Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials
Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most...
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Gespeichert in:
| Autor*in: |
Baldan, A. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2008 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media, LLC 2008 |
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| Übergeordnetes Werk: |
Enthalten in: International journal of thermophysics - Springer US, 1980, 30(2008), 1 vom: 02. Juli, Seite 325-333 |
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| Übergeordnetes Werk: |
volume:30 ; year:2008 ; number:1 ; day:02 ; month:07 ; pages:325-333 |
| Links: |
|---|
| DOI / URN: |
10.1007/s10765-008-0476-z |
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OLC2076470131 |
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| 520 | |a Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. | ||
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10.1007/s10765-008-0476-z doi (DE-627)OLC2076470131 (DE-He213)s10765-008-0476-z-p DE-627 ger DE-627 rakwb eng 530 VZ Baldan, A. verfasserin aut Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials 2008 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2008 Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. Adiabatic calorimetry Benzene High-purity liquid reference material Purity determination Bosma, R. aut Peruzzi, A. aut van der Veen, A. M. H. aut Shimizu, Y. aut Enthalten in International journal of thermophysics Springer US, 1980 30(2008), 1 vom: 02. Juli, Seite 325-333 (DE-627)130512540 (DE-600)764389-5 (DE-576)016085965 0195-928X nnns volume:30 year:2008 number:1 day:02 month:07 pages:325-333 https://doi.org/10.1007/s10765-008-0476-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY GBV_ILN_62 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2050 GBV_ILN_4012 GBV_ILN_4700 AR 30 2008 1 02 07 325-333 |
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10.1007/s10765-008-0476-z doi (DE-627)OLC2076470131 (DE-He213)s10765-008-0476-z-p DE-627 ger DE-627 rakwb eng 530 VZ Baldan, A. verfasserin aut Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials 2008 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2008 Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. Adiabatic calorimetry Benzene High-purity liquid reference material Purity determination Bosma, R. aut Peruzzi, A. aut van der Veen, A. M. H. aut Shimizu, Y. aut Enthalten in International journal of thermophysics Springer US, 1980 30(2008), 1 vom: 02. Juli, Seite 325-333 (DE-627)130512540 (DE-600)764389-5 (DE-576)016085965 0195-928X nnns volume:30 year:2008 number:1 day:02 month:07 pages:325-333 https://doi.org/10.1007/s10765-008-0476-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY GBV_ILN_62 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2050 GBV_ILN_4012 GBV_ILN_4700 AR 30 2008 1 02 07 325-333 |
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10.1007/s10765-008-0476-z doi (DE-627)OLC2076470131 (DE-He213)s10765-008-0476-z-p DE-627 ger DE-627 rakwb eng 530 VZ Baldan, A. verfasserin aut Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials 2008 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2008 Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. Adiabatic calorimetry Benzene High-purity liquid reference material Purity determination Bosma, R. aut Peruzzi, A. aut van der Veen, A. M. H. aut Shimizu, Y. aut Enthalten in International journal of thermophysics Springer US, 1980 30(2008), 1 vom: 02. Juli, Seite 325-333 (DE-627)130512540 (DE-600)764389-5 (DE-576)016085965 0195-928X nnns volume:30 year:2008 number:1 day:02 month:07 pages:325-333 https://doi.org/10.1007/s10765-008-0476-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY GBV_ILN_62 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2050 GBV_ILN_4012 GBV_ILN_4700 AR 30 2008 1 02 07 325-333 |
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10.1007/s10765-008-0476-z doi (DE-627)OLC2076470131 (DE-He213)s10765-008-0476-z-p DE-627 ger DE-627 rakwb eng 530 VZ Baldan, A. verfasserin aut Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials 2008 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2008 Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. Adiabatic calorimetry Benzene High-purity liquid reference material Purity determination Bosma, R. aut Peruzzi, A. aut van der Veen, A. M. H. aut Shimizu, Y. aut Enthalten in International journal of thermophysics Springer US, 1980 30(2008), 1 vom: 02. Juli, Seite 325-333 (DE-627)130512540 (DE-600)764389-5 (DE-576)016085965 0195-928X nnns volume:30 year:2008 number:1 day:02 month:07 pages:325-333 https://doi.org/10.1007/s10765-008-0476-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY GBV_ILN_62 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2050 GBV_ILN_4012 GBV_ILN_4700 AR 30 2008 1 02 07 325-333 |
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10.1007/s10765-008-0476-z doi (DE-627)OLC2076470131 (DE-He213)s10765-008-0476-z-p DE-627 ger DE-627 rakwb eng 530 VZ Baldan, A. verfasserin aut Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials 2008 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2008 Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. Adiabatic calorimetry Benzene High-purity liquid reference material Purity determination Bosma, R. aut Peruzzi, A. aut van der Veen, A. M. H. aut Shimizu, Y. aut Enthalten in International journal of thermophysics Springer US, 1980 30(2008), 1 vom: 02. Juli, Seite 325-333 (DE-627)130512540 (DE-600)764389-5 (DE-576)016085965 0195-928X nnns volume:30 year:2008 number:1 day:02 month:07 pages:325-333 https://doi.org/10.1007/s10765-008-0476-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY GBV_ILN_62 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2050 GBV_ILN_4012 GBV_ILN_4700 AR 30 2008 1 02 07 325-333 |
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Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials |
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Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials |
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Baldan, A. |
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International journal of thermophysics |
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Baldan, A. Bosma, R. Peruzzi, A. van der Veen, A. M. H. Shimizu, Y. |
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adiabatic calorimetry as support to the certification of high-purity liquid reference materials |
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Adiabatic Calorimetry as Support to the Certification of High-Purity Liquid Reference Materials |
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Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. © Springer Science+Business Media, LLC 2008 |
| abstractGer |
Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. © Springer Science+Business Media, LLC 2008 |
| abstract_unstemmed |
Abstract The certification of high-purity liquid reference materials is supported by several analytical techniques (e.g., gas chromatography, liquid chromatography, Karl Fischer coulometry, inductively coupled plasma mass spectrometry, differential scanning calorimetry, adiabatic calorimetry). Most of them provide information on a limited set of specific impurities present in the sample (indirect methods). Adiabatic calorimetry [1] complementarily provides the overall molar fraction of impurities with sensitivity down to few μmol · $ mol^{−1} $ without giving any information about the nature of the impurities present in the sample (direct method). As the combination of adiabatic calorimetry with one (or more than one) indirect chemical techniques was regarded as an optimal methodology, NMi VSL developed an adiabatic calorimetry facility for the purity determination of high-purity liquid reference materials [2]. Within the framework of collaboration with NMIJ, a benzene-certified reference material (NMIJ CRM 4002) from NMIJ was analyzed by adiabatic calorimetry at NMi VSL. The results of this measurement are reported in this paper. Good agreement with the NMIJ-certified purity value (99.992 ± 0.003) cmol · $ mol^{−1} $ was found. The influence of different data analysis approaches (e.g., extrapolation functions, melting ranges) on the measurement results is reported. The uncertainty of the measured purity was estimated. © Springer Science+Business Media, LLC 2008 |
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