Synthesis and Surface Active Properties of Dimeric Gemini Sulfonate Surfactants
Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reacti...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Zhao, Jinzhou [verfasserIn] |
|---|
| Format: |
Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2013 |
|---|
| Anmerkung: |
© 2014, Carl Hanser Publisher, Munich |
|---|
| Übergeordnetes Werk: |
Enthalten in: Tenside, surfactants, detergents - De Gruyter, 1986, 51(2013), 1 vom: 01. Mai, Seite 26-31 |
|---|---|
| Übergeordnetes Werk: |
volume:51 ; year:2013 ; number:1 ; day:01 ; month:05 ; pages:26-31 |
| Links: |
|---|
| DOI / URN: |
10.3139/113.110282 |
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| 520 | |a Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. | ||
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10.3139/113.110282 doi (DE-627)OLC214179479X (DE-B1597)113.110282-p DE-627 ger DE-627 rakwb eng 540 530 VZ 35.00 bkl Zhao, Jinzhou verfasserin aut Synthesis and Surface Active Properties of Dimeric Gemini Sulfonate Surfactants 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 2014, Carl Hanser Publisher, Munich Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. Zhou, Ming aut Wang, Xu aut Yang, Yan aut Enthalten in Tenside, surfactants, detergents De Gruyter, 1986 51(2013), 1 vom: 01. Mai, Seite 26-31 (DE-627)130403423 (DE-600)607624-5 (DE-576)015907090 0932-3414 nnns volume:51 year:2013 number:1 day:01 month:05 pages:26-31 https://doi.org/10.3139/113.110282 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_24 GBV_ILN_30 GBV_ILN_70 GBV_ILN_267 GBV_ILN_2234 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4307 GBV_ILN_4317 GBV_ILN_4323 35.00 VZ AR 51 2013 1 01 05 26-31 |
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10.3139/113.110282 doi (DE-627)OLC214179479X (DE-B1597)113.110282-p DE-627 ger DE-627 rakwb eng 540 530 VZ 35.00 bkl Zhao, Jinzhou verfasserin aut Synthesis and Surface Active Properties of Dimeric Gemini Sulfonate Surfactants 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 2014, Carl Hanser Publisher, Munich Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. Zhou, Ming aut Wang, Xu aut Yang, Yan aut Enthalten in Tenside, surfactants, detergents De Gruyter, 1986 51(2013), 1 vom: 01. Mai, Seite 26-31 (DE-627)130403423 (DE-600)607624-5 (DE-576)015907090 0932-3414 nnns volume:51 year:2013 number:1 day:01 month:05 pages:26-31 https://doi.org/10.3139/113.110282 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_24 GBV_ILN_30 GBV_ILN_70 GBV_ILN_267 GBV_ILN_2234 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4307 GBV_ILN_4317 GBV_ILN_4323 35.00 VZ AR 51 2013 1 01 05 26-31 |
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10.3139/113.110282 doi (DE-627)OLC214179479X (DE-B1597)113.110282-p DE-627 ger DE-627 rakwb eng 540 530 VZ 35.00 bkl Zhao, Jinzhou verfasserin aut Synthesis and Surface Active Properties of Dimeric Gemini Sulfonate Surfactants 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 2014, Carl Hanser Publisher, Munich Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. Zhou, Ming aut Wang, Xu aut Yang, Yan aut Enthalten in Tenside, surfactants, detergents De Gruyter, 1986 51(2013), 1 vom: 01. Mai, Seite 26-31 (DE-627)130403423 (DE-600)607624-5 (DE-576)015907090 0932-3414 nnns volume:51 year:2013 number:1 day:01 month:05 pages:26-31 https://doi.org/10.3139/113.110282 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_24 GBV_ILN_30 GBV_ILN_70 GBV_ILN_267 GBV_ILN_2234 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4307 GBV_ILN_4317 GBV_ILN_4323 35.00 VZ AR 51 2013 1 01 05 26-31 |
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10.3139/113.110282 doi (DE-627)OLC214179479X (DE-B1597)113.110282-p DE-627 ger DE-627 rakwb eng 540 530 VZ 35.00 bkl Zhao, Jinzhou verfasserin aut Synthesis and Surface Active Properties of Dimeric Gemini Sulfonate Surfactants 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 2014, Carl Hanser Publisher, Munich Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. Zhou, Ming aut Wang, Xu aut Yang, Yan aut Enthalten in Tenside, surfactants, detergents De Gruyter, 1986 51(2013), 1 vom: 01. Mai, Seite 26-31 (DE-627)130403423 (DE-600)607624-5 (DE-576)015907090 0932-3414 nnns volume:51 year:2013 number:1 day:01 month:05 pages:26-31 https://doi.org/10.3139/113.110282 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_24 GBV_ILN_30 GBV_ILN_70 GBV_ILN_267 GBV_ILN_2234 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4307 GBV_ILN_4317 GBV_ILN_4323 35.00 VZ AR 51 2013 1 01 05 26-31 |
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10.3139/113.110282 doi (DE-627)OLC214179479X (DE-B1597)113.110282-p DE-627 ger DE-627 rakwb eng 540 530 VZ 35.00 bkl Zhao, Jinzhou verfasserin aut Synthesis and Surface Active Properties of Dimeric Gemini Sulfonate Surfactants 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © 2014, Carl Hanser Publisher, Munich Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. Zhou, Ming aut Wang, Xu aut Yang, Yan aut Enthalten in Tenside, surfactants, detergents De Gruyter, 1986 51(2013), 1 vom: 01. Mai, Seite 26-31 (DE-627)130403423 (DE-600)607624-5 (DE-576)015907090 0932-3414 nnns volume:51 year:2013 number:1 day:01 month:05 pages:26-31 https://doi.org/10.3139/113.110282 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_24 GBV_ILN_30 GBV_ILN_70 GBV_ILN_267 GBV_ILN_2234 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4307 GBV_ILN_4317 GBV_ILN_4323 35.00 VZ AR 51 2013 1 01 05 26-31 |
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synthesis and surface active properties of dimeric gemini sulfonate surfactants |
| title_auth |
Synthesis and Surface Active Properties of Dimeric Gemini Sulfonate Surfactants |
| abstract |
Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. © 2014, Carl Hanser Publisher, Munich |
| abstractGer |
Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. © 2014, Carl Hanser Publisher, Munich |
| abstract_unstemmed |
Abstract Dimeric Gemini sulfonate surfactants 1,2-di-(2-oxoypropyl sulfonate-3-alkylether- propoxy) ethane were prepared by the reaction of ethylene glycol diglycidyl ether with long-chain alcohols, followed by sulfonation with 1,3-propane sultone. Ethylene glycol ether was synthesized by the reaction of epichlorohydrin with ethylene glycol. The chemical structures of the prepared compounds were confirmed by FTIR, 1H NMR and elementary analysis. With the increasing length of the carbon chain, the values of their CMC initially decreased. The longer alkyl chain is, the higher melting point is. The Krafft point of Gemini sulfonate surfactants was below 0°C and they had good water solubility. These compounds were superior in surface active properties to general sulfonate surfactants SDS. The efficiency of adsorption at the water/air interface ($ pC_{20} $) of these surfactants was very high. Their foaming properties and wetting ability toward a felt chip, and lime-soap dispersing ability were investigated. © 2014, Carl Hanser Publisher, Munich |
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Synthesis and Surface Active Properties of Dimeric Gemini Sulfonate Surfactants |
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https://doi.org/10.3139/113.110282 |
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