Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction
Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bime...
Ausführliche Beschreibung
Gespeichert in:
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Orfi, Hamza [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of inorganic and organometallic polymers and materials - Springer US, 1991, 32(2022), 6 vom: 15. März, Seite 2192-2208 |
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| Übergeordnetes Werk: |
volume:32 ; year:2022 ; number:6 ; day:15 ; month:03 ; pages:2192-2208 |
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| DOI / URN: |
10.1007/s10904-022-02262-8 |
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| 245 | 1 | 0 | |a Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction |
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| 520 | |a Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. | ||
| 650 | 4 | |a Heterogeneous catalysis | |
| 650 | 4 | |a Mesoporous natural phosphate | |
| 650 | 4 | |a Core–shell nanoparticles | |
| 650 | 4 | |a Silver | |
| 650 | 4 | |a Cobalt oxide | |
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| 700 | 1 | |a Mekkaoui, Ayoub Abdelkader |0 (orcid)0000-0002-7336-1961 |4 aut | |
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| 700 | 1 | |a Metin, Önder |4 aut | |
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10.1007/s10904-022-02262-8 doi (DE-627)OLC207897899X (DE-He213)s10904-022-02262-8-p DE-627 ger DE-627 rakwb eng 660 VZ Orfi, Hamza verfasserin aut Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. Heterogeneous catalysis Mesoporous natural phosphate Core–shell nanoparticles Silver Cobalt oxide Nitroarenes Mekkaoui, Ayoub Abdelkader (orcid)0000-0002-7336-1961 aut Sündü, Buse aut Laayati, Mouhsine aut Labyad, Salim Adam aut El Firdoussi, Larbi aut Metin, Önder aut El Houssame, Soufiane (orcid)0000-0003-1319-8522 aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 32(2022), 6 vom: 15. März, Seite 2192-2208 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:32 year:2022 number:6 day:15 month:03 pages:2192-2208 https://doi.org/10.1007/s10904-022-02262-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 32 2022 6 15 03 2192-2208 |
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10.1007/s10904-022-02262-8 doi (DE-627)OLC207897899X (DE-He213)s10904-022-02262-8-p DE-627 ger DE-627 rakwb eng 660 VZ Orfi, Hamza verfasserin aut Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. Heterogeneous catalysis Mesoporous natural phosphate Core–shell nanoparticles Silver Cobalt oxide Nitroarenes Mekkaoui, Ayoub Abdelkader (orcid)0000-0002-7336-1961 aut Sündü, Buse aut Laayati, Mouhsine aut Labyad, Salim Adam aut El Firdoussi, Larbi aut Metin, Önder aut El Houssame, Soufiane (orcid)0000-0003-1319-8522 aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 32(2022), 6 vom: 15. März, Seite 2192-2208 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:32 year:2022 number:6 day:15 month:03 pages:2192-2208 https://doi.org/10.1007/s10904-022-02262-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 32 2022 6 15 03 2192-2208 |
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10.1007/s10904-022-02262-8 doi (DE-627)OLC207897899X (DE-He213)s10904-022-02262-8-p DE-627 ger DE-627 rakwb eng 660 VZ Orfi, Hamza verfasserin aut Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. Heterogeneous catalysis Mesoporous natural phosphate Core–shell nanoparticles Silver Cobalt oxide Nitroarenes Mekkaoui, Ayoub Abdelkader (orcid)0000-0002-7336-1961 aut Sündü, Buse aut Laayati, Mouhsine aut Labyad, Salim Adam aut El Firdoussi, Larbi aut Metin, Önder aut El Houssame, Soufiane (orcid)0000-0003-1319-8522 aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 32(2022), 6 vom: 15. März, Seite 2192-2208 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:32 year:2022 number:6 day:15 month:03 pages:2192-2208 https://doi.org/10.1007/s10904-022-02262-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 32 2022 6 15 03 2192-2208 |
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10.1007/s10904-022-02262-8 doi (DE-627)OLC207897899X (DE-He213)s10904-022-02262-8-p DE-627 ger DE-627 rakwb eng 660 VZ Orfi, Hamza verfasserin aut Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. Heterogeneous catalysis Mesoporous natural phosphate Core–shell nanoparticles Silver Cobalt oxide Nitroarenes Mekkaoui, Ayoub Abdelkader (orcid)0000-0002-7336-1961 aut Sündü, Buse aut Laayati, Mouhsine aut Labyad, Salim Adam aut El Firdoussi, Larbi aut Metin, Önder aut El Houssame, Soufiane (orcid)0000-0003-1319-8522 aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 32(2022), 6 vom: 15. März, Seite 2192-2208 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:32 year:2022 number:6 day:15 month:03 pages:2192-2208 https://doi.org/10.1007/s10904-022-02262-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 32 2022 6 15 03 2192-2208 |
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10.1007/s10904-022-02262-8 doi (DE-627)OLC207897899X (DE-He213)s10904-022-02262-8-p DE-627 ger DE-627 rakwb eng 660 VZ Orfi, Hamza verfasserin aut Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. Heterogeneous catalysis Mesoporous natural phosphate Core–shell nanoparticles Silver Cobalt oxide Nitroarenes Mekkaoui, Ayoub Abdelkader (orcid)0000-0002-7336-1961 aut Sündü, Buse aut Laayati, Mouhsine aut Labyad, Salim Adam aut El Firdoussi, Larbi aut Metin, Önder aut El Houssame, Soufiane (orcid)0000-0003-1319-8522 aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 32(2022), 6 vom: 15. März, Seite 2192-2208 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:32 year:2022 number:6 day:15 month:03 pages:2192-2208 https://doi.org/10.1007/s10904-022-02262-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 AR 32 2022 6 15 03 2192-2208 |
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Enthalten in Journal of inorganic and organometallic polymers and materials 32(2022), 6 vom: 15. März, Seite 2192-2208 volume:32 year:2022 number:6 day:15 month:03 pages:2192-2208 |
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660 VZ Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction Heterogeneous catalysis Mesoporous natural phosphate Core–shell nanoparticles Silver Cobalt oxide Nitroarenes |
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Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction |
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Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction |
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Orfi, Hamza Mekkaoui, Ayoub Abdelkader Sündü, Buse Laayati, Mouhsine Labyad, Salim Adam El Firdoussi, Larbi Metin, Önder El Houssame, Soufiane |
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ag, $ co_{3} $$ o_{4} $, ag–$ co_{3} $$ o_{4,} $ and ag/$ co_{3} $$ o_{4} $ nanoparticles decorated mesoporous natural phosphate: effect of metal synergy and preparation method on the catalytic reduction reaction |
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Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction |
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Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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Abstract Addressed herein is a facile method for the preparation of cobalt-silver ($ Co_{x} $–$ Ag_{y} $) nanoparticles decorated mesoporous natural phosphate (m-NP). Various $ Co_{x} $–$ Ag_{y} $NP nanocatalysts were prepared in different forms of Ag and $ Co_{3} $$ O_{4} $ including mono- and bimetallic active sites. The bimetallic nanocatalysts were prepared by two different preparation methods, namely in-situ (Ag–$ Co_{3} $$ O_{4} $) and ex-situ (Ag/$ Co_{3} $$ O_{4} $ core–shell). In the first step, colloidal $ Co_{x} $–$ Ag_{y} $ nanoparticles were synthesized in solution and their formation was monitored by using UV–Visible spectroscopy. Furthermore, the obtained nanoparticles were characterized by XRD and IR spectroscopy. All nanoparticles were deposited on m-NP using a simple wetness impregnation method followed by a calcination at 500 °C. The prepared nanocatalysts were fully characterized by advanced analytical techniques including IR, XRD, XPS, SEM–EDX, FESEM, and TEM. The catalytic reduction of 4-nitrophenol was studied as a model reaction to investigate the effect of synergy created between the metals, oxidation state, catalyst structure, and preparation method on their catalytic activity. Accordingly, reaction kinetics and comparative study of various colloidal $ Co_{x} $–$ Ag_{y} $ and m-NP supported nanocatalysts in the reduction of 4-nitrophenol was carried out. The optimized conditions were used to study the substrate scope of the catalytic reduction over various nitroarenes. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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Ag, $ Co_{3} $$ O_{4} $, Ag–$ Co_{3} $$ O_{4,} $ and Ag/$ Co_{3} $$ O_{4} $ Nanoparticles Decorated Mesoporous Natural Phosphate: Effect of Metal Synergy and Preparation Method on the Catalytic Reduction Reaction |
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