Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC
Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation....
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Song, Weitao [verfasserIn] Cai, Haoran [verfasserIn] Du, Liping [verfasserIn] Zhao, Qi [verfasserIn] Chen, Haiyan [verfasserIn] Li, Guijie [verfasserIn] Wang, Hui [verfasserIn] Xu, Yang [verfasserIn] Ding, Lan [verfasserIn] Ren, Nanqi [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2012 |
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| Schlagwörter: |
High performance liquid chromatography Microwave-assisted steam extraction |
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| Übergeordnetes Werk: |
Enthalten in: Chromatographia - Wiesbaden : Vieweg, 1968, 75(2012), 13-14 vom: 04. Juni, Seite 747-753 |
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| Übergeordnetes Werk: |
volume:75 ; year:2012 ; number:13-14 ; day:04 ; month:06 ; pages:747-753 |
| Links: |
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| DOI / URN: |
10.1007/s10337-012-2252-2 |
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| Katalog-ID: |
SPR009555455 |
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| 520 | |a Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. | ||
| 650 | 4 | |a High performance liquid chromatography |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Microwave-assisted steam extraction |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Dynamic microwave-assisted extraction |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Paeonol |7 (dpeaa)DE-He213 | |
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| 700 | 1 | |a Du, Liping |e verfasserin |4 aut | |
| 700 | 1 | |a Zhao, Qi |e verfasserin |4 aut | |
| 700 | 1 | |a Chen, Haiyan |e verfasserin |4 aut | |
| 700 | 1 | |a Li, Guijie |e verfasserin |4 aut | |
| 700 | 1 | |a Wang, Hui |e verfasserin |4 aut | |
| 700 | 1 | |a Xu, Yang |e verfasserin |4 aut | |
| 700 | 1 | |a Ding, Lan |e verfasserin |4 aut | |
| 700 | 1 | |a Ren, Nanqi |e verfasserin |4 aut | |
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10.1007/s10337-012-2252-2 doi (DE-627)SPR009555455 (SPR)s10337-012-2252-2-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl Song, Weitao verfasserin aut Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. High performance liquid chromatography (dpeaa)DE-He213 Microwave-assisted steam extraction (dpeaa)DE-He213 Dynamic microwave-assisted extraction (dpeaa)DE-He213 Paeonol (dpeaa)DE-He213 Cai, Haoran verfasserin aut Du, Liping verfasserin aut Zhao, Qi verfasserin aut Chen, Haiyan verfasserin aut Li, Guijie verfasserin aut Wang, Hui verfasserin aut Xu, Yang verfasserin aut Ding, Lan verfasserin aut Ren, Nanqi verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 75(2012), 13-14 vom: 04. Juni, Seite 747-753 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:75 year:2012 number:13-14 day:04 month:06 pages:747-753 https://dx.doi.org/10.1007/s10337-012-2252-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 75 2012 13-14 04 06 747-753 |
| spelling |
10.1007/s10337-012-2252-2 doi (DE-627)SPR009555455 (SPR)s10337-012-2252-2-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl Song, Weitao verfasserin aut Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. High performance liquid chromatography (dpeaa)DE-He213 Microwave-assisted steam extraction (dpeaa)DE-He213 Dynamic microwave-assisted extraction (dpeaa)DE-He213 Paeonol (dpeaa)DE-He213 Cai, Haoran verfasserin aut Du, Liping verfasserin aut Zhao, Qi verfasserin aut Chen, Haiyan verfasserin aut Li, Guijie verfasserin aut Wang, Hui verfasserin aut Xu, Yang verfasserin aut Ding, Lan verfasserin aut Ren, Nanqi verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 75(2012), 13-14 vom: 04. Juni, Seite 747-753 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:75 year:2012 number:13-14 day:04 month:06 pages:747-753 https://dx.doi.org/10.1007/s10337-012-2252-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 75 2012 13-14 04 06 747-753 |
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10.1007/s10337-012-2252-2 doi (DE-627)SPR009555455 (SPR)s10337-012-2252-2-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl Song, Weitao verfasserin aut Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. High performance liquid chromatography (dpeaa)DE-He213 Microwave-assisted steam extraction (dpeaa)DE-He213 Dynamic microwave-assisted extraction (dpeaa)DE-He213 Paeonol (dpeaa)DE-He213 Cai, Haoran verfasserin aut Du, Liping verfasserin aut Zhao, Qi verfasserin aut Chen, Haiyan verfasserin aut Li, Guijie verfasserin aut Wang, Hui verfasserin aut Xu, Yang verfasserin aut Ding, Lan verfasserin aut Ren, Nanqi verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 75(2012), 13-14 vom: 04. Juni, Seite 747-753 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:75 year:2012 number:13-14 day:04 month:06 pages:747-753 https://dx.doi.org/10.1007/s10337-012-2252-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 75 2012 13-14 04 06 747-753 |
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10.1007/s10337-012-2252-2 doi (DE-627)SPR009555455 (SPR)s10337-012-2252-2-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl Song, Weitao verfasserin aut Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. High performance liquid chromatography (dpeaa)DE-He213 Microwave-assisted steam extraction (dpeaa)DE-He213 Dynamic microwave-assisted extraction (dpeaa)DE-He213 Paeonol (dpeaa)DE-He213 Cai, Haoran verfasserin aut Du, Liping verfasserin aut Zhao, Qi verfasserin aut Chen, Haiyan verfasserin aut Li, Guijie verfasserin aut Wang, Hui verfasserin aut Xu, Yang verfasserin aut Ding, Lan verfasserin aut Ren, Nanqi verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 75(2012), 13-14 vom: 04. Juni, Seite 747-753 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:75 year:2012 number:13-14 day:04 month:06 pages:747-753 https://dx.doi.org/10.1007/s10337-012-2252-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 75 2012 13-14 04 06 747-753 |
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10.1007/s10337-012-2252-2 doi (DE-627)SPR009555455 (SPR)s10337-012-2252-2-e DE-627 ger DE-627 rakwb eng 540 ASE 540 ASE 35.29 bkl Song, Weitao verfasserin aut Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. High performance liquid chromatography (dpeaa)DE-He213 Microwave-assisted steam extraction (dpeaa)DE-He213 Dynamic microwave-assisted extraction (dpeaa)DE-He213 Paeonol (dpeaa)DE-He213 Cai, Haoran verfasserin aut Du, Liping verfasserin aut Zhao, Qi verfasserin aut Chen, Haiyan verfasserin aut Li, Guijie verfasserin aut Wang, Hui verfasserin aut Xu, Yang verfasserin aut Ding, Lan verfasserin aut Ren, Nanqi verfasserin aut Enthalten in Chromatographia Wiesbaden : Vieweg, 1968 75(2012), 13-14 vom: 04. Juni, Seite 747-753 (DE-627)320592219 (DE-600)2019091-8 1612-1112 nnns volume:75 year:2012 number:13-14 day:04 month:06 pages:747-753 https://dx.doi.org/10.1007/s10337-012-2252-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.29 ASE AR 75 2012 13-14 04 06 747-753 |
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Enthalten in Chromatographia 75(2012), 13-14 vom: 04. Juni, Seite 747-753 volume:75 year:2012 number:13-14 day:04 month:06 pages:747-753 |
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High performance liquid chromatography Microwave-assisted steam extraction Dynamic microwave-assisted extraction Paeonol |
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Song, Weitao @@aut@@ Cai, Haoran @@aut@@ Du, Liping @@aut@@ Zhao, Qi @@aut@@ Chen, Haiyan @@aut@@ Li, Guijie @@aut@@ Wang, Hui @@aut@@ Xu, Yang @@aut@@ Ding, Lan @@aut@@ Ren, Nanqi @@aut@@ |
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2012-06-04T00:00:00Z |
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This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. 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Song, Weitao |
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Song, Weitao ddc 540 bkl 35.29 misc High performance liquid chromatography misc Microwave-assisted steam extraction misc Dynamic microwave-assisted extraction misc Paeonol Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC |
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540 ASE 35.29 bkl Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC High performance liquid chromatography (dpeaa)DE-He213 Microwave-assisted steam extraction (dpeaa)DE-He213 Dynamic microwave-assisted extraction (dpeaa)DE-He213 Paeonol (dpeaa)DE-He213 |
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ddc 540 bkl 35.29 misc High performance liquid chromatography misc Microwave-assisted steam extraction misc Dynamic microwave-assisted extraction misc Paeonol |
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ddc 540 bkl 35.29 misc High performance liquid chromatography misc Microwave-assisted steam extraction misc Dynamic microwave-assisted extraction misc Paeonol |
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Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC |
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Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC |
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Song, Weitao Cai, Haoran Du, Liping Zhao, Qi Chen, Haiyan Li, Guijie Wang, Hui Xu, Yang Ding, Lan Ren, Nanqi |
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Song, Weitao |
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fast determination of paeonol from cortex moutan by microwave-assisted steam extraction followed by hplc |
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Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC |
| abstract |
Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. |
| abstractGer |
Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. |
| abstract_unstemmed |
Abstract In this work, microwave-assisted steam extraction (MASE) followed by high performance liquid chromatography is described for the extraction and determination of paeonol in Cortex moutan. This new approach was based on the combination of microwave-assisted extraction and steam distillation. No organic solvent was used and no clean-up step was required before chromatographic analysis. The extraction vessel and water were both under microwave radiation: the water was still heated while the generated steam flowed through the sample. Factors such as collection volume, microwave power, mass of the sample, and mixed proportion of the sample and quartz sand were investigated. The intra- and inter-day relative standard deviation values of <9 % show that the proposed method had good repeatability. To demonstrate its feasibility, the MASE was compared with other extraction methods such as dynamic microwave-assisted extraction, ultrasonic extraction, and steam distillation, and the experimental results show that the MASE was a rapid, effective, and environmentally friendly alternative for the extraction of paeonol in Cortex moutan. Finally, the proposed method was applied on Cortex moutan samples from different producing areas and the results were satisfactory. |
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Fast Determination of Paeonol from Cortex moutan by Microwave-Assisted Steam Extraction Followed by HPLC |
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Cai, Haoran Du, Liping Zhao, Qi Chen, Haiyan Li, Guijie Wang, Hui Xu, Yang Ding, Lan Ren, Nanqi |
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| score |
7.3994513 |