Importance of heat transfer phenomena during DSC polymer solidification
Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a gener...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Lamberti, Gaetano [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2004 |
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| Schlagwörter: |
Differential Scanning Calorimetry |
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| Anmerkung: |
© Springer-Verlag 2004 |
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| Übergeordnetes Werk: |
Enthalten in: Heat and mass transfer - Berlin : Springer, 1968, 41(2004), 1 vom: 15. Apr., Seite 23-31 |
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| Übergeordnetes Werk: |
volume:41 ; year:2004 ; number:1 ; day:15 ; month:04 ; pages:23-31 |
| Links: |
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| DOI / URN: |
10.1007/s00231-004-0509-5 |
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| 520 | |a Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a generalized code was adopted, which was proposed in a previous communication, together with its preliminary validation [2]. Solidification runs were simulated both under isothermal conditions and under slow cooling rates, comparable to the ones attainable in standard differential scanning calorimetry (DSC). The output DSC signals were simulated, and it is shown that traditional analysis, usually performed on these signals in the frame of crystallization kinetics studies, can give correct results for isothermal tests, but can give suggestions consistently far from real material behaviour during cooling ramps. | ||
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10.1007/s00231-004-0509-5 doi (DE-627)SPR002617013 (SPR)s00231-004-0509-5-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Importance of heat transfer phenomena during DSC polymer solidification 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2004 Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a generalized code was adopted, which was proposed in a previous communication, together with its preliminary validation [2]. Solidification runs were simulated both under isothermal conditions and under slow cooling rates, comparable to the ones attainable in standard differential scanning calorimetry (DSC). The output DSC signals were simulated, and it is shown that traditional analysis, usually performed on these signals in the frame of crystallization kinetics studies, can give correct results for isothermal tests, but can give suggestions consistently far from real material behaviour during cooling ramps. Differential Scanning Calorimetry (dpeaa)DE-He213 Differential Scanning Calorimetry Analysis (dpeaa)DE-He213 Slab Surface (dpeaa)DE-He213 Heat Transfer Phenomenon (dpeaa)DE-He213 Constant Cool Rate (dpeaa)DE-He213 Enthalten in Heat and mass transfer Berlin : Springer, 1968 41(2004), 1 vom: 15. Apr., Seite 23-31 (DE-627)27012635X (DE-600)1476367-9 1432-1181 nnns volume:41 year:2004 number:1 day:15 month:04 pages:23-31 https://dx.doi.org/10.1007/s00231-004-0509-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 41 2004 1 15 04 23-31 |
| spelling |
10.1007/s00231-004-0509-5 doi (DE-627)SPR002617013 (SPR)s00231-004-0509-5-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Importance of heat transfer phenomena during DSC polymer solidification 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2004 Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a generalized code was adopted, which was proposed in a previous communication, together with its preliminary validation [2]. Solidification runs were simulated both under isothermal conditions and under slow cooling rates, comparable to the ones attainable in standard differential scanning calorimetry (DSC). The output DSC signals were simulated, and it is shown that traditional analysis, usually performed on these signals in the frame of crystallization kinetics studies, can give correct results for isothermal tests, but can give suggestions consistently far from real material behaviour during cooling ramps. Differential Scanning Calorimetry (dpeaa)DE-He213 Differential Scanning Calorimetry Analysis (dpeaa)DE-He213 Slab Surface (dpeaa)DE-He213 Heat Transfer Phenomenon (dpeaa)DE-He213 Constant Cool Rate (dpeaa)DE-He213 Enthalten in Heat and mass transfer Berlin : Springer, 1968 41(2004), 1 vom: 15. Apr., Seite 23-31 (DE-627)27012635X (DE-600)1476367-9 1432-1181 nnns volume:41 year:2004 number:1 day:15 month:04 pages:23-31 https://dx.doi.org/10.1007/s00231-004-0509-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 41 2004 1 15 04 23-31 |
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10.1007/s00231-004-0509-5 doi (DE-627)SPR002617013 (SPR)s00231-004-0509-5-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Importance of heat transfer phenomena during DSC polymer solidification 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2004 Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a generalized code was adopted, which was proposed in a previous communication, together with its preliminary validation [2]. Solidification runs were simulated both under isothermal conditions and under slow cooling rates, comparable to the ones attainable in standard differential scanning calorimetry (DSC). The output DSC signals were simulated, and it is shown that traditional analysis, usually performed on these signals in the frame of crystallization kinetics studies, can give correct results for isothermal tests, but can give suggestions consistently far from real material behaviour during cooling ramps. Differential Scanning Calorimetry (dpeaa)DE-He213 Differential Scanning Calorimetry Analysis (dpeaa)DE-He213 Slab Surface (dpeaa)DE-He213 Heat Transfer Phenomenon (dpeaa)DE-He213 Constant Cool Rate (dpeaa)DE-He213 Enthalten in Heat and mass transfer Berlin : Springer, 1968 41(2004), 1 vom: 15. Apr., Seite 23-31 (DE-627)27012635X (DE-600)1476367-9 1432-1181 nnns volume:41 year:2004 number:1 day:15 month:04 pages:23-31 https://dx.doi.org/10.1007/s00231-004-0509-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 41 2004 1 15 04 23-31 |
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10.1007/s00231-004-0509-5 doi (DE-627)SPR002617013 (SPR)s00231-004-0509-5-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Importance of heat transfer phenomena during DSC polymer solidification 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2004 Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a generalized code was adopted, which was proposed in a previous communication, together with its preliminary validation [2]. Solidification runs were simulated both under isothermal conditions and under slow cooling rates, comparable to the ones attainable in standard differential scanning calorimetry (DSC). The output DSC signals were simulated, and it is shown that traditional analysis, usually performed on these signals in the frame of crystallization kinetics studies, can give correct results for isothermal tests, but can give suggestions consistently far from real material behaviour during cooling ramps. Differential Scanning Calorimetry (dpeaa)DE-He213 Differential Scanning Calorimetry Analysis (dpeaa)DE-He213 Slab Surface (dpeaa)DE-He213 Heat Transfer Phenomenon (dpeaa)DE-He213 Constant Cool Rate (dpeaa)DE-He213 Enthalten in Heat and mass transfer Berlin : Springer, 1968 41(2004), 1 vom: 15. Apr., Seite 23-31 (DE-627)27012635X (DE-600)1476367-9 1432-1181 nnns volume:41 year:2004 number:1 day:15 month:04 pages:23-31 https://dx.doi.org/10.1007/s00231-004-0509-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 41 2004 1 15 04 23-31 |
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Enthalten in Heat and mass transfer 41(2004), 1 vom: 15. Apr., Seite 23-31 volume:41 year:2004 number:1 day:15 month:04 pages:23-31 |
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Enthalten in Heat and mass transfer 41(2004), 1 vom: 15. Apr., Seite 23-31 volume:41 year:2004 number:1 day:15 month:04 pages:23-31 |
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Lamberti, Gaetano |
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Lamberti, Gaetano misc Differential Scanning Calorimetry misc Differential Scanning Calorimetry Analysis misc Slab Surface misc Heat Transfer Phenomenon misc Constant Cool Rate Importance of heat transfer phenomena during DSC polymer solidification |
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Importance of heat transfer phenomena during DSC polymer solidification Differential Scanning Calorimetry (dpeaa)DE-He213 Differential Scanning Calorimetry Analysis (dpeaa)DE-He213 Slab Surface (dpeaa)DE-He213 Heat Transfer Phenomenon (dpeaa)DE-He213 Constant Cool Rate (dpeaa)DE-He213 |
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Importance of heat transfer phenomena during DSC polymer solidification |
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importance of heat transfer phenomena during dsc polymer solidification |
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Importance of heat transfer phenomena during DSC polymer solidification |
| abstract |
Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a generalized code was adopted, which was proposed in a previous communication, together with its preliminary validation [2]. Solidification runs were simulated both under isothermal conditions and under slow cooling rates, comparable to the ones attainable in standard differential scanning calorimetry (DSC). The output DSC signals were simulated, and it is shown that traditional analysis, usually performed on these signals in the frame of crystallization kinetics studies, can give correct results for isothermal tests, but can give suggestions consistently far from real material behaviour during cooling ramps. © Springer-Verlag 2004 |
| abstractGer |
Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a generalized code was adopted, which was proposed in a previous communication, together with its preliminary validation [2]. Solidification runs were simulated both under isothermal conditions and under slow cooling rates, comparable to the ones attainable in standard differential scanning calorimetry (DSC). The output DSC signals were simulated, and it is shown that traditional analysis, usually performed on these signals in the frame of crystallization kinetics studies, can give correct results for isothermal tests, but can give suggestions consistently far from real material behaviour during cooling ramps. © Springer-Verlag 2004 |
| abstract_unstemmed |
Abstract In this work, solidification of semi-infinite polymer slabs was modelled accounting for heat transfer and phase change. Transient one-dimensional energy balance was numerically solved, coupled with a suitable crystallization kinetic model, coming from literature [1]. To this purpose a generalized code was adopted, which was proposed in a previous communication, together with its preliminary validation [2]. Solidification runs were simulated both under isothermal conditions and under slow cooling rates, comparable to the ones attainable in standard differential scanning calorimetry (DSC). The output DSC signals were simulated, and it is shown that traditional analysis, usually performed on these signals in the frame of crystallization kinetics studies, can give correct results for isothermal tests, but can give suggestions consistently far from real material behaviour during cooling ramps. © Springer-Verlag 2004 |
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Importance of heat transfer phenomena during DSC polymer solidification |
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https://dx.doi.org/10.1007/s00231-004-0509-5 |
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