Design and model of calibration for chemical measurements
Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process....
Ausführliche Beschreibung
Autor*in: |
Brüggemann, L. [verfasserIn] Wennrich, R. [verfasserIn] |
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Format: |
E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2008 |
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Schlagwörter: |
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Übergeordnetes Werk: |
Enthalten in: Accreditation and quality assurance - Berlin : Springer, 1996, 13(2008), 10 vom: 10. Juni, Seite 567-573 |
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Übergeordnetes Werk: |
volume:13 ; year:2008 ; number:10 ; day:10 ; month:06 ; pages:567-573 |
Links: |
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DOI / URN: |
10.1007/s00769-008-0409-3 |
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Katalog-ID: |
SPR008195447 |
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520 | |a Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany. | ||
650 | 4 | |a Linear calibration |7 (dpeaa)DE-He213 | |
650 | 4 | |a Calibration design |7 (dpeaa)DE-He213 | |
650 | 4 | |a Calibration model |7 (dpeaa)DE-He213 | |
650 | 4 | |a Calibration uncertainty |7 (dpeaa)DE-He213 | |
700 | 1 | |a Wennrich, R. |e verfasserin |4 aut | |
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10.1007/s00769-008-0409-3 doi (DE-627)SPR008195447 (SPR)s00769-008-0409-3-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.07 bkl 35.23 bkl Brüggemann, L. verfasserin aut Design and model of calibration for chemical measurements 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany. Linear calibration (dpeaa)DE-He213 Calibration design (dpeaa)DE-He213 Calibration model (dpeaa)DE-He213 Calibration uncertainty (dpeaa)DE-He213 Wennrich, R. verfasserin aut Enthalten in Accreditation and quality assurance Berlin : Springer, 1996 13(2008), 10 vom: 10. Juni, Seite 567-573 (DE-627)26813281X (DE-600)1472208-2 1432-0517 nnns volume:13 year:2008 number:10 day:10 month:06 pages:567-573 https://dx.doi.org/10.1007/s00769-008-0409-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.07 ASE 35.23 ASE AR 13 2008 10 10 06 567-573 |
spelling |
10.1007/s00769-008-0409-3 doi (DE-627)SPR008195447 (SPR)s00769-008-0409-3-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.07 bkl 35.23 bkl Brüggemann, L. verfasserin aut Design and model of calibration for chemical measurements 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany. Linear calibration (dpeaa)DE-He213 Calibration design (dpeaa)DE-He213 Calibration model (dpeaa)DE-He213 Calibration uncertainty (dpeaa)DE-He213 Wennrich, R. verfasserin aut Enthalten in Accreditation and quality assurance Berlin : Springer, 1996 13(2008), 10 vom: 10. Juni, Seite 567-573 (DE-627)26813281X (DE-600)1472208-2 1432-0517 nnns volume:13 year:2008 number:10 day:10 month:06 pages:567-573 https://dx.doi.org/10.1007/s00769-008-0409-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.07 ASE 35.23 ASE AR 13 2008 10 10 06 567-573 |
allfields_unstemmed |
10.1007/s00769-008-0409-3 doi (DE-627)SPR008195447 (SPR)s00769-008-0409-3-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.07 bkl 35.23 bkl Brüggemann, L. verfasserin aut Design and model of calibration for chemical measurements 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany. Linear calibration (dpeaa)DE-He213 Calibration design (dpeaa)DE-He213 Calibration model (dpeaa)DE-He213 Calibration uncertainty (dpeaa)DE-He213 Wennrich, R. verfasserin aut Enthalten in Accreditation and quality assurance Berlin : Springer, 1996 13(2008), 10 vom: 10. Juni, Seite 567-573 (DE-627)26813281X (DE-600)1472208-2 1432-0517 nnns volume:13 year:2008 number:10 day:10 month:06 pages:567-573 https://dx.doi.org/10.1007/s00769-008-0409-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.07 ASE 35.23 ASE AR 13 2008 10 10 06 567-573 |
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10.1007/s00769-008-0409-3 doi (DE-627)SPR008195447 (SPR)s00769-008-0409-3-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.07 bkl 35.23 bkl Brüggemann, L. verfasserin aut Design and model of calibration for chemical measurements 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany. Linear calibration (dpeaa)DE-He213 Calibration design (dpeaa)DE-He213 Calibration model (dpeaa)DE-He213 Calibration uncertainty (dpeaa)DE-He213 Wennrich, R. verfasserin aut Enthalten in Accreditation and quality assurance Berlin : Springer, 1996 13(2008), 10 vom: 10. Juni, Seite 567-573 (DE-627)26813281X (DE-600)1472208-2 1432-0517 nnns volume:13 year:2008 number:10 day:10 month:06 pages:567-573 https://dx.doi.org/10.1007/s00769-008-0409-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.07 ASE 35.23 ASE AR 13 2008 10 10 06 567-573 |
language |
English |
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Enthalten in Accreditation and quality assurance 13(2008), 10 vom: 10. Juni, Seite 567-573 volume:13 year:2008 number:10 day:10 month:06 pages:567-573 |
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Enthalten in Accreditation and quality assurance 13(2008), 10 vom: 10. Juni, Seite 567-573 volume:13 year:2008 number:10 day:10 month:06 pages:567-573 |
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topic_facet |
Linear calibration Calibration design Calibration model Calibration uncertainty |
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container_title |
Accreditation and quality assurance |
authorswithroles_txt_mv |
Brüggemann, L. @@aut@@ Wennrich, R. @@aut@@ |
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540 660 ASE 35.07 bkl 35.23 bkl Design and model of calibration for chemical measurements Linear calibration (dpeaa)DE-He213 Calibration design (dpeaa)DE-He213 Calibration model (dpeaa)DE-He213 Calibration uncertainty (dpeaa)DE-He213 |
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design and model of calibration for chemical measurements |
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Design and model of calibration for chemical measurements |
abstract |
Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany. |
abstractGer |
Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany. |
abstract_unstemmed |
Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany. |
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Design and model of calibration for chemical measurements |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR008195447</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230519215329.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">201005s2008 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s00769-008-0409-3</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR008195447</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s00769-008-0409-3-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">540</subfield><subfield code="a">660</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">35.07</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">35.23</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Brüggemann, L.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Design and model of calibration for chemical measurements</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2008</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract The international standard ISO 11843 specifies basic methods to design experiments for estimation of critical values referring to the capability of detection. The detection capability depends on the experimental design, the calibration model used, and the errors of the measurement process. This study reports how the specification of the calibration points within the calibration range can be used as a-priori information for evaluation of calibration uncertainty without any consideration of the response variables of the calibration. As result of investigation of the experimental designs, calibration points within the calibration range can be omitted without significant changes of calibration uncertainty. The approach is demonstrated at a practical example, the determination of arsenic in surface water samples taken from a river in Germany.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Linear calibration</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Calibration design</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Calibration model</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Calibration uncertainty</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wennrich, R.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Accreditation and quality assurance</subfield><subfield code="d">Berlin : Springer, 1996</subfield><subfield code="g">13(2008), 10 vom: 10. Juni, Seite 567-573</subfield><subfield code="w">(DE-627)26813281X</subfield><subfield code="w">(DE-600)1472208-2</subfield><subfield code="x">1432-0517</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:13</subfield><subfield code="g">year:2008</subfield><subfield code="g">number:10</subfield><subfield code="g">day:10</subfield><subfield code="g">month:06</subfield><subfield code="g">pages:567-573</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">https://dx.doi.org/10.1007/s00769-008-0409-3</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_SPRINGER</subfield></datafield><datafield tag="912" 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