A study of micropyretic reactions in the Mo–Si–Al ternary system
Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomi...
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| Autor*in: |
Fu, Ming [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
1997 |
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| Systematik: |
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| Anmerkung: |
© The Materials Research Society 1997 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials research - Springer International Publishing, 1986, 12(1997), 6 vom: Juni, Seite 1481-1491 |
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| Übergeordnetes Werk: |
volume:12 ; year:1997 ; number:6 ; month:06 ; pages:1481-1491 |
| Links: |
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| DOI / URN: |
10.1557/JMR.1997.0204 |
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OLC2122146060 |
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| 520 | |a Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. | ||
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10.1557/JMR.1997.0204 doi (DE-627)OLC2122146060 (DE-He213)JMR.1997.0204-p DE-627 ger DE-627 rakwb eng 670 VZ VA 5350 VZ rvk Fu, Ming verfasserin aut A study of micropyretic reactions in the Mo–Si–Al ternary system 1997 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Materials Research Society 1997 Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. Enthalten in Journal of materials research Springer International Publishing, 1986 12(1997), 6 vom: Juni, Seite 1481-1491 (DE-627)129206288 (DE-600)54876-5 (DE-576)01445744X 0884-2914 nnns volume:12 year:1997 number:6 month:06 pages:1481-1491 https://doi.org/10.1557/JMR.1997.0204 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_70 GBV_ILN_100 GBV_ILN_130 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2010 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4319 GBV_ILN_4323 VA 5350 AR 12 1997 6 06 1481-1491 |
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10.1557/JMR.1997.0204 doi (DE-627)OLC2122146060 (DE-He213)JMR.1997.0204-p DE-627 ger DE-627 rakwb eng 670 VZ VA 5350 VZ rvk Fu, Ming verfasserin aut A study of micropyretic reactions in the Mo–Si–Al ternary system 1997 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Materials Research Society 1997 Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. Enthalten in Journal of materials research Springer International Publishing, 1986 12(1997), 6 vom: Juni, Seite 1481-1491 (DE-627)129206288 (DE-600)54876-5 (DE-576)01445744X 0884-2914 nnns volume:12 year:1997 number:6 month:06 pages:1481-1491 https://doi.org/10.1557/JMR.1997.0204 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_70 GBV_ILN_100 GBV_ILN_130 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2010 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4319 GBV_ILN_4323 VA 5350 AR 12 1997 6 06 1481-1491 |
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10.1557/JMR.1997.0204 doi (DE-627)OLC2122146060 (DE-He213)JMR.1997.0204-p DE-627 ger DE-627 rakwb eng 670 VZ VA 5350 VZ rvk Fu, Ming verfasserin aut A study of micropyretic reactions in the Mo–Si–Al ternary system 1997 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Materials Research Society 1997 Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. Enthalten in Journal of materials research Springer International Publishing, 1986 12(1997), 6 vom: Juni, Seite 1481-1491 (DE-627)129206288 (DE-600)54876-5 (DE-576)01445744X 0884-2914 nnns volume:12 year:1997 number:6 month:06 pages:1481-1491 https://doi.org/10.1557/JMR.1997.0204 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_70 GBV_ILN_100 GBV_ILN_130 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2010 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4319 GBV_ILN_4323 VA 5350 AR 12 1997 6 06 1481-1491 |
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10.1557/JMR.1997.0204 doi (DE-627)OLC2122146060 (DE-He213)JMR.1997.0204-p DE-627 ger DE-627 rakwb eng 670 VZ VA 5350 VZ rvk Fu, Ming verfasserin aut A study of micropyretic reactions in the Mo–Si–Al ternary system 1997 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Materials Research Society 1997 Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. Enthalten in Journal of materials research Springer International Publishing, 1986 12(1997), 6 vom: Juni, Seite 1481-1491 (DE-627)129206288 (DE-600)54876-5 (DE-576)01445744X 0884-2914 nnns volume:12 year:1997 number:6 month:06 pages:1481-1491 https://doi.org/10.1557/JMR.1997.0204 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_70 GBV_ILN_100 GBV_ILN_130 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2010 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4319 GBV_ILN_4323 VA 5350 AR 12 1997 6 06 1481-1491 |
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10.1557/JMR.1997.0204 doi (DE-627)OLC2122146060 (DE-He213)JMR.1997.0204-p DE-627 ger DE-627 rakwb eng 670 VZ VA 5350 VZ rvk Fu, Ming verfasserin aut A study of micropyretic reactions in the Mo–Si–Al ternary system 1997 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Materials Research Society 1997 Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. Enthalten in Journal of materials research Springer International Publishing, 1986 12(1997), 6 vom: Juni, Seite 1481-1491 (DE-627)129206288 (DE-600)54876-5 (DE-576)01445744X 0884-2914 nnns volume:12 year:1997 number:6 month:06 pages:1481-1491 https://doi.org/10.1557/JMR.1997.0204 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_70 GBV_ILN_100 GBV_ILN_130 GBV_ILN_602 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2010 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4319 GBV_ILN_4323 VA 5350 AR 12 1997 6 06 1481-1491 |
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A study of micropyretic reactions in the Mo–Si–Al ternary system |
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Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. © The Materials Research Society 1997 |
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Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. © The Materials Research Society 1997 |
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Abstract Micropyretic synthesis technique employs self-sustaining exothermic (combustion) reactions for the preparation of various ceramic, intermetallic, and composite materials. In the present work, the combustion reactions of Mo and Si with Al additions have been systematically studied. The atomic mixtures of the reactant powders are chosen to be Mo + (2 − x)Si + xAl with x = 0−0.4. In comparison with the Mo + 2Si reaction which leads to the formation of $ MoSi_{2} $, the substitution of Al for Si decreases the sample ignition temperature, but increases the intensity of the combustion reactions. In addition, the substitution of Al for Si results in the formation of a ternary intermetallic phase, called molybdenum alumino-silicide Mo(Si, Al)2, in the synthesized product. When the content of Al in the reactant mixtures reaches 0.4, nearly single phase Mo(Si, Al)2 is obtained and no $ MoSi_{2} $ is detected in the reaction product. These influences are analyzed by using x-ray diffraction (XRD), scanning electron microscopy (SEM), and differential thermal analysis (DTA). The effect of Al additions on the reaction mechanism is also discussed. © The Materials Research Society 1997 |
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