Some issues on polymer crystallization kinetics studied by DSC non isothermal tests

Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the ex...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Lamberti, Gaetano [verfasserIn] Naddeo, Carlo

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2006

Schlagwörter:	Polymer Heat Transfer Crystallization Cool Rate Calorimeter

Anmerkung:	© Springer-Verlag 2006

Übergeordnetes Werk:	Enthalten in: Polymer bulletin - Berlin : Springer, 1978, 56(2006), 6 vom: 02. Feb., Seite 591-598
Übergeordnetes Werk:	volume:56 ; year:2006 ; number:6 ; day:02 ; month:02 ; pages:591-598

Links:	Volltext

DOI / URN:	10.1007/s00289-006-0518-2

Katalog-ID:	SPR003737667

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912			\|a GBV_ILN_74
912			\|a GBV_ILN_90
912			\|a GBV_ILN_95
912			\|a GBV_ILN_100
912			\|a GBV_ILN_101
912			\|a GBV_ILN_105
912			\|a GBV_ILN_110
912			\|a GBV_ILN_120
912			\|a GBV_ILN_138
912			\|a GBV_ILN_150
912			\|a GBV_ILN_151
912			\|a GBV_ILN_152
912			\|a GBV_ILN_161
912			\|a GBV_ILN_170
912			\|a GBV_ILN_171
912			\|a GBV_ILN_187
912			\|a GBV_ILN_213
912			\|a GBV_ILN_224
912			\|a GBV_ILN_230
912			\|a GBV_ILN_250
912			\|a GBV_ILN_267
912			\|a GBV_ILN_281
912			\|a GBV_ILN_285
912			\|a GBV_ILN_293
912			\|a GBV_ILN_370
912			\|a GBV_ILN_602
912			\|a GBV_ILN_636
912			\|a GBV_ILN_702
912			\|a GBV_ILN_2001
912			\|a GBV_ILN_2003
912			\|a GBV_ILN_2004
912			\|a GBV_ILN_2005
912			\|a GBV_ILN_2006
912			\|a GBV_ILN_2007
912			\|a GBV_ILN_2009
912			\|a GBV_ILN_2010
912			\|a GBV_ILN_2011
912			\|a GBV_ILN_2014
912			\|a GBV_ILN_2015
912			\|a GBV_ILN_2020
912			\|a GBV_ILN_2021
912			\|a GBV_ILN_2025
912			\|a GBV_ILN_2026
912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2031
912			\|a GBV_ILN_2034
912			\|a GBV_ILN_2037
912			\|a GBV_ILN_2038
912			\|a GBV_ILN_2039
912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2050
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2057
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
912			\|a GBV_ILN_2064
912			\|a GBV_ILN_2065
912			\|a GBV_ILN_2068
912			\|a GBV_ILN_2070
912			\|a GBV_ILN_2086
912			\|a GBV_ILN_2088
912			\|a GBV_ILN_2093
912			\|a GBV_ILN_2106
912			\|a GBV_ILN_2107
912			\|a GBV_ILN_2108
912			\|a GBV_ILN_2110
912			\|a GBV_ILN_2111
912			\|a GBV_ILN_2112
912			\|a GBV_ILN_2113
912			\|a GBV_ILN_2116
912			\|a GBV_ILN_2118
912			\|a GBV_ILN_2119
912			\|a GBV_ILN_2122
912			\|a GBV_ILN_2129
912			\|a GBV_ILN_2143
912			\|a GBV_ILN_2144
912			\|a GBV_ILN_2147
912			\|a GBV_ILN_2148
912			\|a GBV_ILN_2152
912			\|a GBV_ILN_2153
912			\|a GBV_ILN_2188
912			\|a GBV_ILN_2190
912			\|a GBV_ILN_2232
912			\|a GBV_ILN_2336
912			\|a GBV_ILN_2411
912			\|a GBV_ILN_2446
912			\|a GBV_ILN_2470
912			\|a GBV_ILN_2472
912			\|a GBV_ILN_2507
912			\|a GBV_ILN_2522
912			\|a GBV_ILN_2548
912			\|a GBV_ILN_4012
912			\|a GBV_ILN_4035
912			\|a GBV_ILN_4037
912			\|a GBV_ILN_4046
912			\|a GBV_ILN_4112
912			\|a GBV_ILN_4125
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912			\|a GBV_ILN_4333
912			\|a GBV_ILN_4334
912			\|a GBV_ILN_4335
912			\|a GBV_ILN_4336
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publishDate	2006
allfields	10.1007/s00289-006-0518-2 doi (DE-627)SPR003737667 (SPR)s00289-006-0518-2-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer (dpeaa)DE-He213 Heat Transfer (dpeaa)DE-He213 Crystallization (dpeaa)DE-He213 Cool Rate (dpeaa)DE-He213 Calorimeter (dpeaa)DE-He213 Naddeo, Carlo aut Enthalten in Polymer bulletin Berlin : Springer, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://dx.doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2006 6 02 02 591-598
spelling	10.1007/s00289-006-0518-2 doi (DE-627)SPR003737667 (SPR)s00289-006-0518-2-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer (dpeaa)DE-He213 Heat Transfer (dpeaa)DE-He213 Crystallization (dpeaa)DE-He213 Cool Rate (dpeaa)DE-He213 Calorimeter (dpeaa)DE-He213 Naddeo, Carlo aut Enthalten in Polymer bulletin Berlin : Springer, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://dx.doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2006 6 02 02 591-598
allfields_unstemmed	10.1007/s00289-006-0518-2 doi (DE-627)SPR003737667 (SPR)s00289-006-0518-2-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer (dpeaa)DE-He213 Heat Transfer (dpeaa)DE-He213 Crystallization (dpeaa)DE-He213 Cool Rate (dpeaa)DE-He213 Calorimeter (dpeaa)DE-He213 Naddeo, Carlo aut Enthalten in Polymer bulletin Berlin : Springer, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://dx.doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2006 6 02 02 591-598
allfieldsGer	10.1007/s00289-006-0518-2 doi (DE-627)SPR003737667 (SPR)s00289-006-0518-2-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer (dpeaa)DE-He213 Heat Transfer (dpeaa)DE-He213 Crystallization (dpeaa)DE-He213 Cool Rate (dpeaa)DE-He213 Calorimeter (dpeaa)DE-He213 Naddeo, Carlo aut Enthalten in Polymer bulletin Berlin : Springer, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://dx.doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2006 6 02 02 591-598
allfieldsSound	10.1007/s00289-006-0518-2 doi (DE-627)SPR003737667 (SPR)s00289-006-0518-2-e DE-627 ger DE-627 rakwb eng Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer (dpeaa)DE-He213 Heat Transfer (dpeaa)DE-He213 Crystallization (dpeaa)DE-He213 Cool Rate (dpeaa)DE-He213 Calorimeter (dpeaa)DE-He213 Naddeo, Carlo aut Enthalten in Polymer bulletin Berlin : Springer, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://dx.doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2006 6 02 02 591-598
language	English
source	Enthalten in Polymer bulletin 56(2006), 6 vom: 02. Feb., Seite 591-598 volume:56 year:2006 number:6 day:02 month:02 pages:591-598
sourceStr	Enthalten in Polymer bulletin 56(2006), 6 vom: 02. Feb., Seite 591-598 volume:56 year:2006 number:6 day:02 month:02 pages:591-598
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Polymer Heat Transfer Crystallization Cool Rate Calorimeter
isfreeaccess_bool	false
container_title	Polymer bulletin
authorswithroles_txt_mv	Lamberti, Gaetano @@aut@@ Naddeo, Carlo @@aut@@
publishDateDaySort_date	2006-02-02T00:00:00Z
hierarchy_top_id	268761833
id	SPR003737667
language_de	englisch
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author	Lamberti, Gaetano
spellingShingle	Lamberti, Gaetano misc Polymer misc Heat Transfer misc Crystallization misc Cool Rate misc Calorimeter Some issues on polymer crystallization kinetics studied by DSC non isothermal tests
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topic_title	Some issues on polymer crystallization kinetics studied by DSC non isothermal tests Polymer (dpeaa)DE-He213 Heat Transfer (dpeaa)DE-He213 Crystallization (dpeaa)DE-He213 Cool Rate (dpeaa)DE-He213 Calorimeter (dpeaa)DE-He213
topic	misc Polymer misc Heat Transfer misc Crystallization misc Cool Rate misc Calorimeter
topic_unstemmed	misc Polymer misc Heat Transfer misc Crystallization misc Cool Rate misc Calorimeter
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title	Some issues on polymer crystallization kinetics studied by DSC non isothermal tests
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title_full	Some issues on polymer crystallization kinetics studied by DSC non isothermal tests
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author_browse	Lamberti, Gaetano Naddeo, Carlo
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title_sort	some issues on polymer crystallization kinetics studied by dsc non isothermal tests
title_auth	Some issues on polymer crystallization kinetics studied by DSC non isothermal tests
abstract	Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. © Springer-Verlag 2006
abstractGer	Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. © Springer-Verlag 2006
abstract_unstemmed	Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. © Springer-Verlag 2006
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title_short	Some issues on polymer crystallization kinetics studied by DSC non isothermal tests
url	https://dx.doi.org/10.1007/s00289-006-0518-2
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Some issues on polymer crystallization kinetics studied by DSC non isothermal tests

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