Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane

Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectrosc...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Sagar, T. V. [verfasserIn] Padmakar, D. [verfasserIn] Lingaiah, N. [verfasserIn] Sai Prasad, P. S. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2019

Schlagwörter:	Ni–Cu bimetallic catalysts Ni–O–Ce solid solution Ceria support Methane dry reforming Syngas

Übergeordnetes Werk:	Enthalten in: Catalysis letters - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1988, 149(2019), 9 vom: 07. Mai, Seite 2597-2606
Übergeordnetes Werk:	volume:149 ; year:2019 ; number:9 ; day:07 ; month:05 ; pages:2597-2606

Links:	Volltext

DOI / URN:	10.1007/s10562-019-02801-y

Katalog-ID:	SPR01135691X

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520			\|a Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability.
650		4	\|a Ni–Cu bimetallic catalysts \|7 (dpeaa)DE-He213
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650		4	\|a Syngas \|7 (dpeaa)DE-He213
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700	1		\|a Lingaiah, N. \|e verfasserin \|4 aut
700	1		\|a Sai Prasad, P. S. \|e verfasserin \|4 aut
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matchkey_str	article:1572879X:2019----::nlecosldouinomtooteciiyfe_spotdiuieoieaa
hierarchy_sort_str	2019
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publishDate	2019
allfields	10.1007/s10562-019-02801-y doi (DE-627)SPR01135691X (SPR)s10562-019-02801-y-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.17 bkl Sagar, T. V. verfasserin aut Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane 2019 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability. Ni–Cu bimetallic catalysts (dpeaa)DE-He213 Ni–O–Ce solid solution (dpeaa)DE-He213 Ceria support (dpeaa)DE-He213 Methane dry reforming (dpeaa)DE-He213 Syngas (dpeaa)DE-He213 Padmakar, D. verfasserin aut Lingaiah, N. verfasserin aut Sai Prasad, P. S. verfasserin aut Enthalten in Catalysis letters Dordrecht [u.a.] : Springer Science + Business Media B.V, 1988 149(2019), 9 vom: 07. Mai, Seite 2597-2606 (DE-627)306717638 (DE-600)1501518-X 1572-879X nnns volume:149 year:2019 number:9 day:07 month:05 pages:2597-2606 https://dx.doi.org/10.1007/s10562-019-02801-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.17 ASE AR 149 2019 9 07 05 2597-2606
spelling	10.1007/s10562-019-02801-y doi (DE-627)SPR01135691X (SPR)s10562-019-02801-y-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.17 bkl Sagar, T. V. verfasserin aut Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane 2019 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability. Ni–Cu bimetallic catalysts (dpeaa)DE-He213 Ni–O–Ce solid solution (dpeaa)DE-He213 Ceria support (dpeaa)DE-He213 Methane dry reforming (dpeaa)DE-He213 Syngas (dpeaa)DE-He213 Padmakar, D. verfasserin aut Lingaiah, N. verfasserin aut Sai Prasad, P. S. verfasserin aut Enthalten in Catalysis letters Dordrecht [u.a.] : Springer Science + Business Media B.V, 1988 149(2019), 9 vom: 07. Mai, Seite 2597-2606 (DE-627)306717638 (DE-600)1501518-X 1572-879X nnns volume:149 year:2019 number:9 day:07 month:05 pages:2597-2606 https://dx.doi.org/10.1007/s10562-019-02801-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.17 ASE AR 149 2019 9 07 05 2597-2606
allfields_unstemmed	10.1007/s10562-019-02801-y doi (DE-627)SPR01135691X (SPR)s10562-019-02801-y-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.17 bkl Sagar, T. V. verfasserin aut Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane 2019 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability. Ni–Cu bimetallic catalysts (dpeaa)DE-He213 Ni–O–Ce solid solution (dpeaa)DE-He213 Ceria support (dpeaa)DE-He213 Methane dry reforming (dpeaa)DE-He213 Syngas (dpeaa)DE-He213 Padmakar, D. verfasserin aut Lingaiah, N. verfasserin aut Sai Prasad, P. S. verfasserin aut Enthalten in Catalysis letters Dordrecht [u.a.] : Springer Science + Business Media B.V, 1988 149(2019), 9 vom: 07. Mai, Seite 2597-2606 (DE-627)306717638 (DE-600)1501518-X 1572-879X nnns volume:149 year:2019 number:9 day:07 month:05 pages:2597-2606 https://dx.doi.org/10.1007/s10562-019-02801-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.17 ASE AR 149 2019 9 07 05 2597-2606
allfieldsGer	10.1007/s10562-019-02801-y doi (DE-627)SPR01135691X (SPR)s10562-019-02801-y-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.17 bkl Sagar, T. V. verfasserin aut Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane 2019 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability. Ni–Cu bimetallic catalysts (dpeaa)DE-He213 Ni–O–Ce solid solution (dpeaa)DE-He213 Ceria support (dpeaa)DE-He213 Methane dry reforming (dpeaa)DE-He213 Syngas (dpeaa)DE-He213 Padmakar, D. verfasserin aut Lingaiah, N. verfasserin aut Sai Prasad, P. S. verfasserin aut Enthalten in Catalysis letters Dordrecht [u.a.] : Springer Science + Business Media B.V, 1988 149(2019), 9 vom: 07. Mai, Seite 2597-2606 (DE-627)306717638 (DE-600)1501518-X 1572-879X nnns volume:149 year:2019 number:9 day:07 month:05 pages:2597-2606 https://dx.doi.org/10.1007/s10562-019-02801-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.17 ASE AR 149 2019 9 07 05 2597-2606
allfieldsSound	10.1007/s10562-019-02801-y doi (DE-627)SPR01135691X (SPR)s10562-019-02801-y-e DE-627 ger DE-627 rakwb eng 540 660 ASE 35.17 bkl Sagar, T. V. verfasserin aut Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane 2019 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability. Ni–Cu bimetallic catalysts (dpeaa)DE-He213 Ni–O–Ce solid solution (dpeaa)DE-He213 Ceria support (dpeaa)DE-He213 Methane dry reforming (dpeaa)DE-He213 Syngas (dpeaa)DE-He213 Padmakar, D. verfasserin aut Lingaiah, N. verfasserin aut Sai Prasad, P. S. verfasserin aut Enthalten in Catalysis letters Dordrecht [u.a.] : Springer Science + Business Media B.V, 1988 149(2019), 9 vom: 07. Mai, Seite 2597-2606 (DE-627)306717638 (DE-600)1501518-X 1572-879X nnns volume:149 year:2019 number:9 day:07 month:05 pages:2597-2606 https://dx.doi.org/10.1007/s10562-019-02801-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.17 ASE AR 149 2019 9 07 05 2597-2606
language	English
source	Enthalten in Catalysis letters 149(2019), 9 vom: 07. Mai, Seite 2597-2606 volume:149 year:2019 number:9 day:07 month:05 pages:2597-2606
sourceStr	Enthalten in Catalysis letters 149(2019), 9 vom: 07. Mai, Seite 2597-2606 volume:149 year:2019 number:9 day:07 month:05 pages:2597-2606
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Ni–Cu bimetallic catalysts Ni–O–Ce solid solution Ceria support Methane dry reforming Syngas
dewey-raw	540
isfreeaccess_bool	false
container_title	Catalysis letters
authorswithroles_txt_mv	Sagar, T. V. @@aut@@ Padmakar, D. @@aut@@ Lingaiah, N. @@aut@@ Sai Prasad, P. S. @@aut@@
publishDateDaySort_date	2019-05-07T00:00:00Z
hierarchy_top_id	306717638
dewey-sort	3540
id	SPR01135691X
language_de	englisch
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The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. 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author	Sagar, T. V.
spellingShingle	Sagar, T. V. ddc 540 bkl 35.17 misc Ni–Cu bimetallic catalysts misc Ni–O–Ce solid solution misc Ceria support misc Methane dry reforming misc Syngas Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane
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topic_title	540 660 ASE 35.17 bkl Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane Ni–Cu bimetallic catalysts (dpeaa)DE-He213 Ni–O–Ce solid solution (dpeaa)DE-He213 Ceria support (dpeaa)DE-He213 Methane dry reforming (dpeaa)DE-He213 Syngas (dpeaa)DE-He213
topic	ddc 540 bkl 35.17 misc Ni–Cu bimetallic catalysts misc Ni–O–Ce solid solution misc Ceria support misc Methane dry reforming misc Syngas
topic_unstemmed	ddc 540 bkl 35.17 misc Ni–Cu bimetallic catalysts misc Ni–O–Ce solid solution misc Ceria support misc Methane dry reforming misc Syngas
topic_browse	ddc 540 bkl 35.17 misc Ni–Cu bimetallic catalysts misc Ni–O–Ce solid solution misc Ceria support misc Methane dry reforming misc Syngas
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title	Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane
ctrlnum	(DE-627)SPR01135691X (SPR)s10562-019-02801-y-e
title_full	Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane
author_sort	Sagar, T. V.
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author_browse	Sagar, T. V. Padmakar, D. Lingaiah, N. Sai Prasad, P. S.
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title_sort	influence of solid solution formation on the activity of $ ceo_{2} $ supported ni–cu mixed oxide catalysts in dry reforming of methane
title_auth	Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane
abstract	Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability.
abstractGer	Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability.
abstract_unstemmed	Abstract A series of $ CeO_{2} $ supported 20 wt% Ni–Cu mixed oxide catalysts was prepared by co-impregnation, varying the Ni–Cu composition. The catalysts were characterized by nitrogen adsorption for BET surface area, X-ray diffraction (XRD), Temperature programmed reduction (TPR), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), $ H_{2} $ Chemisorption, Scanning electron microscopy (SEM) and CHNS analysis techniques. They were evaluated for dry reforming of methane to produce syngas in the temperature range of 600–800 °C and at a GHSV = 28,800 $ h^{−1} $. 5 wt% Ni + 15 wt% Cu/$ CeO_{2} $ displayed superior activity among the series. The incorporation of Ni metal in $ CeO_{2} $ lattice led to the formation of Ni–O–Ce solid solution up to 5 wt% Ni in the catalyst. This catalyst also showed good stability due to less coke formation. Resistance towards coking was observed to be mainly due to the abundance of labile oxygen in the solid solution. Graphical Abstract Ni incorporation in $ CeO_{2} $ results in significant change in the $ CeO_{2} $ lattice leading to solid solution formation and enhancing metal dispersion. Increase in the oxygen storage capacity (OSC) with the addition of Cu helps improve catalyst stability.
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container_issue	9
title_short	Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane
url	https://dx.doi.org/10.1007/s10562-019-02801-y
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author2	Padmakar, D. Lingaiah, N. Sai Prasad, P. S.
author2Str	Padmakar, D. Lingaiah, N. Sai Prasad, P. S.
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doi_str	10.1007/s10562-019-02801-y
up_date	2024-07-03T22:08:42.673Z
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Influence of Solid Solution Formation on the Activity of $ CeO_{2} $ Supported Ni–Cu Mixed Oxide Catalysts in Dry Reforming of Methane

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