Synthesis of Copper and Lead Ion Imprinted Polymer Submicron Spheres to Remove $ Cu^{2+} $ and $ Pb^{2+} $
Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polyme...
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| Autor*in: |
Jiang, Yang [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021 |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of inorganic and organometallic polymers and materials - Springer US, 1991, 31(2021), 12 vom: 16. Juli, Seite 4628-4636 |
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| Übergeordnetes Werk: |
volume:31 ; year:2021 ; number:12 ; day:16 ; month:07 ; pages:4628-4636 |
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| DOI / URN: |
10.1007/s10904-021-02065-3 |
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| Katalog-ID: |
OLC2077519533 |
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| 520 | |a Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. | ||
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10.1007/s10904-021-02065-3 doi (DE-627)OLC2077519533 (DE-He213)s10904-021-02065-3-p DE-627 ger DE-627 rakwb eng 660 VZ Jiang, Yang verfasserin aut Synthesis of Copper and Lead Ion Imprinted Polymer Submicron Spheres to Remove $ Cu^{2+} $ and $ Pb^{2+} $ 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. Ion imprinted polymer Precipitation polymerization Adsorption capacity Selectivity Tang, Bolin aut Zhao, Pengfei aut Xi, Man aut Li, Yi aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 31(2021), 12 vom: 16. Juli, Seite 4628-4636 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:31 year:2021 number:12 day:16 month:07 pages:4628-4636 https://doi.org/10.1007/s10904-021-02065-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 31 2021 12 16 07 4628-4636 |
| spelling |
10.1007/s10904-021-02065-3 doi (DE-627)OLC2077519533 (DE-He213)s10904-021-02065-3-p DE-627 ger DE-627 rakwb eng 660 VZ Jiang, Yang verfasserin aut Synthesis of Copper and Lead Ion Imprinted Polymer Submicron Spheres to Remove $ Cu^{2+} $ and $ Pb^{2+} $ 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. Ion imprinted polymer Precipitation polymerization Adsorption capacity Selectivity Tang, Bolin aut Zhao, Pengfei aut Xi, Man aut Li, Yi aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 31(2021), 12 vom: 16. Juli, Seite 4628-4636 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:31 year:2021 number:12 day:16 month:07 pages:4628-4636 https://doi.org/10.1007/s10904-021-02065-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 31 2021 12 16 07 4628-4636 |
| allfields_unstemmed |
10.1007/s10904-021-02065-3 doi (DE-627)OLC2077519533 (DE-He213)s10904-021-02065-3-p DE-627 ger DE-627 rakwb eng 660 VZ Jiang, Yang verfasserin aut Synthesis of Copper and Lead Ion Imprinted Polymer Submicron Spheres to Remove $ Cu^{2+} $ and $ Pb^{2+} $ 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. Ion imprinted polymer Precipitation polymerization Adsorption capacity Selectivity Tang, Bolin aut Zhao, Pengfei aut Xi, Man aut Li, Yi aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 31(2021), 12 vom: 16. Juli, Seite 4628-4636 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:31 year:2021 number:12 day:16 month:07 pages:4628-4636 https://doi.org/10.1007/s10904-021-02065-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 31 2021 12 16 07 4628-4636 |
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10.1007/s10904-021-02065-3 doi (DE-627)OLC2077519533 (DE-He213)s10904-021-02065-3-p DE-627 ger DE-627 rakwb eng 660 VZ Jiang, Yang verfasserin aut Synthesis of Copper and Lead Ion Imprinted Polymer Submicron Spheres to Remove $ Cu^{2+} $ and $ Pb^{2+} $ 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. Ion imprinted polymer Precipitation polymerization Adsorption capacity Selectivity Tang, Bolin aut Zhao, Pengfei aut Xi, Man aut Li, Yi aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 31(2021), 12 vom: 16. Juli, Seite 4628-4636 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:31 year:2021 number:12 day:16 month:07 pages:4628-4636 https://doi.org/10.1007/s10904-021-02065-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 31 2021 12 16 07 4628-4636 |
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10.1007/s10904-021-02065-3 doi (DE-627)OLC2077519533 (DE-He213)s10904-021-02065-3-p DE-627 ger DE-627 rakwb eng 660 VZ Jiang, Yang verfasserin aut Synthesis of Copper and Lead Ion Imprinted Polymer Submicron Spheres to Remove $ Cu^{2+} $ and $ Pb^{2+} $ 2021 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. Ion imprinted polymer Precipitation polymerization Adsorption capacity Selectivity Tang, Bolin aut Zhao, Pengfei aut Xi, Man aut Li, Yi aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 31(2021), 12 vom: 16. Juli, Seite 4628-4636 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:31 year:2021 number:12 day:16 month:07 pages:4628-4636 https://doi.org/10.1007/s10904-021-02065-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 31 2021 12 16 07 4628-4636 |
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synthesis of copper and lead ion imprinted polymer submicron spheres to remove $ cu^{2+} $ and $ pb^{2+} $ |
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Synthesis of Copper and Lead Ion Imprinted Polymer Submicron Spheres to Remove $ Cu^{2+} $ and $ Pb^{2+} $ |
| abstract |
Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 |
| abstractGer |
Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 |
| abstract_unstemmed |
Abstract In this paper, Methacrylic acid (MAA) and 4-vinyl pyridine (4-VP) as functional monomers, Ethylene glycol two methyl acrylate (EGDMA) as crosslinking agent, isopropyl alcohol as the solvent, prepared the Cu(II)- and Pb(II)- imprinted polymers (IIPs) submicron spheres by precipitation polymerization. The presence/absence of the template ion in the preparation of the imprinted polymer was confirmed by EDX spectroscopy, and the structure of the particles was investigated using IR, SEM and BET analysis. From different components of crosslinker/monomer (C/M) ratio analysis, C/M at 1:3 was the optimal ratio for preparing IIPs. Atomic absorption spectroscopy (AAS) was characterized the imprinted polymers absorption behavior. The results show that the maximum adsorption capacity of $ Cu^{2+} $ and $ Pb^{2+} $ -imprinted polymer were 26.9 mg $ g^{−1} $ and 25.3 mg $ g^{−1} $, respectively. They also have good adsorption capacity and superior selectivity property for $ Cu^{2+} $ and $ Pb^{2+} $ in water, respectively. The selectivity factors (α) for $ Ni^{2+} $, $ Zn^{2+} $, $ Co^{2+} $ and $ Fe^{2+} $ were 16.5 ($ Cu^{2+} $) and 12.1 ($ Pb^{2+} $), 13.8 ($ Cu^{2+} $) and 16.2 ($ Pb^{2+} $), 10.8 ($ Cu^{2+} $) and 10.1 ($ Pb^{2+} $), 20.4 ($ Cu^{2+} $) and 20.7 ($ Pb^{2+} $), respectively. The regeneration experiment result demonstrates an excellent re-utilization property of these two type IIPs, after ten uses, the adsorption capacity can maintain above 60%. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 |
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