A multiresidue method for determination of trace levels of pesticides in air and water

Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) an...
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Gespeichert in:

Autor*in:	Millet, M. [verfasserIn] Wortham, H. Sanusi, A. Mirabel, P.

Format:	Artikel
Sprache:	Englisch

Erschienen:	1996

Schlagwörter:	Fractionation Butyl Aqueous Sample Glass Fiber Filter Methyl Ether

Anmerkung:	© Springer-Verlag New York Inc 1996

Übergeordnetes Werk:	Enthalten in: Archives of environmental contamination and toxicology - Springer-Verlag, 1973, 31(1996), 4 vom: Nov., Seite 543-556
Übergeordnetes Werk:	volume:31 ; year:1996 ; number:4 ; month:11 ; pages:543-556

Links:	Volltext

DOI / URN:	10.1007/BF00212439

Katalog-ID:	OLC2070694682

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allfields	10.1007/BF00212439 doi (DE-627)OLC2070694682 (DE-He213)BF00212439-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Millet, M. verfasserin aut A multiresidue method for determination of trace levels of pesticides in air and water 1996 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc 1996 Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) and particles (on glass fiber filters), HPLC-based fractionation of the extracted residues using a silica column, and a linear gradient of n-hexane/tert butyl methyl ether followed by GC-ECD and HPLC-UV analyses of each fraction. Prior to analysis with GC-ECD, a methylation procedure using $ BF_{3} $/methanol was developed for the analysis of the fraction which contains chlorophenoxy acid herbicides. The recoveries of the extraction procedure of liquid samples and of the methylation were greater than 92 and 97% with a standard deviation lower than 8 and 5%, respectively. The detection limits varied between 0.1 and 0.01 μg · $ ml^{−1} $ for the 13 pesticides studied with a standard deviation less than 9%. This method was used for the determination of pesticides in 18 fogwater samples (soluble + insoluble), 31 rainwater samples, and 17 air (gas + particles) samples collected between 1991 and 1993 in Colmar (east of France). Fractionation Butyl Aqueous Sample Glass Fiber Filter Methyl Ether Wortham, H. aut Sanusi, A. aut Mirabel, P. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 31(1996), 4 vom: Nov., Seite 543-556 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:31 year:1996 number:4 month:11 pages:543-556 https://doi.org/10.1007/BF00212439 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_31 GBV_ILN_69 GBV_ILN_70 GBV_ILN_130 GBV_ILN_154 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4277 GBV_ILN_4307 GBV_ILN_4313 AR 31 1996 4 11 543-556
spelling	10.1007/BF00212439 doi (DE-627)OLC2070694682 (DE-He213)BF00212439-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Millet, M. verfasserin aut A multiresidue method for determination of trace levels of pesticides in air and water 1996 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc 1996 Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) and particles (on glass fiber filters), HPLC-based fractionation of the extracted residues using a silica column, and a linear gradient of n-hexane/tert butyl methyl ether followed by GC-ECD and HPLC-UV analyses of each fraction. Prior to analysis with GC-ECD, a methylation procedure using $ BF_{3} $/methanol was developed for the analysis of the fraction which contains chlorophenoxy acid herbicides. The recoveries of the extraction procedure of liquid samples and of the methylation were greater than 92 and 97% with a standard deviation lower than 8 and 5%, respectively. The detection limits varied between 0.1 and 0.01 μg · $ ml^{−1} $ for the 13 pesticides studied with a standard deviation less than 9%. This method was used for the determination of pesticides in 18 fogwater samples (soluble + insoluble), 31 rainwater samples, and 17 air (gas + particles) samples collected between 1991 and 1993 in Colmar (east of France). Fractionation Butyl Aqueous Sample Glass Fiber Filter Methyl Ether Wortham, H. aut Sanusi, A. aut Mirabel, P. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 31(1996), 4 vom: Nov., Seite 543-556 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:31 year:1996 number:4 month:11 pages:543-556 https://doi.org/10.1007/BF00212439 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_31 GBV_ILN_69 GBV_ILN_70 GBV_ILN_130 GBV_ILN_154 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4277 GBV_ILN_4307 GBV_ILN_4313 AR 31 1996 4 11 543-556
allfields_unstemmed	10.1007/BF00212439 doi (DE-627)OLC2070694682 (DE-He213)BF00212439-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Millet, M. verfasserin aut A multiresidue method for determination of trace levels of pesticides in air and water 1996 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc 1996 Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) and particles (on glass fiber filters), HPLC-based fractionation of the extracted residues using a silica column, and a linear gradient of n-hexane/tert butyl methyl ether followed by GC-ECD and HPLC-UV analyses of each fraction. Prior to analysis with GC-ECD, a methylation procedure using $ BF_{3} $/methanol was developed for the analysis of the fraction which contains chlorophenoxy acid herbicides. The recoveries of the extraction procedure of liquid samples and of the methylation were greater than 92 and 97% with a standard deviation lower than 8 and 5%, respectively. The detection limits varied between 0.1 and 0.01 μg · $ ml^{−1} $ for the 13 pesticides studied with a standard deviation less than 9%. This method was used for the determination of pesticides in 18 fogwater samples (soluble + insoluble), 31 rainwater samples, and 17 air (gas + particles) samples collected between 1991 and 1993 in Colmar (east of France). Fractionation Butyl Aqueous Sample Glass Fiber Filter Methyl Ether Wortham, H. aut Sanusi, A. aut Mirabel, P. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 31(1996), 4 vom: Nov., Seite 543-556 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:31 year:1996 number:4 month:11 pages:543-556 https://doi.org/10.1007/BF00212439 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_31 GBV_ILN_69 GBV_ILN_70 GBV_ILN_130 GBV_ILN_154 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4277 GBV_ILN_4307 GBV_ILN_4313 AR 31 1996 4 11 543-556
allfieldsGer	10.1007/BF00212439 doi (DE-627)OLC2070694682 (DE-He213)BF00212439-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Millet, M. verfasserin aut A multiresidue method for determination of trace levels of pesticides in air and water 1996 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc 1996 Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) and particles (on glass fiber filters), HPLC-based fractionation of the extracted residues using a silica column, and a linear gradient of n-hexane/tert butyl methyl ether followed by GC-ECD and HPLC-UV analyses of each fraction. Prior to analysis with GC-ECD, a methylation procedure using $ BF_{3} $/methanol was developed for the analysis of the fraction which contains chlorophenoxy acid herbicides. The recoveries of the extraction procedure of liquid samples and of the methylation were greater than 92 and 97% with a standard deviation lower than 8 and 5%, respectively. The detection limits varied between 0.1 and 0.01 μg · $ ml^{−1} $ for the 13 pesticides studied with a standard deviation less than 9%. This method was used for the determination of pesticides in 18 fogwater samples (soluble + insoluble), 31 rainwater samples, and 17 air (gas + particles) samples collected between 1991 and 1993 in Colmar (east of France). Fractionation Butyl Aqueous Sample Glass Fiber Filter Methyl Ether Wortham, H. aut Sanusi, A. aut Mirabel, P. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 31(1996), 4 vom: Nov., Seite 543-556 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:31 year:1996 number:4 month:11 pages:543-556 https://doi.org/10.1007/BF00212439 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_31 GBV_ILN_69 GBV_ILN_70 GBV_ILN_130 GBV_ILN_154 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4277 GBV_ILN_4307 GBV_ILN_4313 AR 31 1996 4 11 543-556
allfieldsSound	10.1007/BF00212439 doi (DE-627)OLC2070694682 (DE-He213)BF00212439-p DE-627 ger DE-627 rakwb eng 333.7 610 VZ Millet, M. verfasserin aut A multiresidue method for determination of trace levels of pesticides in air and water 1996 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag New York Inc 1996 Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) and particles (on glass fiber filters), HPLC-based fractionation of the extracted residues using a silica column, and a linear gradient of n-hexane/tert butyl methyl ether followed by GC-ECD and HPLC-UV analyses of each fraction. Prior to analysis with GC-ECD, a methylation procedure using $ BF_{3} $/methanol was developed for the analysis of the fraction which contains chlorophenoxy acid herbicides. The recoveries of the extraction procedure of liquid samples and of the methylation were greater than 92 and 97% with a standard deviation lower than 8 and 5%, respectively. The detection limits varied between 0.1 and 0.01 μg · $ ml^{−1} $ for the 13 pesticides studied with a standard deviation less than 9%. This method was used for the determination of pesticides in 18 fogwater samples (soluble + insoluble), 31 rainwater samples, and 17 air (gas + particles) samples collected between 1991 and 1993 in Colmar (east of France). Fractionation Butyl Aqueous Sample Glass Fiber Filter Methyl Ether Wortham, H. aut Sanusi, A. aut Mirabel, P. aut Enthalten in Archives of environmental contamination and toxicology Springer-Verlag, 1973 31(1996), 4 vom: Nov., Seite 543-556 (DE-627)129397725 (DE-600)185986-9 (DE-576)01478100X 0090-4341 nnns volume:31 year:1996 number:4 month:11 pages:543-556 https://doi.org/10.1007/BF00212439 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW GBV_ILN_11 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_31 GBV_ILN_69 GBV_ILN_70 GBV_ILN_130 GBV_ILN_154 GBV_ILN_252 GBV_ILN_601 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4103 GBV_ILN_4219 GBV_ILN_4277 GBV_ILN_4307 GBV_ILN_4313 AR 31 1996 4 11 543-556
language	English
source	Enthalten in Archives of environmental contamination and toxicology 31(1996), 4 vom: Nov., Seite 543-556 volume:31 year:1996 number:4 month:11 pages:543-556
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author	Millet, M.
spellingShingle	Millet, M. ddc 333.7 misc Fractionation misc Butyl misc Aqueous Sample misc Glass Fiber Filter misc Methyl Ether A multiresidue method for determination of trace levels of pesticides in air and water
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topic_title	333.7 610 VZ A multiresidue method for determination of trace levels of pesticides in air and water Fractionation Butyl Aqueous Sample Glass Fiber Filter Methyl Ether
topic	ddc 333.7 misc Fractionation misc Butyl misc Aqueous Sample misc Glass Fiber Filter misc Methyl Ether
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title	A multiresidue method for determination of trace levels of pesticides in air and water
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title_full	A multiresidue method for determination of trace levels of pesticides in air and water
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title_sort	a multiresidue method for determination of trace levels of pesticides in air and water
title_auth	A multiresidue method for determination of trace levels of pesticides in air and water
abstract	Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) and particles (on glass fiber filters), HPLC-based fractionation of the extracted residues using a silica column, and a linear gradient of n-hexane/tert butyl methyl ether followed by GC-ECD and HPLC-UV analyses of each fraction. Prior to analysis with GC-ECD, a methylation procedure using $ BF_{3} $/methanol was developed for the analysis of the fraction which contains chlorophenoxy acid herbicides. The recoveries of the extraction procedure of liquid samples and of the methylation were greater than 92 and 97% with a standard deviation lower than 8 and 5%, respectively. The detection limits varied between 0.1 and 0.01 μg · $ ml^{−1} $ for the 13 pesticides studied with a standard deviation less than 9%. This method was used for the determination of pesticides in 18 fogwater samples (soluble + insoluble), 31 rainwater samples, and 17 air (gas + particles) samples collected between 1991 and 1993 in Colmar (east of France). © Springer-Verlag New York Inc 1996
abstractGer	Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) and particles (on glass fiber filters), HPLC-based fractionation of the extracted residues using a silica column, and a linear gradient of n-hexane/tert butyl methyl ether followed by GC-ECD and HPLC-UV analyses of each fraction. Prior to analysis with GC-ECD, a methylation procedure using $ BF_{3} $/methanol was developed for the analysis of the fraction which contains chlorophenoxy acid herbicides. The recoveries of the extraction procedure of liquid samples and of the methylation were greater than 92 and 97% with a standard deviation lower than 8 and 5%, respectively. The detection limits varied between 0.1 and 0.01 μg · $ ml^{−1} $ for the 13 pesticides studied with a standard deviation less than 9%. This method was used for the determination of pesticides in 18 fogwater samples (soluble + insoluble), 31 rainwater samples, and 17 air (gas + particles) samples collected between 1991 and 1993 in Colmar (east of France). © Springer-Verlag New York Inc 1996
abstract_unstemmed	Abstract A multiresidue analytical method is described for the analysis of 13 pesticides in fogwater, rainwater, gas, and particles. This method is based upon solid-liquid extraction using Sep-$ Pak^{™} $t$ C_{18} $ light cartridges for aqueous samples, soxhlet for gas (adsorbed on XAD-$ 2^{®} $) and particles (on glass fiber filters), HPLC-based fractionation of the extracted residues using a silica column, and a linear gradient of n-hexane/tert butyl methyl ether followed by GC-ECD and HPLC-UV analyses of each fraction. Prior to analysis with GC-ECD, a methylation procedure using $ BF_{3} $/methanol was developed for the analysis of the fraction which contains chlorophenoxy acid herbicides. The recoveries of the extraction procedure of liquid samples and of the methylation were greater than 92 and 97% with a standard deviation lower than 8 and 5%, respectively. The detection limits varied between 0.1 and 0.01 μg · $ ml^{−1} $ for the 13 pesticides studied with a standard deviation less than 9%. This method was used for the determination of pesticides in 18 fogwater samples (soluble + insoluble), 31 rainwater samples, and 17 air (gas + particles) samples collected between 1991 and 1993 in Colmar (east of France). © Springer-Verlag New York Inc 1996
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title_short	A multiresidue method for determination of trace levels of pesticides in air and water
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