Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection
Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column a...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
He, Mei-Lian [verfasserIn] Cheng, Xiao-Wei [verfasserIn] Chen, Jia-Kuan [verfasserIn] Zhou, Tong-Shui [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2006 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Chromatographia - Wiesbaden : Vieweg, 1968, 64(2006), 11-12 vom: 16. Nov., Seite 713-717 |
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| Übergeordnetes Werk: |
volume:64 ; year:2006 ; number:11-12 ; day:16 ; month:11 ; pages:713-717 |
| Links: |
|---|
| DOI / URN: |
10.1365/s10337-006-0099-0 |
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| Katalog-ID: |
SPR009532196 |
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| 245 | 1 | 0 | |a Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection |
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| 520 | |a Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. | ||
| 650 | 4 | |a Column liquid chromatography |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Diode-array detection |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Geniposide and geniposidic acid |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Crocin 1 and 2 |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Chlorogenic acid |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Cheng, Xiao-Wei |e verfasserin |4 aut | |
| 700 | 1 | |a Chen, Jia-Kuan |e verfasserin |4 aut | |
| 700 | 1 | |a Zhou, Tong-Shui |e verfasserin |4 aut | |
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10.1365/s10337-006-0099-0 doi (DE-627)SPR009532196 (SPR)s10337-006-0099-0-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl He, Mei-Lian verfasserin aut Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. Column liquid chromatography (dpeaa)DE-He213 Diode-array detection (dpeaa)DE-He213 Geniposide and geniposidic acid (dpeaa)DE-He213 Crocin 1 and 2 (dpeaa)DE-He213 Chlorogenic acid (dpeaa)DE-He213 Cheng, Xiao-Wei verfasserin aut Chen, Jia-Kuan verfasserin aut Zhou, Tong-Shui verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 64(2006), 11-12 vom: 16. Nov., Seite 713-717 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:64 year:2006 number:11-12 day:16 month:11 pages:713-717 https://dx.doi.org/10.1365/s10337-006-0099-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 64 2006 11-12 16 11 713-717 |
| spelling |
10.1365/s10337-006-0099-0 doi (DE-627)SPR009532196 (SPR)s10337-006-0099-0-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl He, Mei-Lian verfasserin aut Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. Column liquid chromatography (dpeaa)DE-He213 Diode-array detection (dpeaa)DE-He213 Geniposide and geniposidic acid (dpeaa)DE-He213 Crocin 1 and 2 (dpeaa)DE-He213 Chlorogenic acid (dpeaa)DE-He213 Cheng, Xiao-Wei verfasserin aut Chen, Jia-Kuan verfasserin aut Zhou, Tong-Shui verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 64(2006), 11-12 vom: 16. Nov., Seite 713-717 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:64 year:2006 number:11-12 day:16 month:11 pages:713-717 https://dx.doi.org/10.1365/s10337-006-0099-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 64 2006 11-12 16 11 713-717 |
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10.1365/s10337-006-0099-0 doi (DE-627)SPR009532196 (SPR)s10337-006-0099-0-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl He, Mei-Lian verfasserin aut Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. Column liquid chromatography (dpeaa)DE-He213 Diode-array detection (dpeaa)DE-He213 Geniposide and geniposidic acid (dpeaa)DE-He213 Crocin 1 and 2 (dpeaa)DE-He213 Chlorogenic acid (dpeaa)DE-He213 Cheng, Xiao-Wei verfasserin aut Chen, Jia-Kuan verfasserin aut Zhou, Tong-Shui verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 64(2006), 11-12 vom: 16. Nov., Seite 713-717 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:64 year:2006 number:11-12 day:16 month:11 pages:713-717 https://dx.doi.org/10.1365/s10337-006-0099-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 64 2006 11-12 16 11 713-717 |
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10.1365/s10337-006-0099-0 doi (DE-627)SPR009532196 (SPR)s10337-006-0099-0-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl He, Mei-Lian verfasserin aut Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. Column liquid chromatography (dpeaa)DE-He213 Diode-array detection (dpeaa)DE-He213 Geniposide and geniposidic acid (dpeaa)DE-He213 Crocin 1 and 2 (dpeaa)DE-He213 Chlorogenic acid (dpeaa)DE-He213 Cheng, Xiao-Wei verfasserin aut Chen, Jia-Kuan verfasserin aut Zhou, Tong-Shui verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 64(2006), 11-12 vom: 16. Nov., Seite 713-717 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:64 year:2006 number:11-12 day:16 month:11 pages:713-717 https://dx.doi.org/10.1365/s10337-006-0099-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 64 2006 11-12 16 11 713-717 |
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10.1365/s10337-006-0099-0 doi (DE-627)SPR009532196 (SPR)s10337-006-0099-0-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl He, Mei-Lian verfasserin aut Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. Column liquid chromatography (dpeaa)DE-He213 Diode-array detection (dpeaa)DE-He213 Geniposide and geniposidic acid (dpeaa)DE-He213 Crocin 1 and 2 (dpeaa)DE-He213 Chlorogenic acid (dpeaa)DE-He213 Cheng, Xiao-Wei verfasserin aut Chen, Jia-Kuan verfasserin aut Zhou, Tong-Shui verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 64(2006), 11-12 vom: 16. Nov., Seite 713-717 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:64 year:2006 number:11-12 day:16 month:11 pages:713-717 https://dx.doi.org/10.1365/s10337-006-0099-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 64 2006 11-12 16 11 713-717 |
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Enthalten in Chromatographia 64(2006), 11-12 vom: 16. Nov., Seite 713-717 volume:64 year:2006 number:11-12 day:16 month:11 pages:713-717 |
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Enthalten in Chromatographia 64(2006), 11-12 vom: 16. Nov., Seite 713-717 volume:64 year:2006 number:11-12 day:16 month:11 pages:713-717 |
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findex.gbv.de |
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Column liquid chromatography Diode-array detection Geniposide and geniposidic acid Crocin 1 and 2 Chlorogenic acid |
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He, Mei-Lian @@aut@@ Cheng, Xiao-Wei @@aut@@ Chen, Jia-Kuan @@aut@@ Zhou, Tong-Shui @@aut@@ |
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2006-11-16T00:00:00Z |
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Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Column liquid chromatography</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Diode-array detection</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Geniposide and geniposidic acid</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Crocin 1 and 2</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Chlorogenic acid</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Cheng, Xiao-Wei</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Chen, Jia-Kuan</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Zhou, Tong-Shui</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Chromatographia</subfield><subfield code="d">Wiesbaden : Vieweg, 1968</subfield><subfield code="g">64(2006), 11-12 vom: 16. 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He, Mei-Lian |
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He, Mei-Lian ddc 540 bkl 35.29 misc Column liquid chromatography misc Diode-array detection misc Geniposide and geniposidic acid misc Crocin 1 and 2 misc Chlorogenic acid Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection |
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540 ASE 35.29 bkl Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection Column liquid chromatography (dpeaa)DE-He213 Diode-array detection (dpeaa)DE-He213 Geniposide and geniposidic acid (dpeaa)DE-He213 Crocin 1 and 2 (dpeaa)DE-He213 Chlorogenic acid (dpeaa)DE-He213 |
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ddc 540 bkl 35.29 misc Column liquid chromatography misc Diode-array detection misc Geniposide and geniposidic acid misc Crocin 1 and 2 misc Chlorogenic acid |
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ddc 540 bkl 35.29 misc Column liquid chromatography misc Diode-array detection misc Geniposide and geniposidic acid misc Crocin 1 and 2 misc Chlorogenic acid |
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ddc 540 bkl 35.29 misc Column liquid chromatography misc Diode-array detection misc Geniposide and geniposidic acid misc Crocin 1 and 2 misc Chlorogenic acid |
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Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection |
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Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection |
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He, Mei-Lian |
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He, Mei-Lian Cheng, Xiao-Wei Chen, Jia-Kuan Zhou, Tong-Shui |
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simultaneous determination of five major biologically active ingredients in different parts of gardenia jasminoides fruits by hplc with diode-array detection |
| title_auth |
Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection |
| abstract |
Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. |
| abstractGer |
Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. |
| abstract_unstemmed |
Abstract A simple, sensitive and specific HPLC method for the simultaneous separation and determination of geniposide, geniposidic acid, chlorogenic acid, crocin 1 and 2 in fruits of Gardenia jasminoides Ellis was developed. Optimum chromatographic performance was obtained with a $ C_{18} $ column and acetonitrile—0.1% aqueous trifluoroacetic acid (v/v) as mobile phase. Isolated peaks were detected at 240 nm for geniposidic acid and geniposide, 330 nm for chlorogenic acid and 440 nm for crocin 1 and 2, respectively. Comparison of spectra recorded with a diode-array detector during elution of peaks enabled determination of method specificity. Quantitative determinations on different parts of gardenia fruit demonstrated that all these compounds were abundant mainly in pericarps and pulps and only iridoid glycosides were also presented in sepals and seeds of the fruits. |
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| container_issue |
11-12 |
| title_short |
Simultaneous Determination of Five Major Biologically Active Ingredients in Different Parts of Gardenia jasminoides Fruits by HPLC with Diode-Array Detection |
| url |
https://dx.doi.org/10.1365/s10337-006-0099-0 |
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| author2 |
Cheng, Xiao-Wei Chen, Jia-Kuan Zhou, Tong-Shui |
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Cheng, Xiao-Wei Chen, Jia-Kuan Zhou, Tong-Shui |
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| doi_str |
10.1365/s10337-006-0099-0 |
| up_date |
2024-07-04T02:25:20.329Z |
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| score |
7.398691 |