Carbamoyl Derivatives of a Pyridine-Based Tetraamine

The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	K. Bilakhiya, Anvarhusen [verfasserIn] Heinemann, Frank W. Grohmann, Andreas

Format:	Artikel

Erschienen:	2007

Systematik:	VA 8360

Anmerkung:	© 1946 – 2014: Verlag der Zeitschrift für Naturforschung

Übergeordnetes Werk:	Enthalten in: Zeitschrift für Naturforschung. B, Chemical sciences - Verlag der Zeitschrift für Naturforschung, 1947, 62(2007), 4 vom: 01. Apr., Seite 519-522
Übergeordnetes Werk:	volume:62 ; year:2007 ; number:4 ; day:01 ; month:04 ; pages:519-522

Links:	Volltext

DOI / URN:	10.1515/znb-2007-0405

Katalog-ID:	OLC2138874435

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520			\|a The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups.
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allfields	10.1515/znb-2007-0405 doi (DE-627)OLC2138874435 (DE-B1597)znb-2007-0405-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk K. Bilakhiya, Anvarhusen verfasserin aut Carbamoyl Derivatives of a Pyridine-Based Tetraamine 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups. Heinemann, Frank W. aut Grohmann, Andreas aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 62(2007), 4 vom: 01. Apr., Seite 519-522 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:62 year:2007 number:4 day:01 month:04 pages:519-522 https://doi.org/10.1515/znb-2007-0405 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_120 GBV_ILN_121 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4116 GBV_ILN_4125 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4317 GBV_ILN_4320 VA 8360 AR 62 2007 4 01 04 519-522
spelling	10.1515/znb-2007-0405 doi (DE-627)OLC2138874435 (DE-B1597)znb-2007-0405-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk K. Bilakhiya, Anvarhusen verfasserin aut Carbamoyl Derivatives of a Pyridine-Based Tetraamine 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups. Heinemann, Frank W. aut Grohmann, Andreas aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 62(2007), 4 vom: 01. Apr., Seite 519-522 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:62 year:2007 number:4 day:01 month:04 pages:519-522 https://doi.org/10.1515/znb-2007-0405 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_120 GBV_ILN_121 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4116 GBV_ILN_4125 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4317 GBV_ILN_4320 VA 8360 AR 62 2007 4 01 04 519-522
allfields_unstemmed	10.1515/znb-2007-0405 doi (DE-627)OLC2138874435 (DE-B1597)znb-2007-0405-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk K. Bilakhiya, Anvarhusen verfasserin aut Carbamoyl Derivatives of a Pyridine-Based Tetraamine 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups. Heinemann, Frank W. aut Grohmann, Andreas aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 62(2007), 4 vom: 01. Apr., Seite 519-522 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:62 year:2007 number:4 day:01 month:04 pages:519-522 https://doi.org/10.1515/znb-2007-0405 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_120 GBV_ILN_121 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4116 GBV_ILN_4125 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4317 GBV_ILN_4320 VA 8360 AR 62 2007 4 01 04 519-522
allfieldsGer	10.1515/znb-2007-0405 doi (DE-627)OLC2138874435 (DE-B1597)znb-2007-0405-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk K. Bilakhiya, Anvarhusen verfasserin aut Carbamoyl Derivatives of a Pyridine-Based Tetraamine 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups. Heinemann, Frank W. aut Grohmann, Andreas aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 62(2007), 4 vom: 01. Apr., Seite 519-522 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:62 year:2007 number:4 day:01 month:04 pages:519-522 https://doi.org/10.1515/znb-2007-0405 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_120 GBV_ILN_121 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4116 GBV_ILN_4125 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4317 GBV_ILN_4320 VA 8360 AR 62 2007 4 01 04 519-522
allfieldsSound	10.1515/znb-2007-0405 doi (DE-627)OLC2138874435 (DE-B1597)znb-2007-0405-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk K. Bilakhiya, Anvarhusen verfasserin aut Carbamoyl Derivatives of a Pyridine-Based Tetraamine 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups. Heinemann, Frank W. aut Grohmann, Andreas aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 62(2007), 4 vom: 01. Apr., Seite 519-522 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:62 year:2007 number:4 day:01 month:04 pages:519-522 https://doi.org/10.1515/znb-2007-0405 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_120 GBV_ILN_121 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4116 GBV_ILN_4125 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4317 GBV_ILN_4320 VA 8360 AR 62 2007 4 01 04 519-522
source	Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences 62(2007), 4 vom: 01. Apr., Seite 519-522 volume:62 year:2007 number:4 day:01 month:04 pages:519-522
sourceStr	Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences 62(2007), 4 vom: 01. Apr., Seite 519-522 volume:62 year:2007 number:4 day:01 month:04 pages:519-522
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author	K. Bilakhiya, Anvarhusen
spellingShingle	K. Bilakhiya, Anvarhusen ddc 540 rvk VA 8360 Carbamoyl Derivatives of a Pyridine-Based Tetraamine
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topic_title	540 VZ VA 8360 VZ rvk Carbamoyl Derivatives of a Pyridine-Based Tetraamine
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title	Carbamoyl Derivatives of a Pyridine-Based Tetraamine
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title_full	Carbamoyl Derivatives of a Pyridine-Based Tetraamine
author_sort	K. Bilakhiya, Anvarhusen
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author_browse	K. Bilakhiya, Anvarhusen Heinemann, Frank W. Grohmann, Andreas
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title_sort	carbamoyl derivatives of a pyridine-based tetraamine
title_auth	Carbamoyl Derivatives of a Pyridine-Based Tetraamine
abstract	The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
abstractGer	The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
abstract_unstemmed	The reaction of four equivalents of phenyl or tert-butyl isocyanate with the pyridine-derived tetraamine 2,6-$ C_{3} $$ H_{3} $N[CMe($ CH_{2} $$ NH_{2} $)2]2 in toluene gives high yields of the quadruply ureido substituted products 2,6-$ C_{5} $$ H_{3} $N[CMe($ CH_{2} $R)2]2 [R = -NH(CO)NHPh and -NH(CO)$ NH^{t} $Bu]. Full spectroscopic data for both compounds are given. A single crystal X-ray structure determination of the phenyl derivative reveals an intricate network of both intra- and intermolecular hydrogen bonds involving the C=O and both NH functionalities in all ureido groups. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
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title_short	Carbamoyl Derivatives of a Pyridine-Based Tetraamine
url	https://doi.org/10.1515/znb-2007-0405
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