Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)

By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4}...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Drewes, C. [verfasserIn] Preetz, W.

Format:	Artikel

Erschienen:	1999

Systematik:	VA 8360

Anmerkung:	© 1946 – 2014: Verlag der Zeitschrift für Naturforschung

Übergeordnetes Werk:	Enthalten in: Zeitschrift für Naturforschung. B, Chemical sciences - Verlag der Zeitschrift für Naturforschung, 1947, 54(1999), 10 vom: 01. Okt., Seite 1219-1221
Übergeordnetes Werk:	volume:54 ; year:1999 ; number:10 ; day:01 ; month:10 ; pages:1219-1221

Links:	Volltext

DOI / URN:	10.1515/znb-1999-1001

Katalog-ID:	OLC2139458869

Internformat


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520			\|a By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations.
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Indexfelder

author_variant	c d cd w p wp
matchkey_str	article:09320776:1999----::yteepkrnnkitlsrkuvnimnbnymnntoerhdolshxbrtsnhsspcradrsasrcuefim
hierarchy_sort_str	1999
publishDate	1999
allfields	10.1515/znb-1999-1001 doi (DE-627)OLC2139458869 (DE-B1597)znb-1999-1001-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Drewes, C. verfasserin aut Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-) 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations. Preetz, W. aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 54(1999), 10 vom: 01. Okt., Seite 1219-1221 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:54 year:1999 number:10 day:01 month:10 pages:1219-1221 https://doi.org/10.1515/znb-1999-1001 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_100 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2409 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4116 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4319 GBV_ILN_4320 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 54 1999 10 01 10 1219-1221
spelling	10.1515/znb-1999-1001 doi (DE-627)OLC2139458869 (DE-B1597)znb-1999-1001-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Drewes, C. verfasserin aut Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-) 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations. Preetz, W. aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 54(1999), 10 vom: 01. Okt., Seite 1219-1221 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:54 year:1999 number:10 day:01 month:10 pages:1219-1221 https://doi.org/10.1515/znb-1999-1001 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_100 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2409 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4116 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4319 GBV_ILN_4320 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 54 1999 10 01 10 1219-1221
allfields_unstemmed	10.1515/znb-1999-1001 doi (DE-627)OLC2139458869 (DE-B1597)znb-1999-1001-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Drewes, C. verfasserin aut Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-) 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations. Preetz, W. aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 54(1999), 10 vom: 01. Okt., Seite 1219-1221 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:54 year:1999 number:10 day:01 month:10 pages:1219-1221 https://doi.org/10.1515/znb-1999-1001 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_100 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2409 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4116 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4319 GBV_ILN_4320 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 54 1999 10 01 10 1219-1221
allfieldsGer	10.1515/znb-1999-1001 doi (DE-627)OLC2139458869 (DE-B1597)znb-1999-1001-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Drewes, C. verfasserin aut Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-) 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations. Preetz, W. aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 54(1999), 10 vom: 01. Okt., Seite 1219-1221 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:54 year:1999 number:10 day:01 month:10 pages:1219-1221 https://doi.org/10.1515/znb-1999-1001 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_100 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2409 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4116 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4319 GBV_ILN_4320 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 54 1999 10 01 10 1219-1221
allfieldsSound	10.1515/znb-1999-1001 doi (DE-627)OLC2139458869 (DE-B1597)znb-1999-1001-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Drewes, C. verfasserin aut Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-) 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations. Preetz, W. aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 54(1999), 10 vom: 01. Okt., Seite 1219-1221 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:54 year:1999 number:10 day:01 month:10 pages:1219-1221 https://doi.org/10.1515/znb-1999-1001 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_40 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_100 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2409 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4116 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4319 GBV_ILN_4320 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 54 1999 10 01 10 1219-1221
source	Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences 54(1999), 10 vom: 01. Okt., Seite 1219-1221 volume:54 year:1999 number:10 day:01 month:10 pages:1219-1221
sourceStr	Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences 54(1999), 10 vom: 01. Okt., Seite 1219-1221 volume:54 year:1999 number:10 day:01 month:10 pages:1219-1221
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author	Drewes, C.
spellingShingle	Drewes, C. ddc 540 rvk VA 8360 Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)
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topic_title	540 VZ VA 8360 VZ rvk Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)
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title	Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)
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title_full	Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)
author_sort	Drewes, C.
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author_browse	Drewes, C. Preetz, W.
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title_sort	synthese, spektren und kristallstruktur von cis-monobenzylmononitrotetrahydro-closo-hexaborat(2-) / synthesis, spectra and crystal structure of cis-monobenzylmononitrotetrahydro-closo-hexaborate(2-)
title_auth	Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)
abstract	By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
abstractGer	By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
abstract_unstemmed	By electrochemical oxidation of (n-$ Bu_{4} $N)[$ B_{6} $$ H_{5} $$ H^{fac} $($ CH_{2} $Ph)] in the presence of nitrite ions in dichloromethane solution cis-[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)(N $ O_{2} $)]2- is formed. X-ray diffraction analysis has been performed on a single crystal of cis-($ Ph_{4} $P)2[$ B_{6} $$ H_{4} $($ CH_{2} $Ph)($ NO_{2} $)] $ HO_{2} $$ CH_{3} $CN (triclinic, space group Pl̅ a = 11.338(5), b = 11.377(5), c = 21.081 (5) Å, α = 93.727(5), ß = 98.872(5), γ = 105.926(5)°, Z = 2). The 11B NMR spectrum is consistent with a disubstituted octahedral $ B_{6} $ cage with local $ C_{2v} $ symmetry. The IR and Raman spectra exhibit characteristic CH, $ NO_{2} $, BN, BH and $ B_{6} $ vibrations. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
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title_short	Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)
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up_date	2024-07-03T20:09:28.755Z
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Synthese, Spektren und Kristallstruktur von cis-Monobenzylmononitrotetrahydro-closo-hexaborat(2-) / Synthesis, Spectra and Crystal Structure of cis-Monobenzylmononitrotetrahydro-closo-hexaborate(2-)

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