Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia
Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bat...
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Gespeichert in:
| Autor*in: |
Relić, Dubravka [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2013 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media Dordrecht 2013 |
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| Übergeordnetes Werk: |
Enthalten in: Environmental monitoring and assessment - Springer Netherlands, 1981, 185(2013), 9 vom: 19. Feb., Seite 7627-7645 |
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| Übergeordnetes Werk: |
volume:185 ; year:2013 ; number:9 ; day:19 ; month:02 ; pages:7627-7645 |
| Links: |
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| DOI / URN: |
10.1007/s10661-013-3124-4 |
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OLC2073757855 |
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| 520 | |a Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. | ||
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| 700 | 1 | |a Stanković, Ratomir |4 aut | |
| 700 | 1 | |a Popović, Aleksandar |4 aut | |
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10.1007/s10661-013-3124-4 doi (DE-627)OLC2073757855 (DE-He213)s10661-013-3124-4-p DE-627 ger DE-627 rakwb eng 333.7 VZ Relić, Dubravka verfasserin aut Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media Dordrecht 2013 Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. Metals Extraction techniques Risk assessment code Sediment Đorđević, Dragana aut Sakan, Sanja aut Anđelković, Ivan aut Pantelić, Ana aut Stanković, Ratomir aut Popović, Aleksandar aut Enthalten in Environmental monitoring and assessment Springer Netherlands, 1981 185(2013), 9 vom: 19. Feb., Seite 7627-7645 (DE-627)130549649 (DE-600)782621-7 (DE-576)476125413 0167-6369 nnns volume:185 year:2013 number:9 day:19 month:02 pages:7627-7645 https://doi.org/10.1007/s10661-013-3124-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW SSG-OLC-FOR SSG-OLC-IBL GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 AR 185 2013 9 19 02 7627-7645 |
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10.1007/s10661-013-3124-4 doi (DE-627)OLC2073757855 (DE-He213)s10661-013-3124-4-p DE-627 ger DE-627 rakwb eng 333.7 VZ Relić, Dubravka verfasserin aut Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media Dordrecht 2013 Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. Metals Extraction techniques Risk assessment code Sediment Đorđević, Dragana aut Sakan, Sanja aut Anđelković, Ivan aut Pantelić, Ana aut Stanković, Ratomir aut Popović, Aleksandar aut Enthalten in Environmental monitoring and assessment Springer Netherlands, 1981 185(2013), 9 vom: 19. Feb., Seite 7627-7645 (DE-627)130549649 (DE-600)782621-7 (DE-576)476125413 0167-6369 nnns volume:185 year:2013 number:9 day:19 month:02 pages:7627-7645 https://doi.org/10.1007/s10661-013-3124-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW SSG-OLC-FOR SSG-OLC-IBL GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 AR 185 2013 9 19 02 7627-7645 |
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10.1007/s10661-013-3124-4 doi (DE-627)OLC2073757855 (DE-He213)s10661-013-3124-4-p DE-627 ger DE-627 rakwb eng 333.7 VZ Relić, Dubravka verfasserin aut Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media Dordrecht 2013 Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. Metals Extraction techniques Risk assessment code Sediment Đorđević, Dragana aut Sakan, Sanja aut Anđelković, Ivan aut Pantelić, Ana aut Stanković, Ratomir aut Popović, Aleksandar aut Enthalten in Environmental monitoring and assessment Springer Netherlands, 1981 185(2013), 9 vom: 19. Feb., Seite 7627-7645 (DE-627)130549649 (DE-600)782621-7 (DE-576)476125413 0167-6369 nnns volume:185 year:2013 number:9 day:19 month:02 pages:7627-7645 https://doi.org/10.1007/s10661-013-3124-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW SSG-OLC-FOR SSG-OLC-IBL GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 AR 185 2013 9 19 02 7627-7645 |
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10.1007/s10661-013-3124-4 doi (DE-627)OLC2073757855 (DE-He213)s10661-013-3124-4-p DE-627 ger DE-627 rakwb eng 333.7 VZ Relić, Dubravka verfasserin aut Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media Dordrecht 2013 Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. Metals Extraction techniques Risk assessment code Sediment Đorđević, Dragana aut Sakan, Sanja aut Anđelković, Ivan aut Pantelić, Ana aut Stanković, Ratomir aut Popović, Aleksandar aut Enthalten in Environmental monitoring and assessment Springer Netherlands, 1981 185(2013), 9 vom: 19. Feb., Seite 7627-7645 (DE-627)130549649 (DE-600)782621-7 (DE-576)476125413 0167-6369 nnns volume:185 year:2013 number:9 day:19 month:02 pages:7627-7645 https://doi.org/10.1007/s10661-013-3124-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW SSG-OLC-FOR SSG-OLC-IBL GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 AR 185 2013 9 19 02 7627-7645 |
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10.1007/s10661-013-3124-4 doi (DE-627)OLC2073757855 (DE-He213)s10661-013-3124-4-p DE-627 ger DE-627 rakwb eng 333.7 VZ Relić, Dubravka verfasserin aut Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media Dordrecht 2013 Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. Metals Extraction techniques Risk assessment code Sediment Đorđević, Dragana aut Sakan, Sanja aut Anđelković, Ivan aut Pantelić, Ana aut Stanković, Ratomir aut Popović, Aleksandar aut Enthalten in Environmental monitoring and assessment Springer Netherlands, 1981 185(2013), 9 vom: 19. Feb., Seite 7627-7645 (DE-627)130549649 (DE-600)782621-7 (DE-576)476125413 0167-6369 nnns volume:185 year:2013 number:9 day:19 month:02 pages:7627-7645 https://doi.org/10.1007/s10661-013-3124-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-UMW SSG-OLC-FOR SSG-OLC-IBL GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 AR 185 2013 9 19 02 7627-7645 |
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Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia |
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Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia |
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Relić, Dubravka |
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Environmental monitoring and assessment |
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Relić, Dubravka Đorđević, Dragana Sakan, Sanja Anđelković, Ivan Pantelić, Ana Stanković, Ratomir Popović, Aleksandar |
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333.7 |
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conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the petrochemical industry, serbia |
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Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia |
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Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. © Springer Science+Business Media Dordrecht 2013 |
| abstractGer |
Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. © Springer Science+Business Media Dordrecht 2013 |
| abstract_unstemmed |
Abstract In this paper, the main objective was fractionation of Cd, Cu, Ni, Pb, Zn, Ca, Fe, and K in certificate material and sediment samples gathered from and around the Petrochemical Industry using the conventional, microwave and ultrasonic sequential extraction. Microwave oven and ultrasound bath were used as an energy source for achieving faster extraction. Additional heating and boiling of samples were avoided by using lower power and shorter time for microwave and ultrasound extraction. Precision and accuracy of procedure were evaluated by using certificate material (BCR701). Acceptable accuracy of metals (87.0–111.3 %) was achieved for all three-step sequential of conventional extraction protocol. An accuracy of the fourth step has been verified with two certificate materials: BCR143R and 146R. The range of total extracted metal concentrations from sediments was similar for all three extraction techniques. A significant high percentage of Cd, Cu, and Zn were obtained after extraction of the exchangeable and acid soluble sediment fraction. Principal component analysis of values obtained after determination of risk assessment code using conventional and ultrasound sequential extraction show similarity of these values. Accuracy, recovery, and risk assessment code values imply that ultrasound sequential extraction is a more suitable, accelerated sequential extraction procedure (30 min per extraction step) than microwave extraction in applied conditions. © Springer Science+Business Media Dordrecht 2013 |
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Conventional, microwave, and ultrasound sequential extractions for the fractionation of metals in sediments within the Petrochemical Industry, Serbia |
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