Synthesis of high surface area and plate-like Magnesium Oxide nanoparticles by pH-controlled precipitation method
Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall metho...
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| Autor*in: |
Sreekanth, R. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021 |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021 |
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| Übergeordnetes Werk: |
Enthalten in: Applied physics. A, Materials science & processing - Springer Berlin Heidelberg, 1981, 127(2021), 10 vom: 28. Sept. |
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| Übergeordnetes Werk: |
volume:127 ; year:2021 ; number:10 ; day:28 ; month:09 |
| Links: |
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| DOI / URN: |
10.1007/s00339-021-04939-2 |
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OLC2077052597 |
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| 520 | |a Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall method. The Rietveld refinement was carried out to find cell dimensions, micro-strain, and $ Mg^{2+} $ vacancies. The Rietveld refinement showed a good fit with R-factors. SEM images show agglomerated plate-like morphology. The surface area data were evaluated by Brunner–Emmet–Teller method and found to be 246.95 g/$ m^{2} $ with an average pore diameter of 6.721 nm. Smaller size and high surface area of MgO contributed to the observed band gap value of 5.8 eV. These nanoparticles with small size and high surface area have potential applications as catalysts and in the next generation biosensor applications. Graphic abstract | ||
| 650 | 4 | |a MgO nanoparticles | |
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10.1007/s00339-021-04939-2 doi (DE-627)OLC2077052597 (DE-He213)s00339-021-04939-2-p DE-627 ger DE-627 rakwb eng 530 620 VZ 530 VZ UA 9001.A VZ rvk Sreekanth, R. verfasserin aut Synthesis of high surface area and plate-like Magnesium Oxide nanoparticles by pH-controlled precipitation method 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021 Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall method. The Rietveld refinement was carried out to find cell dimensions, micro-strain, and $ Mg^{2+} $ vacancies. The Rietveld refinement showed a good fit with R-factors. SEM images show agglomerated plate-like morphology. The surface area data were evaluated by Brunner–Emmet–Teller method and found to be 246.95 g/$ m^{2} $ with an average pore diameter of 6.721 nm. Smaller size and high surface area of MgO contributed to the observed band gap value of 5.8 eV. These nanoparticles with small size and high surface area have potential applications as catalysts and in the next generation biosensor applications. Graphic abstract MgO nanoparticles X-ray diffraction Williamson-Hall plot BET Rietveld refinement Pattar, Jayadev (orcid)0000-0002-4315-9842 aut Anupama, A. V. aut Mallikarjunaswamy, A. M. M. aut Enthalten in Applied physics. A, Materials science & processing Springer Berlin Heidelberg, 1981 127(2021), 10 vom: 28. Sept. (DE-627)129861340 (DE-600)283365-7 (DE-576)015171930 0947-8396 nnns volume:127 year:2021 number:10 day:28 month:09 https://doi.org/10.1007/s00339-021-04939-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2018 GBV_ILN_4277 UA 9001.A AR 127 2021 10 28 09 |
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10.1007/s00339-021-04939-2 doi (DE-627)OLC2077052597 (DE-He213)s00339-021-04939-2-p DE-627 ger DE-627 rakwb eng 530 620 VZ 530 VZ UA 9001.A VZ rvk Sreekanth, R. verfasserin aut Synthesis of high surface area and plate-like Magnesium Oxide nanoparticles by pH-controlled precipitation method 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021 Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall method. The Rietveld refinement was carried out to find cell dimensions, micro-strain, and $ Mg^{2+} $ vacancies. The Rietveld refinement showed a good fit with R-factors. SEM images show agglomerated plate-like morphology. The surface area data were evaluated by Brunner–Emmet–Teller method and found to be 246.95 g/$ m^{2} $ with an average pore diameter of 6.721 nm. Smaller size and high surface area of MgO contributed to the observed band gap value of 5.8 eV. These nanoparticles with small size and high surface area have potential applications as catalysts and in the next generation biosensor applications. Graphic abstract MgO nanoparticles X-ray diffraction Williamson-Hall plot BET Rietveld refinement Pattar, Jayadev (orcid)0000-0002-4315-9842 aut Anupama, A. V. aut Mallikarjunaswamy, A. M. M. aut Enthalten in Applied physics. A, Materials science & processing Springer Berlin Heidelberg, 1981 127(2021), 10 vom: 28. Sept. (DE-627)129861340 (DE-600)283365-7 (DE-576)015171930 0947-8396 nnns volume:127 year:2021 number:10 day:28 month:09 https://doi.org/10.1007/s00339-021-04939-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2018 GBV_ILN_4277 UA 9001.A AR 127 2021 10 28 09 |
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10.1007/s00339-021-04939-2 doi (DE-627)OLC2077052597 (DE-He213)s00339-021-04939-2-p DE-627 ger DE-627 rakwb eng 530 620 VZ 530 VZ UA 9001.A VZ rvk Sreekanth, R. verfasserin aut Synthesis of high surface area and plate-like Magnesium Oxide nanoparticles by pH-controlled precipitation method 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021 Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall method. The Rietveld refinement was carried out to find cell dimensions, micro-strain, and $ Mg^{2+} $ vacancies. The Rietveld refinement showed a good fit with R-factors. SEM images show agglomerated plate-like morphology. The surface area data were evaluated by Brunner–Emmet–Teller method and found to be 246.95 g/$ m^{2} $ with an average pore diameter of 6.721 nm. Smaller size and high surface area of MgO contributed to the observed band gap value of 5.8 eV. These nanoparticles with small size and high surface area have potential applications as catalysts and in the next generation biosensor applications. Graphic abstract MgO nanoparticles X-ray diffraction Williamson-Hall plot BET Rietveld refinement Pattar, Jayadev (orcid)0000-0002-4315-9842 aut Anupama, A. V. aut Mallikarjunaswamy, A. M. M. aut Enthalten in Applied physics. A, Materials science & processing Springer Berlin Heidelberg, 1981 127(2021), 10 vom: 28. Sept. (DE-627)129861340 (DE-600)283365-7 (DE-576)015171930 0947-8396 nnns volume:127 year:2021 number:10 day:28 month:09 https://doi.org/10.1007/s00339-021-04939-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2018 GBV_ILN_4277 UA 9001.A AR 127 2021 10 28 09 |
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10.1007/s00339-021-04939-2 doi (DE-627)OLC2077052597 (DE-He213)s00339-021-04939-2-p DE-627 ger DE-627 rakwb eng 530 620 VZ 530 VZ UA 9001.A VZ rvk Sreekanth, R. verfasserin aut Synthesis of high surface area and plate-like Magnesium Oxide nanoparticles by pH-controlled precipitation method 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021 Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall method. The Rietveld refinement was carried out to find cell dimensions, micro-strain, and $ Mg^{2+} $ vacancies. The Rietveld refinement showed a good fit with R-factors. SEM images show agglomerated plate-like morphology. The surface area data were evaluated by Brunner–Emmet–Teller method and found to be 246.95 g/$ m^{2} $ with an average pore diameter of 6.721 nm. Smaller size and high surface area of MgO contributed to the observed band gap value of 5.8 eV. These nanoparticles with small size and high surface area have potential applications as catalysts and in the next generation biosensor applications. Graphic abstract MgO nanoparticles X-ray diffraction Williamson-Hall plot BET Rietveld refinement Pattar, Jayadev (orcid)0000-0002-4315-9842 aut Anupama, A. V. aut Mallikarjunaswamy, A. M. M. aut Enthalten in Applied physics. A, Materials science & processing Springer Berlin Heidelberg, 1981 127(2021), 10 vom: 28. Sept. (DE-627)129861340 (DE-600)283365-7 (DE-576)015171930 0947-8396 nnns volume:127 year:2021 number:10 day:28 month:09 https://doi.org/10.1007/s00339-021-04939-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2018 GBV_ILN_4277 UA 9001.A AR 127 2021 10 28 09 |
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Sreekanth, R. |
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synthesis of high surface area and plate-like magnesium oxide nanoparticles by ph-controlled precipitation method |
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Synthesis of high surface area and plate-like Magnesium Oxide nanoparticles by pH-controlled precipitation method |
| abstract |
Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall method. The Rietveld refinement was carried out to find cell dimensions, micro-strain, and $ Mg^{2+} $ vacancies. The Rietveld refinement showed a good fit with R-factors. SEM images show agglomerated plate-like morphology. The surface area data were evaluated by Brunner–Emmet–Teller method and found to be 246.95 g/$ m^{2} $ with an average pore diameter of 6.721 nm. Smaller size and high surface area of MgO contributed to the observed band gap value of 5.8 eV. These nanoparticles with small size and high surface area have potential applications as catalysts and in the next generation biosensor applications. Graphic abstract © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021 |
| abstractGer |
Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall method. The Rietveld refinement was carried out to find cell dimensions, micro-strain, and $ Mg^{2+} $ vacancies. The Rietveld refinement showed a good fit with R-factors. SEM images show agglomerated plate-like morphology. The surface area data were evaluated by Brunner–Emmet–Teller method and found to be 246.95 g/$ m^{2} $ with an average pore diameter of 6.721 nm. Smaller size and high surface area of MgO contributed to the observed band gap value of 5.8 eV. These nanoparticles with small size and high surface area have potential applications as catalysts and in the next generation biosensor applications. Graphic abstract © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021 |
| abstract_unstemmed |
Synthesized magnesium oxide (MgO) nanoparticles by a simple pH-controlled precipitation method using Mg ($ SO_{4} $)2 as a precursor. The XRD spectra of MgO recorded at room temperature showed FCC structure. Crystallite size for synthesized MgO was calculated using Scherrer and Williamson-Hall method. The Rietveld refinement was carried out to find cell dimensions, micro-strain, and $ Mg^{2+} $ vacancies. The Rietveld refinement showed a good fit with R-factors. SEM images show agglomerated plate-like morphology. The surface area data were evaluated by Brunner–Emmet–Teller method and found to be 246.95 g/$ m^{2} $ with an average pore diameter of 6.721 nm. Smaller size and high surface area of MgO contributed to the observed band gap value of 5.8 eV. These nanoparticles with small size and high surface area have potential applications as catalysts and in the next generation biosensor applications. Graphic abstract © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021 |
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Synthesis of high surface area and plate-like Magnesium Oxide nanoparticles by pH-controlled precipitation method |
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Pattar, Jayadev Anupama, A. V. Mallikarjunaswamy, A. M. M. |
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