A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods
Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization technique...
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Gespeichert in:
| Autor*in: |
Durgababu, G. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science / Materials in electronics - Springer US, 1990, 33(2022), 10 vom: 10. März, Seite 7973-7982 |
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| Übergeordnetes Werk: |
volume:33 ; year:2022 ; number:10 ; day:10 ; month:03 ; pages:7973-7982 |
| Links: |
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| DOI / URN: |
10.1007/s10854-022-07947-x |
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| Katalog-ID: |
OLC2078378763 |
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| 520 | |a Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization techniques to unveil the structural, lattice strain, and optical properties. Among these, Powder X-ray diffraction studies of the grown crystals revealed that the crystal system remains same as orthorhombic with few high intense peaks observed at (111), (013), and (213) and lattice strain evaluated in case of SR grown crystals. The high transmittance was observed from UV–Visible spectroscopy studies for SR grown crystals as compared to conventional grown crystals. The cut-off wavelengths were measured at ~ 420 nm, 430 nm and band gap energies at 3.025 eV, 3.052 eV, respectively, for Conventional and SR method grown crystals. The photoluminescent spectra revealed red shift in the emission peaks of grown crystals which are in good coherence with UV–Visible spectra. The crystalline perfection of grown 4C3N crystals were assessed by HRXRD technique. The full width at half maximum values of the diffracted planes (308) confirmed that the crystalline perfection of SR grown crystals is better than that of the crystals grown by SEST method which could be responsible for the enhancement of optical transparency of SR grown crystals. | ||
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10.1007/s10854-022-07947-x doi (DE-627)OLC2078378763 (DE-He213)s10854-022-07947-x-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Durgababu, G. verfasserin aut A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization techniques to unveil the structural, lattice strain, and optical properties. Among these, Powder X-ray diffraction studies of the grown crystals revealed that the crystal system remains same as orthorhombic with few high intense peaks observed at (111), (013), and (213) and lattice strain evaluated in case of SR grown crystals. The high transmittance was observed from UV–Visible spectroscopy studies for SR grown crystals as compared to conventional grown crystals. The cut-off wavelengths were measured at ~ 420 nm, 430 nm and band gap energies at 3.025 eV, 3.052 eV, respectively, for Conventional and SR method grown crystals. The photoluminescent spectra revealed red shift in the emission peaks of grown crystals which are in good coherence with UV–Visible spectra. The crystalline perfection of grown 4C3N crystals were assessed by HRXRD technique. The full width at half maximum values of the diffracted planes (308) confirmed that the crystalline perfection of SR grown crystals is better than that of the crystals grown by SEST method which could be responsible for the enhancement of optical transparency of SR grown crystals. Bhagavannarayana, G. (orcid)0000-0003-3638-5945 aut Kamalesh, T. aut Govindaraj, R. aut Nagaraju, G. J. aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 33(2022), 10 vom: 10. März, Seite 7973-7982 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:33 year:2022 number:10 day:10 month:03 pages:7973-7982 https://doi.org/10.1007/s10854-022-07947-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 AR 33 2022 10 10 03 7973-7982 |
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10.1007/s10854-022-07947-x doi (DE-627)OLC2078378763 (DE-He213)s10854-022-07947-x-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Durgababu, G. verfasserin aut A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization techniques to unveil the structural, lattice strain, and optical properties. Among these, Powder X-ray diffraction studies of the grown crystals revealed that the crystal system remains same as orthorhombic with few high intense peaks observed at (111), (013), and (213) and lattice strain evaluated in case of SR grown crystals. The high transmittance was observed from UV–Visible spectroscopy studies for SR grown crystals as compared to conventional grown crystals. The cut-off wavelengths were measured at ~ 420 nm, 430 nm and band gap energies at 3.025 eV, 3.052 eV, respectively, for Conventional and SR method grown crystals. The photoluminescent spectra revealed red shift in the emission peaks of grown crystals which are in good coherence with UV–Visible spectra. The crystalline perfection of grown 4C3N crystals were assessed by HRXRD technique. The full width at half maximum values of the diffracted planes (308) confirmed that the crystalline perfection of SR grown crystals is better than that of the crystals grown by SEST method which could be responsible for the enhancement of optical transparency of SR grown crystals. Bhagavannarayana, G. (orcid)0000-0003-3638-5945 aut Kamalesh, T. aut Govindaraj, R. aut Nagaraju, G. J. aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 33(2022), 10 vom: 10. März, Seite 7973-7982 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:33 year:2022 number:10 day:10 month:03 pages:7973-7982 https://doi.org/10.1007/s10854-022-07947-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 AR 33 2022 10 10 03 7973-7982 |
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10.1007/s10854-022-07947-x doi (DE-627)OLC2078378763 (DE-He213)s10854-022-07947-x-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Durgababu, G. verfasserin aut A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization techniques to unveil the structural, lattice strain, and optical properties. Among these, Powder X-ray diffraction studies of the grown crystals revealed that the crystal system remains same as orthorhombic with few high intense peaks observed at (111), (013), and (213) and lattice strain evaluated in case of SR grown crystals. The high transmittance was observed from UV–Visible spectroscopy studies for SR grown crystals as compared to conventional grown crystals. The cut-off wavelengths were measured at ~ 420 nm, 430 nm and band gap energies at 3.025 eV, 3.052 eV, respectively, for Conventional and SR method grown crystals. The photoluminescent spectra revealed red shift in the emission peaks of grown crystals which are in good coherence with UV–Visible spectra. The crystalline perfection of grown 4C3N crystals were assessed by HRXRD technique. The full width at half maximum values of the diffracted planes (308) confirmed that the crystalline perfection of SR grown crystals is better than that of the crystals grown by SEST method which could be responsible for the enhancement of optical transparency of SR grown crystals. Bhagavannarayana, G. (orcid)0000-0003-3638-5945 aut Kamalesh, T. aut Govindaraj, R. aut Nagaraju, G. J. aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 33(2022), 10 vom: 10. März, Seite 7973-7982 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:33 year:2022 number:10 day:10 month:03 pages:7973-7982 https://doi.org/10.1007/s10854-022-07947-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 AR 33 2022 10 10 03 7973-7982 |
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10.1007/s10854-022-07947-x doi (DE-627)OLC2078378763 (DE-He213)s10854-022-07947-x-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Durgababu, G. verfasserin aut A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization techniques to unveil the structural, lattice strain, and optical properties. Among these, Powder X-ray diffraction studies of the grown crystals revealed that the crystal system remains same as orthorhombic with few high intense peaks observed at (111), (013), and (213) and lattice strain evaluated in case of SR grown crystals. The high transmittance was observed from UV–Visible spectroscopy studies for SR grown crystals as compared to conventional grown crystals. The cut-off wavelengths were measured at ~ 420 nm, 430 nm and band gap energies at 3.025 eV, 3.052 eV, respectively, for Conventional and SR method grown crystals. The photoluminescent spectra revealed red shift in the emission peaks of grown crystals which are in good coherence with UV–Visible spectra. The crystalline perfection of grown 4C3N crystals were assessed by HRXRD technique. The full width at half maximum values of the diffracted planes (308) confirmed that the crystalline perfection of SR grown crystals is better than that of the crystals grown by SEST method which could be responsible for the enhancement of optical transparency of SR grown crystals. Bhagavannarayana, G. (orcid)0000-0003-3638-5945 aut Kamalesh, T. aut Govindaraj, R. aut Nagaraju, G. J. aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 33(2022), 10 vom: 10. März, Seite 7973-7982 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:33 year:2022 number:10 day:10 month:03 pages:7973-7982 https://doi.org/10.1007/s10854-022-07947-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 AR 33 2022 10 10 03 7973-7982 |
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A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods |
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A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods |
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Durgababu, G. |
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Journal of materials science / Materials in electronics |
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Journal of materials science / Materials in electronics |
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eng |
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600 - Technology |
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2022 |
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7973 |
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Durgababu, G. Bhagavannarayana, G. Kamalesh, T. Govindaraj, R. Nagaraju, G. J. |
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33 |
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Durgababu, G. |
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10.1007/s10854-022-07947-x |
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600 670 620 |
| title_sort |
a comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and sankaranarayanan–ramasamy methods |
| title_auth |
A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods |
| abstract |
Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization techniques to unveil the structural, lattice strain, and optical properties. Among these, Powder X-ray diffraction studies of the grown crystals revealed that the crystal system remains same as orthorhombic with few high intense peaks observed at (111), (013), and (213) and lattice strain evaluated in case of SR grown crystals. The high transmittance was observed from UV–Visible spectroscopy studies for SR grown crystals as compared to conventional grown crystals. The cut-off wavelengths were measured at ~ 420 nm, 430 nm and band gap energies at 3.025 eV, 3.052 eV, respectively, for Conventional and SR method grown crystals. The photoluminescent spectra revealed red shift in the emission peaks of grown crystals which are in good coherence with UV–Visible spectra. The crystalline perfection of grown 4C3N crystals were assessed by HRXRD technique. The full width at half maximum values of the diffracted planes (308) confirmed that the crystalline perfection of SR grown crystals is better than that of the crystals grown by SEST method which could be responsible for the enhancement of optical transparency of SR grown crystals. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
| abstractGer |
Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization techniques to unveil the structural, lattice strain, and optical properties. Among these, Powder X-ray diffraction studies of the grown crystals revealed that the crystal system remains same as orthorhombic with few high intense peaks observed at (111), (013), and (213) and lattice strain evaluated in case of SR grown crystals. The high transmittance was observed from UV–Visible spectroscopy studies for SR grown crystals as compared to conventional grown crystals. The cut-off wavelengths were measured at ~ 420 nm, 430 nm and band gap energies at 3.025 eV, 3.052 eV, respectively, for Conventional and SR method grown crystals. The photoluminescent spectra revealed red shift in the emission peaks of grown crystals which are in good coherence with UV–Visible spectra. The crystalline perfection of grown 4C3N crystals were assessed by HRXRD technique. The full width at half maximum values of the diffracted planes (308) confirmed that the crystalline perfection of SR grown crystals is better than that of the crystals grown by SEST method which could be responsible for the enhancement of optical transparency of SR grown crystals. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
| abstract_unstemmed |
Abstract Single crystal of novel organic 4-chloro 3-nitrobenzophenone (4C3N) is grown by both the conventional slow evaporation solution technique (SEST) and Sankarnarayanan–Ramasamy (SR) method from acetone as solvent medium. The grown crystals were subjected to different characterization techniques to unveil the structural, lattice strain, and optical properties. Among these, Powder X-ray diffraction studies of the grown crystals revealed that the crystal system remains same as orthorhombic with few high intense peaks observed at (111), (013), and (213) and lattice strain evaluated in case of SR grown crystals. The high transmittance was observed from UV–Visible spectroscopy studies for SR grown crystals as compared to conventional grown crystals. The cut-off wavelengths were measured at ~ 420 nm, 430 nm and band gap energies at 3.025 eV, 3.052 eV, respectively, for Conventional and SR method grown crystals. The photoluminescent spectra revealed red shift in the emission peaks of grown crystals which are in good coherence with UV–Visible spectra. The crystalline perfection of grown 4C3N crystals were assessed by HRXRD technique. The full width at half maximum values of the diffracted planes (308) confirmed that the crystalline perfection of SR grown crystals is better than that of the crystals grown by SEST method which could be responsible for the enhancement of optical transparency of SR grown crystals. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 |
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10 |
| title_short |
A comparative study of 4-chloro 3-nitro benzophenone crystals grown by slow evaporation solution and Sankaranarayanan–Ramasamy methods |
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https://doi.org/10.1007/s10854-022-07947-x |
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Bhagavannarayana, G. Kamalesh, T. Govindaraj, R. Nagaraju, G. J. |
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Bhagavannarayana, G. Kamalesh, T. Govindaraj, R. Nagaraju, G. J. |
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| up_date |
2024-07-03T20:09:46.455Z |
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