Depth-dependent calibration for quantitative elemental depth profiling of copper alloys using laser-induced plasma spectroscopy
Abstract This work presents new calibration procedures for deep elemental depth profile analysis of bronze artifacts. A simple ablation model is developed for the estimation of the ablation rate and hence for deriving the depth spatial calibration scale. Elemental quantification is obtained through...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Agresti, Juri [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2014 |
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| Schlagwörter: |
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| Systematik: |
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| Anmerkung: |
© Springer-Verlag Berlin Heidelberg 2014 |
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| Übergeordnetes Werk: |
Enthalten in: Applied physics. A, Materials science & processing - Springer Berlin Heidelberg, 1981, 117(2014), 1 vom: 27. März, Seite 217-221 |
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| Übergeordnetes Werk: |
volume:117 ; year:2014 ; number:1 ; day:27 ; month:03 ; pages:217-221 |
| Links: |
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| DOI / URN: |
10.1007/s00339-014-8363-x |
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| 520 | |a Abstract This work presents new calibration procedures for deep elemental depth profile analysis of bronze artifacts. A simple ablation model is developed for the estimation of the ablation rate and hence for deriving the depth spatial calibration scale. Elemental quantification is obtained through the construction of calibration surfaces, using reference samples of known composition, relating laser-induced plasma spectroscopy (LIPS) intensity ratios, content of atomic species and number of laser pulses. Such a method represents a refinement of the standard LIPS quantification approach based on calibration curves, which is extended here to the generation of significantly deep craters into the material under investigation up to several hundred microns. The depth dependence of the calibration surfaces measured is discussed in the framework of a simplified model of depth-dependent plasma temperature. | ||
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10.1007/s00339-014-8363-x doi (DE-627)OLC2074222572 (DE-He213)s00339-014-8363-x-p DE-627 ger DE-627 rakwb eng 530 620 VZ 530 VZ UA 9001.A VZ rvk Agresti, Juri verfasserin aut Depth-dependent calibration for quantitative elemental depth profiling of copper alloys using laser-induced plasma spectroscopy 2014 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag Berlin Heidelberg 2014 Abstract This work presents new calibration procedures for deep elemental depth profile analysis of bronze artifacts. A simple ablation model is developed for the estimation of the ablation rate and hence for deriving the depth spatial calibration scale. Elemental quantification is obtained through the construction of calibration surfaces, using reference samples of known composition, relating laser-induced plasma spectroscopy (LIPS) intensity ratios, content of atomic species and number of laser pulses. Such a method represents a refinement of the standard LIPS quantification approach based on calibration curves, which is extended here to the generation of significantly deep craters into the material under investigation up to several hundred microns. The depth dependence of the calibration surfaces measured is discussed in the framework of a simplified model of depth-dependent plasma temperature. Depth Profile Ablation Rate Apparent Temperature Ablation Depth Crater Wall Siano, Salvatore aut Enthalten in Applied physics. A, Materials science & processing Springer Berlin Heidelberg, 1981 117(2014), 1 vom: 27. März, Seite 217-221 (DE-627)129861340 (DE-600)283365-7 (DE-576)015171930 0947-8396 nnns volume:117 year:2014 number:1 day:27 month:03 pages:217-221 https://doi.org/10.1007/s00339-014-8363-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_22 GBV_ILN_30 GBV_ILN_60 GBV_ILN_70 GBV_ILN_130 GBV_ILN_170 GBV_ILN_2018 GBV_ILN_4126 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4313 GBV_ILN_4318 GBV_ILN_4319 GBV_ILN_4700 UA 9001.A AR 117 2014 1 27 03 217-221 |
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Depth-dependent calibration for quantitative elemental depth profiling of copper alloys using laser-induced plasma spectroscopy |
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Agresti, Juri |
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Applied physics. A, Materials science & processing |
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Applied physics. A, Materials science & processing |
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Agresti, Juri Siano, Salvatore |
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10.1007/s00339-014-8363-x |
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530 620 |
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depth-dependent calibration for quantitative elemental depth profiling of copper alloys using laser-induced plasma spectroscopy |
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Depth-dependent calibration for quantitative elemental depth profiling of copper alloys using laser-induced plasma spectroscopy |
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Abstract This work presents new calibration procedures for deep elemental depth profile analysis of bronze artifacts. A simple ablation model is developed for the estimation of the ablation rate and hence for deriving the depth spatial calibration scale. Elemental quantification is obtained through the construction of calibration surfaces, using reference samples of known composition, relating laser-induced plasma spectroscopy (LIPS) intensity ratios, content of atomic species and number of laser pulses. Such a method represents a refinement of the standard LIPS quantification approach based on calibration curves, which is extended here to the generation of significantly deep craters into the material under investigation up to several hundred microns. The depth dependence of the calibration surfaces measured is discussed in the framework of a simplified model of depth-dependent plasma temperature. © Springer-Verlag Berlin Heidelberg 2014 |
| abstractGer |
Abstract This work presents new calibration procedures for deep elemental depth profile analysis of bronze artifacts. A simple ablation model is developed for the estimation of the ablation rate and hence for deriving the depth spatial calibration scale. Elemental quantification is obtained through the construction of calibration surfaces, using reference samples of known composition, relating laser-induced plasma spectroscopy (LIPS) intensity ratios, content of atomic species and number of laser pulses. Such a method represents a refinement of the standard LIPS quantification approach based on calibration curves, which is extended here to the generation of significantly deep craters into the material under investigation up to several hundred microns. The depth dependence of the calibration surfaces measured is discussed in the framework of a simplified model of depth-dependent plasma temperature. © Springer-Verlag Berlin Heidelberg 2014 |
| abstract_unstemmed |
Abstract This work presents new calibration procedures for deep elemental depth profile analysis of bronze artifacts. A simple ablation model is developed for the estimation of the ablation rate and hence for deriving the depth spatial calibration scale. Elemental quantification is obtained through the construction of calibration surfaces, using reference samples of known composition, relating laser-induced plasma spectroscopy (LIPS) intensity ratios, content of atomic species and number of laser pulses. Such a method represents a refinement of the standard LIPS quantification approach based on calibration curves, which is extended here to the generation of significantly deep craters into the material under investigation up to several hundred microns. The depth dependence of the calibration surfaces measured is discussed in the framework of a simplified model of depth-dependent plasma temperature. © Springer-Verlag Berlin Heidelberg 2014 |
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Depth-dependent calibration for quantitative elemental depth profiling of copper alloys using laser-induced plasma spectroscopy |
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