Novel triazole-based aluminum complex for ring-opening polymerization of lactones
Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system pro...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Hermanová, Soňa [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2011 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer-Verlag 2011 |
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| Übergeordnetes Werk: |
Enthalten in: Polymer bulletin - Berlin : Springer, 1978, 67(2011), 9 vom: 23. Juni, Seite 1751-1760 |
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| Übergeordnetes Werk: |
volume:67 ; year:2011 ; number:9 ; day:23 ; month:06 ; pages:1751-1760 |
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| DOI / URN: |
10.1007/s00289-011-0486-z |
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| Katalog-ID: |
SPR003748812 |
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| 100 | 1 | |a Hermanová, Soňa |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Novel triazole-based aluminum complex for ring-opening polymerization of lactones |
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| 520 | |a Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system produced polymers with high conversion (81–85 %) but broader distribution (Mw/Mn = 1.5–1.8). The system of catalyst and benzyl alcohol produced relative monodisperse PCLs (Mw/Mn ~ 1.2) with defined molecular weight at 1/1ratio, 60 °C and an initial concentration of ε-CL equal to 0.5 mol/L. | ||
| 650 | 4 | |a Aluminum |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Polycaprolactone |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Ring-opening polymerization |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Moya Cabrera, Monica M. |4 aut | |
| 700 | 1 | |a Vyroubalová, Zdeňka |4 aut | |
| 700 | 1 | |a Vojtová, Lucy |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Polymer bulletin |d Berlin : Springer, 1978 |g 67(2011), 9 vom: 23. Juni, Seite 1751-1760 |w (DE-627)268761833 |w (DE-600)1473175-7 |x 1436-2449 |7 nnns |
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10.1007/s00289-011-0486-z doi (DE-627)SPR003748812 (SPR)s00289-011-0486-z-e DE-627 ger DE-627 rakwb eng Hermanová, Soňa verfasserin aut Novel triazole-based aluminum complex for ring-opening polymerization of lactones 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2011 Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system produced polymers with high conversion (81–85 %) but broader distribution (Mw/Mn = 1.5–1.8). The system of catalyst and benzyl alcohol produced relative monodisperse PCLs (Mw/Mn ~ 1.2) with defined molecular weight at 1/1ratio, 60 °C and an initial concentration of ε-CL equal to 0.5 mol/L. Aluminum (dpeaa)DE-He213 Polycaprolactone (dpeaa)DE-He213 Ring-opening polymerization (dpeaa)DE-He213 Moya Cabrera, Monica M. aut Vyroubalová, Zdeňka aut Vojtová, Lucy aut Enthalten in Polymer bulletin Berlin : Springer, 1978 67(2011), 9 vom: 23. Juni, Seite 1751-1760 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:67 year:2011 number:9 day:23 month:06 pages:1751-1760 https://dx.doi.org/10.1007/s00289-011-0486-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 67 2011 9 23 06 1751-1760 |
| spelling |
10.1007/s00289-011-0486-z doi (DE-627)SPR003748812 (SPR)s00289-011-0486-z-e DE-627 ger DE-627 rakwb eng Hermanová, Soňa verfasserin aut Novel triazole-based aluminum complex for ring-opening polymerization of lactones 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2011 Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system produced polymers with high conversion (81–85 %) but broader distribution (Mw/Mn = 1.5–1.8). The system of catalyst and benzyl alcohol produced relative monodisperse PCLs (Mw/Mn ~ 1.2) with defined molecular weight at 1/1ratio, 60 °C and an initial concentration of ε-CL equal to 0.5 mol/L. Aluminum (dpeaa)DE-He213 Polycaprolactone (dpeaa)DE-He213 Ring-opening polymerization (dpeaa)DE-He213 Moya Cabrera, Monica M. aut Vyroubalová, Zdeňka aut Vojtová, Lucy aut Enthalten in Polymer bulletin Berlin : Springer, 1978 67(2011), 9 vom: 23. Juni, Seite 1751-1760 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:67 year:2011 number:9 day:23 month:06 pages:1751-1760 https://dx.doi.org/10.1007/s00289-011-0486-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 67 2011 9 23 06 1751-1760 |
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10.1007/s00289-011-0486-z doi (DE-627)SPR003748812 (SPR)s00289-011-0486-z-e DE-627 ger DE-627 rakwb eng Hermanová, Soňa verfasserin aut Novel triazole-based aluminum complex for ring-opening polymerization of lactones 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2011 Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system produced polymers with high conversion (81–85 %) but broader distribution (Mw/Mn = 1.5–1.8). The system of catalyst and benzyl alcohol produced relative monodisperse PCLs (Mw/Mn ~ 1.2) with defined molecular weight at 1/1ratio, 60 °C and an initial concentration of ε-CL equal to 0.5 mol/L. Aluminum (dpeaa)DE-He213 Polycaprolactone (dpeaa)DE-He213 Ring-opening polymerization (dpeaa)DE-He213 Moya Cabrera, Monica M. aut Vyroubalová, Zdeňka aut Vojtová, Lucy aut Enthalten in Polymer bulletin Berlin : Springer, 1978 67(2011), 9 vom: 23. Juni, Seite 1751-1760 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:67 year:2011 number:9 day:23 month:06 pages:1751-1760 https://dx.doi.org/10.1007/s00289-011-0486-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 67 2011 9 23 06 1751-1760 |
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10.1007/s00289-011-0486-z doi (DE-627)SPR003748812 (SPR)s00289-011-0486-z-e DE-627 ger DE-627 rakwb eng Hermanová, Soňa verfasserin aut Novel triazole-based aluminum complex for ring-opening polymerization of lactones 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2011 Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system produced polymers with high conversion (81–85 %) but broader distribution (Mw/Mn = 1.5–1.8). The system of catalyst and benzyl alcohol produced relative monodisperse PCLs (Mw/Mn ~ 1.2) with defined molecular weight at 1/1ratio, 60 °C and an initial concentration of ε-CL equal to 0.5 mol/L. Aluminum (dpeaa)DE-He213 Polycaprolactone (dpeaa)DE-He213 Ring-opening polymerization (dpeaa)DE-He213 Moya Cabrera, Monica M. aut Vyroubalová, Zdeňka aut Vojtová, Lucy aut Enthalten in Polymer bulletin Berlin : Springer, 1978 67(2011), 9 vom: 23. Juni, Seite 1751-1760 (DE-627)268761833 (DE-600)1473175-7 1436-2449 nnns volume:67 year:2011 number:9 day:23 month:06 pages:1751-1760 https://dx.doi.org/10.1007/s00289-011-0486-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2411 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 67 2011 9 23 06 1751-1760 |
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Enthalten in Polymer bulletin 67(2011), 9 vom: 23. Juni, Seite 1751-1760 volume:67 year:2011 number:9 day:23 month:06 pages:1751-1760 |
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Hermanová, Soňa @@aut@@ Moya Cabrera, Monica M. @@aut@@ Vyroubalová, Zdeňka @@aut@@ Vojtová, Lucy @@aut@@ |
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Hermanová, Soňa |
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Hermanová, Soňa misc Aluminum misc Polycaprolactone misc Ring-opening polymerization Novel triazole-based aluminum complex for ring-opening polymerization of lactones |
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Novel triazole-based aluminum complex for ring-opening polymerization of lactones Aluminum (dpeaa)DE-He213 Polycaprolactone (dpeaa)DE-He213 Ring-opening polymerization (dpeaa)DE-He213 |
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misc Aluminum misc Polycaprolactone misc Ring-opening polymerization |
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novel triazole-based aluminum complex for ring-opening polymerization of lactones |
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Novel triazole-based aluminum complex for ring-opening polymerization of lactones |
| abstract |
Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system produced polymers with high conversion (81–85 %) but broader distribution (Mw/Mn = 1.5–1.8). The system of catalyst and benzyl alcohol produced relative monodisperse PCLs (Mw/Mn ~ 1.2) with defined molecular weight at 1/1ratio, 60 °C and an initial concentration of ε-CL equal to 0.5 mol/L. © Springer-Verlag 2011 |
| abstractGer |
Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system produced polymers with high conversion (81–85 %) but broader distribution (Mw/Mn = 1.5–1.8). The system of catalyst and benzyl alcohol produced relative monodisperse PCLs (Mw/Mn ~ 1.2) with defined molecular weight at 1/1ratio, 60 °C and an initial concentration of ε-CL equal to 0.5 mol/L. © Springer-Verlag 2011 |
| abstract_unstemmed |
Abstract Novel triazole-based aluminum complex {O,O′-[4,5-P(O)$ Ph_{2} $tz]-$ AlMe_{2} $ was studied as the catalyst for the ring-opening polymerization of caprolactone (ε-CL) in chlorobenzene. In the presence of methanol, isopropanol, and bifunctional poly(ethylene glycol), the catalytic system produced polymers with high conversion (81–85 %) but broader distribution (Mw/Mn = 1.5–1.8). The system of catalyst and benzyl alcohol produced relative monodisperse PCLs (Mw/Mn ~ 1.2) with defined molecular weight at 1/1ratio, 60 °C and an initial concentration of ε-CL equal to 0.5 mol/L. © Springer-Verlag 2011 |
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Novel triazole-based aluminum complex for ring-opening polymerization of lactones |
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https://dx.doi.org/10.1007/s00289-011-0486-z |
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Moya Cabrera, Monica M. Vyroubalová, Zdeňka Vojtová, Lucy |
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Moya Cabrera, Monica M. Vyroubalová, Zdeňka Vojtová, Lucy |
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10.1007/s00289-011-0486-z |
| up_date |
2024-07-03T21:25:16.888Z |
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