Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid

Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipo...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Elz, Sigurd [verfasserIn] Buschauer, Armin Dräger, Martin Schunack, Walter

Format:	Artikel

Erschienen:	1983

Systematik:	VA 8360

Anmerkung:	© 1946 – 2014: Verlag der Zeitschrift für Naturforschung

Übergeordnetes Werk:	Enthalten in: Zeitschrift für Naturforschung. B, Chemical sciences - Verlag der Zeitschrift für Naturforschung, 1947, 38(1983), 10 vom: 01. Okt., Seite 1203-1207
Übergeordnetes Werk:	volume:38 ; year:1983 ; number:10 ; day:01 ; month:10 ; pages:1203-1207

Links:	Volltext

DOI / URN:	10.1515/znb-1983-1007

Katalog-ID:	OLC2140081943

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520			\|a Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds.
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allfields	10.1515/znb-1983-1007 doi (DE-627)OLC2140081943 (DE-B1597)znb-1983-1007-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Elz, Sigurd verfasserin aut Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid 1983 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds. Buschauer, Armin aut Dräger, Martin aut Schunack, Walter aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 38(1983), 10 vom: 01. Okt., Seite 1203-1207 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:38 year:1983 number:10 day:01 month:10 pages:1203-1207 https://doi.org/10.1515/znb-1983-1007 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_55 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_252 GBV_ILN_259 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2110 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4028 GBV_ILN_4029 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4103 GBV_ILN_4116 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4309 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4318 GBV_ILN_4319 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 38 1983 10 01 10 1203-1207
spelling	10.1515/znb-1983-1007 doi (DE-627)OLC2140081943 (DE-B1597)znb-1983-1007-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Elz, Sigurd verfasserin aut Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid 1983 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds. Buschauer, Armin aut Dräger, Martin aut Schunack, Walter aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 38(1983), 10 vom: 01. Okt., Seite 1203-1207 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:38 year:1983 number:10 day:01 month:10 pages:1203-1207 https://doi.org/10.1515/znb-1983-1007 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_55 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_252 GBV_ILN_259 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2110 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4028 GBV_ILN_4029 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4103 GBV_ILN_4116 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4309 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4318 GBV_ILN_4319 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 38 1983 10 01 10 1203-1207
allfields_unstemmed	10.1515/znb-1983-1007 doi (DE-627)OLC2140081943 (DE-B1597)znb-1983-1007-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Elz, Sigurd verfasserin aut Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid 1983 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds. Buschauer, Armin aut Dräger, Martin aut Schunack, Walter aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 38(1983), 10 vom: 01. Okt., Seite 1203-1207 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:38 year:1983 number:10 day:01 month:10 pages:1203-1207 https://doi.org/10.1515/znb-1983-1007 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_55 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_252 GBV_ILN_259 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2110 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4028 GBV_ILN_4029 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4103 GBV_ILN_4116 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4309 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4318 GBV_ILN_4319 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 38 1983 10 01 10 1203-1207
allfieldsGer	10.1515/znb-1983-1007 doi (DE-627)OLC2140081943 (DE-B1597)znb-1983-1007-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Elz, Sigurd verfasserin aut Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid 1983 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds. Buschauer, Armin aut Dräger, Martin aut Schunack, Walter aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 38(1983), 10 vom: 01. Okt., Seite 1203-1207 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:38 year:1983 number:10 day:01 month:10 pages:1203-1207 https://doi.org/10.1515/znb-1983-1007 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_55 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_252 GBV_ILN_259 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2110 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4028 GBV_ILN_4029 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4103 GBV_ILN_4116 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4309 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4318 GBV_ILN_4319 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 38 1983 10 01 10 1203-1207
allfieldsSound	10.1515/znb-1983-1007 doi (DE-627)OLC2140081943 (DE-B1597)znb-1983-1007-p DE-627 ger DE-627 rakwb 540 VZ 540 VZ VA 8360 VZ rvk Elz, Sigurd verfasserin aut Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid 1983 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 1946 – 2014: Verlag der Zeitschrift für Naturforschung Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds. Buschauer, Armin aut Dräger, Martin aut Schunack, Walter aut Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences Verlag der Zeitschrift für Naturforschung, 1947 38(1983), 10 vom: 01. Okt., Seite 1203-1207 (DE-627)129307386 (DE-600)124635-5 (DE-576)014504928 0932-0776 nnns volume:38 year:1983 number:10 day:01 month:10 pages:1203-1207 https://doi.org/10.1515/znb-1983-1007 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-FOR SSG-OPC-FOR GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_55 GBV_ILN_59 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_105 GBV_ILN_120 GBV_ILN_121 GBV_ILN_130 GBV_ILN_252 GBV_ILN_259 GBV_ILN_267 GBV_ILN_285 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2110 GBV_ILN_2185 GBV_ILN_2221 GBV_ILN_2237 GBV_ILN_2279 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4027 GBV_ILN_4028 GBV_ILN_4029 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4103 GBV_ILN_4116 GBV_ILN_4126 GBV_ILN_4155 GBV_ILN_4266 GBV_ILN_4277 GBV_ILN_4302 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4309 GBV_ILN_4310 GBV_ILN_4314 GBV_ILN_4315 GBV_ILN_4316 GBV_ILN_4317 GBV_ILN_4318 GBV_ILN_4319 GBV_ILN_4321 GBV_ILN_4323 GBV_ILN_4700 VA 8360 AR 38 1983 10 01 10 1203-1207
source	Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences 38(1983), 10 vom: 01. Okt., Seite 1203-1207 volume:38 year:1983 number:10 day:01 month:10 pages:1203-1207
sourceStr	Enthalten in Zeitschrift für Naturforschung. B, Chemical sciences 38(1983), 10 vom: 01. Okt., Seite 1203-1207 volume:38 year:1983 number:10 day:01 month:10 pages:1203-1207
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author	Elz, Sigurd
spellingShingle	Elz, Sigurd ddc 540 rvk VA 8360 Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid
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topic_title	540 VZ VA 8360 VZ rvk Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid
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title	Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid
ctrlnum	(DE-627)OLC2140081943 (DE-B1597)znb-1983-1007-p
title_full	Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid
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author_browse	Elz, Sigurd Buschauer, Armin Dräger, Martin Schunack, Walter
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title_sort	darstellung, eigenschaften und kristallstruktur der n-[2-(4.5.6.7-tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / preparation, properties and crystal structure of n-[2-(4.5.6.7-tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic acid
title_auth	Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid
abstract	Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
abstractGer	Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
abstract_unstemmed	Abstract During syntheses using the phthalimide rest in liquid, ethanolic or aqueous ammonia, phthalamides, phthalimides or phthalamic acids are formed depending on reaction condi-tions and work-up. As demonstrated by the synthesis of the title compound via hydrolysis of 4 with aqueous ammonia, dipolar ions of phthalamic acids are obtained if the phthal-imide-N substituent is sufficiently basic. The crystal structure of 5 • 4H2O has been determined and refined until R = 0.0878. It shows a vast system of hydrogen bonds. © 1946 – 2014: Verlag der Zeitschrift für Naturforschung
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title_short	Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid
url	https://doi.org/10.1515/znb-1983-1007
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author2	Buschauer, Armin Dräger, Martin Schunack, Walter
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doi_str	10.1515/znb-1983-1007
up_date	2024-07-03T22:19:21.456Z
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Darstellung, Eigenschaften und Kristallstruktur der N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl] -phthalamidsäure / Preparation, Properties and Crystal Structure of N-[2-(4.5.6.7-Tetrahydro-2-benzimidazolyl)-ethyl]-phthalamic Acid

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