Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles

Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all th...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Mandal, Debabrata [verfasserIn] Sharma, Lalit Kumar Mukherjee, Samrat

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2016

Schlagwörter:	Excitonic Emission Ionize Oxygen Vacancy Longitudinal Optical Transverse Optical Trap Exciton

Anmerkung:	© Springer-Verlag Berlin Heidelberg 2016

Übergeordnetes Werk:	Enthalten in: Applied physics - Berlin : Springer, 1973, 122(2016), 12 vom: 19. Nov.
Übergeordnetes Werk:	volume:122 ; year:2016 ; number:12 ; day:19 ; month:11

Links:	Volltext

DOI / URN:	10.1007/s00339-016-0573-y

Katalog-ID:	SPR004157710

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520			\|a Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T.
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publishDate	2016
allfields	10.1007/s00339-016-0573-y doi (DE-627)SPR004157710 (SPR)s00339-016-0573-y-e DE-627 ger DE-627 rakwb eng Mandal, Debabrata verfasserin aut Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag Berlin Heidelberg 2016 Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T. Excitonic Emission (dpeaa)DE-He213 Ionize Oxygen Vacancy (dpeaa)DE-He213 Longitudinal Optical (dpeaa)DE-He213 Transverse Optical (dpeaa)DE-He213 Trap Exciton (dpeaa)DE-He213 Sharma, Lalit Kumar aut Mukherjee, Samrat aut Enthalten in Applied physics Berlin : Springer, 1973 122(2016), 12 vom: 19. Nov. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:122 year:2016 number:12 day:19 month:11 https://dx.doi.org/10.1007/s00339-016-0573-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 122 2016 12 19 11
spelling	10.1007/s00339-016-0573-y doi (DE-627)SPR004157710 (SPR)s00339-016-0573-y-e DE-627 ger DE-627 rakwb eng Mandal, Debabrata verfasserin aut Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag Berlin Heidelberg 2016 Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T. Excitonic Emission (dpeaa)DE-He213 Ionize Oxygen Vacancy (dpeaa)DE-He213 Longitudinal Optical (dpeaa)DE-He213 Transverse Optical (dpeaa)DE-He213 Trap Exciton (dpeaa)DE-He213 Sharma, Lalit Kumar aut Mukherjee, Samrat aut Enthalten in Applied physics Berlin : Springer, 1973 122(2016), 12 vom: 19. Nov. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:122 year:2016 number:12 day:19 month:11 https://dx.doi.org/10.1007/s00339-016-0573-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 122 2016 12 19 11
allfields_unstemmed	10.1007/s00339-016-0573-y doi (DE-627)SPR004157710 (SPR)s00339-016-0573-y-e DE-627 ger DE-627 rakwb eng Mandal, Debabrata verfasserin aut Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag Berlin Heidelberg 2016 Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T. Excitonic Emission (dpeaa)DE-He213 Ionize Oxygen Vacancy (dpeaa)DE-He213 Longitudinal Optical (dpeaa)DE-He213 Transverse Optical (dpeaa)DE-He213 Trap Exciton (dpeaa)DE-He213 Sharma, Lalit Kumar aut Mukherjee, Samrat aut Enthalten in Applied physics Berlin : Springer, 1973 122(2016), 12 vom: 19. Nov. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:122 year:2016 number:12 day:19 month:11 https://dx.doi.org/10.1007/s00339-016-0573-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 122 2016 12 19 11
allfieldsGer	10.1007/s00339-016-0573-y doi (DE-627)SPR004157710 (SPR)s00339-016-0573-y-e DE-627 ger DE-627 rakwb eng Mandal, Debabrata verfasserin aut Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag Berlin Heidelberg 2016 Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T. Excitonic Emission (dpeaa)DE-He213 Ionize Oxygen Vacancy (dpeaa)DE-He213 Longitudinal Optical (dpeaa)DE-He213 Transverse Optical (dpeaa)DE-He213 Trap Exciton (dpeaa)DE-He213 Sharma, Lalit Kumar aut Mukherjee, Samrat aut Enthalten in Applied physics Berlin : Springer, 1973 122(2016), 12 vom: 19. Nov. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:122 year:2016 number:12 day:19 month:11 https://dx.doi.org/10.1007/s00339-016-0573-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 122 2016 12 19 11
allfieldsSound	10.1007/s00339-016-0573-y doi (DE-627)SPR004157710 (SPR)s00339-016-0573-y-e DE-627 ger DE-627 rakwb eng Mandal, Debabrata verfasserin aut Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag Berlin Heidelberg 2016 Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T. Excitonic Emission (dpeaa)DE-He213 Ionize Oxygen Vacancy (dpeaa)DE-He213 Longitudinal Optical (dpeaa)DE-He213 Transverse Optical (dpeaa)DE-He213 Trap Exciton (dpeaa)DE-He213 Sharma, Lalit Kumar aut Mukherjee, Samrat aut Enthalten in Applied physics Berlin : Springer, 1973 122(2016), 12 vom: 19. Nov. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:122 year:2016 number:12 day:19 month:11 https://dx.doi.org/10.1007/s00339-016-0573-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 122 2016 12 19 11
language	English
source	Enthalten in Applied physics 122(2016), 12 vom: 19. Nov. volume:122 year:2016 number:12 day:19 month:11
sourceStr	Enthalten in Applied physics 122(2016), 12 vom: 19. Nov. volume:122 year:2016 number:12 day:19 month:11
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Excitonic Emission Ionize Oxygen Vacancy Longitudinal Optical Transverse Optical Trap Exciton
isfreeaccess_bool	false
container_title	Applied physics
authorswithroles_txt_mv	Mandal, Debabrata @@aut@@ Sharma, Lalit Kumar @@aut@@ Mukherjee, Samrat @@aut@@
publishDateDaySort_date	2016-11-19T00:00:00Z
hierarchy_top_id	235503231
id	SPR004157710
language_de	englisch
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author	Mandal, Debabrata
spellingShingle	Mandal, Debabrata misc Excitonic Emission misc Ionize Oxygen Vacancy misc Longitudinal Optical misc Transverse Optical misc Trap Exciton Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles
authorStr	Mandal, Debabrata
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topic_title	Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles Excitonic Emission (dpeaa)DE-He213 Ionize Oxygen Vacancy (dpeaa)DE-He213 Longitudinal Optical (dpeaa)DE-He213 Transverse Optical (dpeaa)DE-He213 Trap Exciton (dpeaa)DE-He213
topic	misc Excitonic Emission misc Ionize Oxygen Vacancy misc Longitudinal Optical misc Transverse Optical misc Trap Exciton
topic_unstemmed	misc Excitonic Emission misc Ionize Oxygen Vacancy misc Longitudinal Optical misc Transverse Optical misc Trap Exciton
topic_browse	misc Excitonic Emission misc Ionize Oxygen Vacancy misc Longitudinal Optical misc Transverse Optical misc Trap Exciton
format_facet	Elektronische Aufsätze Aufsätze Elektronische Ressource
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title	Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles
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title_full	Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles
author_sort	Mandal, Debabrata
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author_browse	Mandal, Debabrata Sharma, Lalit Kumar Mukherjee, Samrat
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author-letter	Mandal, Debabrata
doi_str_mv	10.1007/s00339-016-0573-y
title_sort	defect-induced weak ferromagnetism in transition metal-doped zno nanoparticles
title_auth	Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles
abstract	Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T. © Springer-Verlag Berlin Heidelberg 2016
abstractGer	Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T. © Springer-Verlag Berlin Heidelberg 2016
abstract_unstemmed	Abstract In this work, citric acid-capped and ethylene glycol-stabilized pristine and transition metal (TM=Co, Fe, Mn and Ni)-doped ZnO nanoparticles with the generic formula $ Zn_{1−x} %$ TM_{x} $O, x = 0.01 and 0.02, have been synthesized by sol–gel method. XRD confirmed the phase purity of all the samples. Average crystallite size calculated from Scherrer formula was within the range of 43 ± 25 nm for different doped samples. The Raman spectra of (Co, Mn and Ni)-doped ZnO show strong E2 (high) and E1 (LO) modes. The synthesized samples also show strong luminescent emission from inherent Zn and O point defects (interstitial and vacancies) along with a sharp excitonic peak centred at 362 nm. Magnetic studies at 300 K reveal that all samples show weak room-temperature ferromagnetism at low magnetic fields with unsaturated M–H plot up to a measuring field of 5 T. © Springer-Verlag Berlin Heidelberg 2016
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container_issue	12
title_short	Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles
url	https://dx.doi.org/10.1007/s00339-016-0573-y
remote_bool	true
author2	Sharma, Lalit Kumar Mukherjee, Samrat
author2Str	Sharma, Lalit Kumar Mukherjee, Samrat
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doi_str	10.1007/s00339-016-0573-y
up_date	2024-07-03T23:53:52.027Z
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Defect-induced weak ferromagnetism in transition metal-doped ZnO nanoparticles

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