organohalogen compounds. Organophosphorus compounds are determined by gas chromatography using a flame photometric detector. Recovery studies were conducted on 42 halogenated compounds, 38 organophosphorus compounds, and 7 carbamates. Fifty-eight of 87 compounds tested produced recoveries in excess of 80%; another 13 compounds yielded recoveries exceeding 60%, while the recoveries on the remaining 16 compounds fell below 60%. © Springer-Verlag New York Inc. 1977 |
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| title_short |
A multiclass, multiresidue analytical method for pesticides in water |
| url |
https://doi.org/10.1007/BF02097757 |
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| author2 |
Reid, Stuart J. Kantor, Edward J. |
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Reid, Stuart J. Kantor, Edward J. |
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| doi_str |
10.1007/BF02097757 |
| up_date |
2024-07-04T01:58:58.157Z |
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