Synthesis and Characterization of Modified Poly(vinyl alcohol) Membrane and Study of Its Enhanced Water-Induced Shape-Memory Behavior
Abstract Nowadays, shape-memory polymers (SMPs) are regarded as smart materials. To get new functions, SMPs should be modified or fabricated in the composite form. Herein, poly (vinyl alcohol) (PVA) membranes were prepared by a solution casting method and subsequently modified using a solution of bo...
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| Autor*in: |
Panda, Pradeep Kumar [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Schlagwörter: |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of polymers and the environment - Springer US, 2000, 30(2022), 8 vom: 18. Apr., Seite 3409-3419 |
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| Übergeordnetes Werk: |
volume:30 ; year:2022 ; number:8 ; day:18 ; month:04 ; pages:3409-3419 |
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| DOI / URN: |
10.1007/s10924-022-02454-w |
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OLC2079178911 |
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| 520 | |a Abstract Nowadays, shape-memory polymers (SMPs) are regarded as smart materials. To get new functions, SMPs should be modified or fabricated in the composite form. Herein, poly (vinyl alcohol) (PVA) membranes were prepared by a solution casting method and subsequently modified using a solution of borax and glutaraldehyde. The physicochemical properties, including the mechanism of water-induced shape-memory behavior of all prepared membranes, were systematically studied. From the results obtained, it is observed that the modification agents into the PVA polymer matrix, enhanced the properties of the prepared modified membranes. The modified membranes have more hydrophilicity than pure PVA membrane. The gel fraction value of modified membranes was more than 90%. The crystallinity of modified samples was lower than pure PVA membrane due to the destruction of original inter and intra-molecular hydrogen bonding. In addition, mechanical properties (tensile strength and elongation at break) were evaluated for both modified and unmodified PVA membranes. The shape recovery time of modified membranes were much lower than that of pure PVA membrane. The shape recovery values of all samples were almost 100%. Increase in the water immersion time (0 to 14 s) of the PVAG (modified with borax) sample, the storage modulus and glass transition temperature was drastically decreases from 9711 to 4226 MPa, and 35.03 to 12.35 °C, respectively. Further, in vitro biodegradation studies were conducted for all the prepared samples. Therefore, the above fabricated membranes can be applied in the biomedical field where water is the primary stimulus. | ||
| 650 | 4 | |a Poly (vinyl alcohol) | |
| 650 | 4 | |a Membrane technology | |
| 650 | 4 | |a Modification | |
| 650 | 4 | |a Shape-memory properties | |
| 650 | 4 | |a Biodegradation | |
| 700 | 1 | |a Dash, Pranjyan |4 aut | |
| 700 | 1 | |a Biswal, Achyuta Kumar |4 aut | |
| 700 | 1 | |a Chang, Yen-Hsiang |4 aut | |
| 700 | 1 | |a Misra, Pramila Kumari |4 aut | |
| 700 | 1 | |a Yang, Jen-Ming |0 (orcid)0000-0003-4586-573X |4 aut | |
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10.1007/s10924-022-02454-w doi (DE-627)OLC2079178911 (DE-He213)s10924-022-02454-w-p DE-627 ger DE-627 rakwb eng 660 VZ 58.53$jAbfallwirtschaft bkl 58.52$jTechnischer Bodenschutz$jtechnischer Gewässerschutz bkl 43.50$jUmweltbelastungen bkl Panda, Pradeep Kumar verfasserin aut Synthesis and Characterization of Modified Poly(vinyl alcohol) Membrane and Study of Its Enhanced Water-Induced Shape-Memory Behavior 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Nowadays, shape-memory polymers (SMPs) are regarded as smart materials. To get new functions, SMPs should be modified or fabricated in the composite form. Herein, poly (vinyl alcohol) (PVA) membranes were prepared by a solution casting method and subsequently modified using a solution of borax and glutaraldehyde. The physicochemical properties, including the mechanism of water-induced shape-memory behavior of all prepared membranes, were systematically studied. From the results obtained, it is observed that the modification agents into the PVA polymer matrix, enhanced the properties of the prepared modified membranes. The modified membranes have more hydrophilicity than pure PVA membrane. The gel fraction value of modified membranes was more than 90%. The crystallinity of modified samples was lower than pure PVA membrane due to the destruction of original inter and intra-molecular hydrogen bonding. In addition, mechanical properties (tensile strength and elongation at break) were evaluated for both modified and unmodified PVA membranes. The shape recovery time of modified membranes were much lower than that of pure PVA membrane. The shape recovery values of all samples were almost 100%. Increase in the water immersion time (0 to 14 s) of the PVAG (modified with borax) sample, the storage modulus and glass transition temperature was drastically decreases from 9711 to 4226 MPa, and 35.03 to 12.35 °C, respectively. Further, in vitro biodegradation studies were conducted for all the prepared samples. Therefore, the above fabricated membranes can be applied in the biomedical field where water is the primary stimulus. Poly (vinyl alcohol) Membrane technology Modification Shape-memory properties Biodegradation Dash, Pranjyan aut Biswal, Achyuta Kumar aut Chang, Yen-Hsiang aut Misra, Pramila Kumari aut Yang, Jen-Ming (orcid)0000-0003-4586-573X aut Enthalten in Journal of polymers and the environment Springer US, 2000 30(2022), 8 vom: 18. Apr., Seite 3409-3419 (DE-627)325700176 (DE-600)2039366-0 (DE-576)9325700174 1566-2543 nnns volume:30 year:2022 number:8 day:18 month:04 pages:3409-3419 https://doi.org/10.1007/s10924-022-02454-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 58.53$jAbfallwirtschaft VZ 106418831 (DE-625)106418831 58.52$jTechnischer Bodenschutz$jtechnischer Gewässerschutz VZ 106420747 (DE-625)106420747 43.50$jUmweltbelastungen VZ 106416782 (DE-625)106416782 AR 30 2022 8 18 04 3409-3419 |
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10.1007/s10924-022-02454-w doi (DE-627)OLC2079178911 (DE-He213)s10924-022-02454-w-p DE-627 ger DE-627 rakwb eng 660 VZ 58.53$jAbfallwirtschaft bkl 58.52$jTechnischer Bodenschutz$jtechnischer Gewässerschutz bkl 43.50$jUmweltbelastungen bkl Panda, Pradeep Kumar verfasserin aut Synthesis and Characterization of Modified Poly(vinyl alcohol) Membrane and Study of Its Enhanced Water-Induced Shape-Memory Behavior 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Nowadays, shape-memory polymers (SMPs) are regarded as smart materials. To get new functions, SMPs should be modified or fabricated in the composite form. Herein, poly (vinyl alcohol) (PVA) membranes were prepared by a solution casting method and subsequently modified using a solution of borax and glutaraldehyde. The physicochemical properties, including the mechanism of water-induced shape-memory behavior of all prepared membranes, were systematically studied. From the results obtained, it is observed that the modification agents into the PVA polymer matrix, enhanced the properties of the prepared modified membranes. The modified membranes have more hydrophilicity than pure PVA membrane. The gel fraction value of modified membranes was more than 90%. The crystallinity of modified samples was lower than pure PVA membrane due to the destruction of original inter and intra-molecular hydrogen bonding. In addition, mechanical properties (tensile strength and elongation at break) were evaluated for both modified and unmodified PVA membranes. The shape recovery time of modified membranes were much lower than that of pure PVA membrane. The shape recovery values of all samples were almost 100%. Increase in the water immersion time (0 to 14 s) of the PVAG (modified with borax) sample, the storage modulus and glass transition temperature was drastically decreases from 9711 to 4226 MPa, and 35.03 to 12.35 °C, respectively. Further, in vitro biodegradation studies were conducted for all the prepared samples. Therefore, the above fabricated membranes can be applied in the biomedical field where water is the primary stimulus. Poly (vinyl alcohol) Membrane technology Modification Shape-memory properties Biodegradation Dash, Pranjyan aut Biswal, Achyuta Kumar aut Chang, Yen-Hsiang aut Misra, Pramila Kumari aut Yang, Jen-Ming (orcid)0000-0003-4586-573X aut Enthalten in Journal of polymers and the environment Springer US, 2000 30(2022), 8 vom: 18. Apr., Seite 3409-3419 (DE-627)325700176 (DE-600)2039366-0 (DE-576)9325700174 1566-2543 nnns volume:30 year:2022 number:8 day:18 month:04 pages:3409-3419 https://doi.org/10.1007/s10924-022-02454-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 58.53$jAbfallwirtschaft VZ 106418831 (DE-625)106418831 58.52$jTechnischer Bodenschutz$jtechnischer Gewässerschutz VZ 106420747 (DE-625)106420747 43.50$jUmweltbelastungen VZ 106416782 (DE-625)106416782 AR 30 2022 8 18 04 3409-3419 |
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10.1007/s10924-022-02454-w doi (DE-627)OLC2079178911 (DE-He213)s10924-022-02454-w-p DE-627 ger DE-627 rakwb eng 660 VZ 58.53$jAbfallwirtschaft bkl 58.52$jTechnischer Bodenschutz$jtechnischer Gewässerschutz bkl 43.50$jUmweltbelastungen bkl Panda, Pradeep Kumar verfasserin aut Synthesis and Characterization of Modified Poly(vinyl alcohol) Membrane and Study of Its Enhanced Water-Induced Shape-Memory Behavior 2022 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract Nowadays, shape-memory polymers (SMPs) are regarded as smart materials. To get new functions, SMPs should be modified or fabricated in the composite form. Herein, poly (vinyl alcohol) (PVA) membranes were prepared by a solution casting method and subsequently modified using a solution of borax and glutaraldehyde. The physicochemical properties, including the mechanism of water-induced shape-memory behavior of all prepared membranes, were systematically studied. From the results obtained, it is observed that the modification agents into the PVA polymer matrix, enhanced the properties of the prepared modified membranes. The modified membranes have more hydrophilicity than pure PVA membrane. The gel fraction value of modified membranes was more than 90%. The crystallinity of modified samples was lower than pure PVA membrane due to the destruction of original inter and intra-molecular hydrogen bonding. In addition, mechanical properties (tensile strength and elongation at break) were evaluated for both modified and unmodified PVA membranes. The shape recovery time of modified membranes were much lower than that of pure PVA membrane. The shape recovery values of all samples were almost 100%. Increase in the water immersion time (0 to 14 s) of the PVAG (modified with borax) sample, the storage modulus and glass transition temperature was drastically decreases from 9711 to 4226 MPa, and 35.03 to 12.35 °C, respectively. Further, in vitro biodegradation studies were conducted for all the prepared samples. Therefore, the above fabricated membranes can be applied in the biomedical field where water is the primary stimulus. Poly (vinyl alcohol) Membrane technology Modification Shape-memory properties Biodegradation Dash, Pranjyan aut Biswal, Achyuta Kumar aut Chang, Yen-Hsiang aut Misra, Pramila Kumari aut Yang, Jen-Ming (orcid)0000-0003-4586-573X aut Enthalten in Journal of polymers and the environment Springer US, 2000 30(2022), 8 vom: 18. Apr., Seite 3409-3419 (DE-627)325700176 (DE-600)2039366-0 (DE-576)9325700174 1566-2543 nnns volume:30 year:2022 number:8 day:18 month:04 pages:3409-3419 https://doi.org/10.1007/s10924-022-02454-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 58.53$jAbfallwirtschaft VZ 106418831 (DE-625)106418831 58.52$jTechnischer Bodenschutz$jtechnischer Gewässerschutz VZ 106420747 (DE-625)106420747 43.50$jUmweltbelastungen VZ 106416782 (DE-625)106416782 AR 30 2022 8 18 04 3409-3419 |
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Synthesis and Characterization of Modified Poly(vinyl alcohol) Membrane and Study of Its Enhanced Water-Induced Shape-Memory Behavior |
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Abstract Nowadays, shape-memory polymers (SMPs) are regarded as smart materials. To get new functions, SMPs should be modified or fabricated in the composite form. Herein, poly (vinyl alcohol) (PVA) membranes were prepared by a solution casting method and subsequently modified using a solution of borax and glutaraldehyde. The physicochemical properties, including the mechanism of water-induced shape-memory behavior of all prepared membranes, were systematically studied. From the results obtained, it is observed that the modification agents into the PVA polymer matrix, enhanced the properties of the prepared modified membranes. The modified membranes have more hydrophilicity than pure PVA membrane. The gel fraction value of modified membranes was more than 90%. The crystallinity of modified samples was lower than pure PVA membrane due to the destruction of original inter and intra-molecular hydrogen bonding. In addition, mechanical properties (tensile strength and elongation at break) were evaluated for both modified and unmodified PVA membranes. The shape recovery time of modified membranes were much lower than that of pure PVA membrane. The shape recovery values of all samples were almost 100%. Increase in the water immersion time (0 to 14 s) of the PVAG (modified with borax) sample, the storage modulus and glass transition temperature was drastically decreases from 9711 to 4226 MPa, and 35.03 to 12.35 °C, respectively. Further, in vitro biodegradation studies were conducted for all the prepared samples. Therefore, the above fabricated membranes can be applied in the biomedical field where water is the primary stimulus. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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Abstract Nowadays, shape-memory polymers (SMPs) are regarded as smart materials. To get new functions, SMPs should be modified or fabricated in the composite form. Herein, poly (vinyl alcohol) (PVA) membranes were prepared by a solution casting method and subsequently modified using a solution of borax and glutaraldehyde. The physicochemical properties, including the mechanism of water-induced shape-memory behavior of all prepared membranes, were systematically studied. From the results obtained, it is observed that the modification agents into the PVA polymer matrix, enhanced the properties of the prepared modified membranes. The modified membranes have more hydrophilicity than pure PVA membrane. The gel fraction value of modified membranes was more than 90%. The crystallinity of modified samples was lower than pure PVA membrane due to the destruction of original inter and intra-molecular hydrogen bonding. In addition, mechanical properties (tensile strength and elongation at break) were evaluated for both modified and unmodified PVA membranes. The shape recovery time of modified membranes were much lower than that of pure PVA membrane. The shape recovery values of all samples were almost 100%. Increase in the water immersion time (0 to 14 s) of the PVAG (modified with borax) sample, the storage modulus and glass transition temperature was drastically decreases from 9711 to 4226 MPa, and 35.03 to 12.35 °C, respectively. Further, in vitro biodegradation studies were conducted for all the prepared samples. Therefore, the above fabricated membranes can be applied in the biomedical field where water is the primary stimulus. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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Abstract Nowadays, shape-memory polymers (SMPs) are regarded as smart materials. To get new functions, SMPs should be modified or fabricated in the composite form. Herein, poly (vinyl alcohol) (PVA) membranes were prepared by a solution casting method and subsequently modified using a solution of borax and glutaraldehyde. The physicochemical properties, including the mechanism of water-induced shape-memory behavior of all prepared membranes, were systematically studied. From the results obtained, it is observed that the modification agents into the PVA polymer matrix, enhanced the properties of the prepared modified membranes. The modified membranes have more hydrophilicity than pure PVA membrane. The gel fraction value of modified membranes was more than 90%. The crystallinity of modified samples was lower than pure PVA membrane due to the destruction of original inter and intra-molecular hydrogen bonding. In addition, mechanical properties (tensile strength and elongation at break) were evaluated for both modified and unmodified PVA membranes. The shape recovery time of modified membranes were much lower than that of pure PVA membrane. The shape recovery values of all samples were almost 100%. Increase in the water immersion time (0 to 14 s) of the PVAG (modified with borax) sample, the storage modulus and glass transition temperature was drastically decreases from 9711 to 4226 MPa, and 35.03 to 12.35 °C, respectively. Further, in vitro biodegradation studies were conducted for all the prepared samples. Therefore, the above fabricated membranes can be applied in the biomedical field where water is the primary stimulus. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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