In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile)
Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most r...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Pitna Laskova, Barbora [verfasserIn] Kavan, Ladislav [verfasserIn] Zukalova, Marketa [verfasserIn] Mocek, Karel [verfasserIn] Frank, Otakar [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2016 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Monatshefte für Chemie - Wien [u.a.] : Springer, 1880, 147(2016), 5 vom: 09. März, Seite 951-959 |
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| Übergeordnetes Werk: |
volume:147 ; year:2016 ; number:5 ; day:09 ; month:03 ; pages:951-959 |
| Links: |
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| DOI / URN: |
10.1007/s00706-016-1678-x |
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| Katalog-ID: |
SPR007474946 |
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| 520 | |a Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract | ||
| 650 | 4 | |a Raman spectroscopy |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Electrochemistry |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Nanochemistry |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Phase transition |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Kavan, Ladislav |e verfasserin |4 aut | |
| 700 | 1 | |a Zukalova, Marketa |e verfasserin |4 aut | |
| 700 | 1 | |a Mocek, Karel |e verfasserin |4 aut | |
| 700 | 1 | |a Frank, Otakar |e verfasserin |4 aut | |
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10.1007/s00706-016-1678-x doi (DE-627)SPR007474946 (SPR)s00706-016-1678-x-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Pitna Laskova, Barbora verfasserin aut In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract Raman spectroscopy (dpeaa)DE-He213 Electrochemistry (dpeaa)DE-He213 Nanochemistry (dpeaa)DE-He213 Phase transition (dpeaa)DE-He213 Kavan, Ladislav verfasserin aut Zukalova, Marketa verfasserin aut Mocek, Karel verfasserin aut Frank, Otakar verfasserin aut Enthalten in Monatshefte für Chemie Wien [u.a.] : Springer, 1880 147(2016), 5 vom: 09. März, Seite 951-959 (DE-627)25462992X (DE-600)1462037-6 1434-4475 nnns volume:147 year:2016 number:5 day:09 month:03 pages:951-959 https://dx.doi.org/10.1007/s00706-016-1678-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 147 2016 5 09 03 951-959 |
| spelling |
10.1007/s00706-016-1678-x doi (DE-627)SPR007474946 (SPR)s00706-016-1678-x-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Pitna Laskova, Barbora verfasserin aut In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract Raman spectroscopy (dpeaa)DE-He213 Electrochemistry (dpeaa)DE-He213 Nanochemistry (dpeaa)DE-He213 Phase transition (dpeaa)DE-He213 Kavan, Ladislav verfasserin aut Zukalova, Marketa verfasserin aut Mocek, Karel verfasserin aut Frank, Otakar verfasserin aut Enthalten in Monatshefte für Chemie Wien [u.a.] : Springer, 1880 147(2016), 5 vom: 09. März, Seite 951-959 (DE-627)25462992X (DE-600)1462037-6 1434-4475 nnns volume:147 year:2016 number:5 day:09 month:03 pages:951-959 https://dx.doi.org/10.1007/s00706-016-1678-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 147 2016 5 09 03 951-959 |
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10.1007/s00706-016-1678-x doi (DE-627)SPR007474946 (SPR)s00706-016-1678-x-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Pitna Laskova, Barbora verfasserin aut In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract Raman spectroscopy (dpeaa)DE-He213 Electrochemistry (dpeaa)DE-He213 Nanochemistry (dpeaa)DE-He213 Phase transition (dpeaa)DE-He213 Kavan, Ladislav verfasserin aut Zukalova, Marketa verfasserin aut Mocek, Karel verfasserin aut Frank, Otakar verfasserin aut Enthalten in Monatshefte für Chemie Wien [u.a.] : Springer, 1880 147(2016), 5 vom: 09. März, Seite 951-959 (DE-627)25462992X (DE-600)1462037-6 1434-4475 nnns volume:147 year:2016 number:5 day:09 month:03 pages:951-959 https://dx.doi.org/10.1007/s00706-016-1678-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 147 2016 5 09 03 951-959 |
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10.1007/s00706-016-1678-x doi (DE-627)SPR007474946 (SPR)s00706-016-1678-x-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Pitna Laskova, Barbora verfasserin aut In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract Raman spectroscopy (dpeaa)DE-He213 Electrochemistry (dpeaa)DE-He213 Nanochemistry (dpeaa)DE-He213 Phase transition (dpeaa)DE-He213 Kavan, Ladislav verfasserin aut Zukalova, Marketa verfasserin aut Mocek, Karel verfasserin aut Frank, Otakar verfasserin aut Enthalten in Monatshefte für Chemie Wien [u.a.] : Springer, 1880 147(2016), 5 vom: 09. März, Seite 951-959 (DE-627)25462992X (DE-600)1462037-6 1434-4475 nnns volume:147 year:2016 number:5 day:09 month:03 pages:951-959 https://dx.doi.org/10.1007/s00706-016-1678-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 147 2016 5 09 03 951-959 |
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10.1007/s00706-016-1678-x doi (DE-627)SPR007474946 (SPR)s00706-016-1678-x-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Pitna Laskova, Barbora verfasserin aut In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract Raman spectroscopy (dpeaa)DE-He213 Electrochemistry (dpeaa)DE-He213 Nanochemistry (dpeaa)DE-He213 Phase transition (dpeaa)DE-He213 Kavan, Ladislav verfasserin aut Zukalova, Marketa verfasserin aut Mocek, Karel verfasserin aut Frank, Otakar verfasserin aut Enthalten in Monatshefte für Chemie Wien [u.a.] : Springer, 1880 147(2016), 5 vom: 09. März, Seite 951-959 (DE-627)25462992X (DE-600)1462037-6 1434-4475 nnns volume:147 year:2016 number:5 day:09 month:03 pages:951-959 https://dx.doi.org/10.1007/s00706-016-1678-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 147 2016 5 09 03 951-959 |
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Enthalten in Monatshefte für Chemie 147(2016), 5 vom: 09. März, Seite 951-959 volume:147 year:2016 number:5 day:09 month:03 pages:951-959 |
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Raman spectroscopy Electrochemistry Nanochemistry Phase transition |
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Monatshefte für Chemie |
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Pitna Laskova, Barbora @@aut@@ Kavan, Ladislav @@aut@@ Zukalova, Marketa @@aut@@ Mocek, Karel @@aut@@ Frank, Otakar @@aut@@ |
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The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. 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Pitna Laskova, Barbora |
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540 ASE 35.00 bkl In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) Raman spectroscopy (dpeaa)DE-He213 Electrochemistry (dpeaa)DE-He213 Nanochemistry (dpeaa)DE-He213 Phase transition (dpeaa)DE-He213 |
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In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) |
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In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) |
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in situ raman spectroelectrochemistry as a useful tool for detection of $ tio_{2} $(anatase) impurities in $ tio_{2} $(b) and $ tio_{2} $(rutile) |
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In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) |
| abstract |
Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract |
| abstractGer |
Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract |
| abstract_unstemmed |
Abstract The $ TiO_{2} $(B) and $ TiO_{2} $(rutile) polymorphs are often contaminated by anatase phase residues from synthesis. The detection of anatase in $ TiO_{2} $ material can be difficult in case of small anatase impurities. In situ Raman spectroelectrochemistry is presented here as the most reliable method for unequivocal determination of anatase phase in $ TiO_{2} $ powder. Anatase detection is based on an occurrence of Raman vibrational bands of orthorhombic lithium titanate, a product of Li insertion in anatase, in Raman spectra of $ TiO_{2} $(B) and $ TiO_{2} $(rutile) materials during electrochemical $ Li^{+} $ insertion/extraction. Graphical abstract |
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5 |
| title_short |
In situ Raman spectroelectrochemistry as a useful tool for detection of $ TiO_{2} $(anatase) impurities in $ TiO_{2} $(B) and $ TiO_{2} $(rutile) |
| url |
https://dx.doi.org/10.1007/s00706-016-1678-x |
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true |
| author2 |
Kavan, Ladislav Zukalova, Marketa Mocek, Karel Frank, Otakar |
| author2Str |
Kavan, Ladislav Zukalova, Marketa Mocek, Karel Frank, Otakar |
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25462992X |
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c |
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| doi_str |
10.1007/s00706-016-1678-x |
| up_date |
2024-07-04T03:23:05.889Z |
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| score |
7.400769 |