Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones
During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%),...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Shchekotikhin, A. E. [verfasserIn] Luzikov, Yu. N. [verfasserIn] Buyanov, V. N. [verfasserIn] Preobrazhenskaya, M. N. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2009 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Chemistry of heterocyclic compounds - New York, NY [u.a.] : Consultants Bureau, 1965, 45(2009), 2 vom: Feb., Seite 151-160 |
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| Übergeordnetes Werk: |
volume:45 ; year:2009 ; number:2 ; month:02 ; pages:151-160 |
| Links: |
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| DOI / URN: |
10.1007/s10593-009-0244-4 |
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| Katalog-ID: |
SPR011607068 |
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| 100 | 1 | |a Shchekotikhin, A. E. |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones |
| 264 | 1 | |c 2009 | |
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| 520 | |a During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. | ||
| 650 | 4 | |a anthra[2,1- |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a ][1,3]dioxole-6,11-dione |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a anthra[2,3- |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a ]furan-5,10-dione |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a anthra[1,2- |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a ]furan-6,11-dione |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a anthra[1,3- |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a ]furan-2,6,11(3H)-trione |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a 2,3-dichloroquinizarine |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a methyl pivaloylacetate |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a condensation |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a modification |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Luzikov, Yu. N. |e verfasserin |4 aut | |
| 700 | 1 | |a Buyanov, V. N. |e verfasserin |4 aut | |
| 700 | 1 | |a Preobrazhenskaya, M. N. |e verfasserin |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Chemistry of heterocyclic compounds |d New York, NY [u.a.] : Consultants Bureau, 1965 |g 45(2009), 2 vom: Feb., Seite 151-160 |w (DE-627)325568561 |w (DE-600)2037128-7 |x 1573-8353 |7 nnns |
| 773 | 1 | 8 | |g volume:45 |g year:2009 |g number:2 |g month:02 |g pages:151-160 |
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2009 |
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2009 |
| allfields |
10.1007/s10593-009-0244-4 doi (DE-627)SPR011607068 (SPR)s10593-009-0244-4-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Shchekotikhin, A. E. verfasserin aut Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. anthra[2,1- (dpeaa)DE-He213 ][1,3]dioxole-6,11-dione (dpeaa)DE-He213 anthra[2,3- (dpeaa)DE-He213 ]furan-5,10-dione (dpeaa)DE-He213 anthra[1,2- (dpeaa)DE-He213 ]furan-6,11-dione (dpeaa)DE-He213 anthra[1,3- (dpeaa)DE-He213 ]furan-2,6,11(3H)-trione (dpeaa)DE-He213 2,3-dichloroquinizarine (dpeaa)DE-He213 methyl pivaloylacetate (dpeaa)DE-He213 condensation (dpeaa)DE-He213 modification (dpeaa)DE-He213 Luzikov, Yu. N. verfasserin aut Buyanov, V. N. verfasserin aut Preobrazhenskaya, M. N. verfasserin aut Enthalten in Chemistry of heterocyclic compounds New York, NY [u.a.] : Consultants Bureau, 1965 45(2009), 2 vom: Feb., Seite 151-160 (DE-627)325568561 (DE-600)2037128-7 1573-8353 nnns volume:45 year:2009 number:2 month:02 pages:151-160 https://dx.doi.org/10.1007/s10593-009-0244-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 45 2009 2 02 151-160 |
| spelling |
10.1007/s10593-009-0244-4 doi (DE-627)SPR011607068 (SPR)s10593-009-0244-4-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Shchekotikhin, A. E. verfasserin aut Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. anthra[2,1- (dpeaa)DE-He213 ][1,3]dioxole-6,11-dione (dpeaa)DE-He213 anthra[2,3- (dpeaa)DE-He213 ]furan-5,10-dione (dpeaa)DE-He213 anthra[1,2- (dpeaa)DE-He213 ]furan-6,11-dione (dpeaa)DE-He213 anthra[1,3- (dpeaa)DE-He213 ]furan-2,6,11(3H)-trione (dpeaa)DE-He213 2,3-dichloroquinizarine (dpeaa)DE-He213 methyl pivaloylacetate (dpeaa)DE-He213 condensation (dpeaa)DE-He213 modification (dpeaa)DE-He213 Luzikov, Yu. N. verfasserin aut Buyanov, V. N. verfasserin aut Preobrazhenskaya, M. N. verfasserin aut Enthalten in Chemistry of heterocyclic compounds New York, NY [u.a.] : Consultants Bureau, 1965 45(2009), 2 vom: Feb., Seite 151-160 (DE-627)325568561 (DE-600)2037128-7 1573-8353 nnns volume:45 year:2009 number:2 month:02 pages:151-160 https://dx.doi.org/10.1007/s10593-009-0244-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 45 2009 2 02 151-160 |
| allfields_unstemmed |
10.1007/s10593-009-0244-4 doi (DE-627)SPR011607068 (SPR)s10593-009-0244-4-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Shchekotikhin, A. E. verfasserin aut Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. anthra[2,1- (dpeaa)DE-He213 ][1,3]dioxole-6,11-dione (dpeaa)DE-He213 anthra[2,3- (dpeaa)DE-He213 ]furan-5,10-dione (dpeaa)DE-He213 anthra[1,2- (dpeaa)DE-He213 ]furan-6,11-dione (dpeaa)DE-He213 anthra[1,3- (dpeaa)DE-He213 ]furan-2,6,11(3H)-trione (dpeaa)DE-He213 2,3-dichloroquinizarine (dpeaa)DE-He213 methyl pivaloylacetate (dpeaa)DE-He213 condensation (dpeaa)DE-He213 modification (dpeaa)DE-He213 Luzikov, Yu. N. verfasserin aut Buyanov, V. N. verfasserin aut Preobrazhenskaya, M. N. verfasserin aut Enthalten in Chemistry of heterocyclic compounds New York, NY [u.a.] : Consultants Bureau, 1965 45(2009), 2 vom: Feb., Seite 151-160 (DE-627)325568561 (DE-600)2037128-7 1573-8353 nnns volume:45 year:2009 number:2 month:02 pages:151-160 https://dx.doi.org/10.1007/s10593-009-0244-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 45 2009 2 02 151-160 |
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10.1007/s10593-009-0244-4 doi (DE-627)SPR011607068 (SPR)s10593-009-0244-4-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Shchekotikhin, A. E. verfasserin aut Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. anthra[2,1- (dpeaa)DE-He213 ][1,3]dioxole-6,11-dione (dpeaa)DE-He213 anthra[2,3- (dpeaa)DE-He213 ]furan-5,10-dione (dpeaa)DE-He213 anthra[1,2- (dpeaa)DE-He213 ]furan-6,11-dione (dpeaa)DE-He213 anthra[1,3- (dpeaa)DE-He213 ]furan-2,6,11(3H)-trione (dpeaa)DE-He213 2,3-dichloroquinizarine (dpeaa)DE-He213 methyl pivaloylacetate (dpeaa)DE-He213 condensation (dpeaa)DE-He213 modification (dpeaa)DE-He213 Luzikov, Yu. N. verfasserin aut Buyanov, V. N. verfasserin aut Preobrazhenskaya, M. N. verfasserin aut Enthalten in Chemistry of heterocyclic compounds New York, NY [u.a.] : Consultants Bureau, 1965 45(2009), 2 vom: Feb., Seite 151-160 (DE-627)325568561 (DE-600)2037128-7 1573-8353 nnns volume:45 year:2009 number:2 month:02 pages:151-160 https://dx.doi.org/10.1007/s10593-009-0244-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 45 2009 2 02 151-160 |
| allfieldsSound |
10.1007/s10593-009-0244-4 doi (DE-627)SPR011607068 (SPR)s10593-009-0244-4-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Shchekotikhin, A. E. verfasserin aut Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. anthra[2,1- (dpeaa)DE-He213 ][1,3]dioxole-6,11-dione (dpeaa)DE-He213 anthra[2,3- (dpeaa)DE-He213 ]furan-5,10-dione (dpeaa)DE-He213 anthra[1,2- (dpeaa)DE-He213 ]furan-6,11-dione (dpeaa)DE-He213 anthra[1,3- (dpeaa)DE-He213 ]furan-2,6,11(3H)-trione (dpeaa)DE-He213 2,3-dichloroquinizarine (dpeaa)DE-He213 methyl pivaloylacetate (dpeaa)DE-He213 condensation (dpeaa)DE-He213 modification (dpeaa)DE-He213 Luzikov, Yu. N. verfasserin aut Buyanov, V. N. verfasserin aut Preobrazhenskaya, M. N. verfasserin aut Enthalten in Chemistry of heterocyclic compounds New York, NY [u.a.] : Consultants Bureau, 1965 45(2009), 2 vom: Feb., Seite 151-160 (DE-627)325568561 (DE-600)2037128-7 1573-8353 nnns volume:45 year:2009 number:2 month:02 pages:151-160 https://dx.doi.org/10.1007/s10593-009-0244-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 45 2009 2 02 151-160 |
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English |
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Enthalten in Chemistry of heterocyclic compounds 45(2009), 2 vom: Feb., Seite 151-160 volume:45 year:2009 number:2 month:02 pages:151-160 |
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Enthalten in Chemistry of heterocyclic compounds 45(2009), 2 vom: Feb., Seite 151-160 volume:45 year:2009 number:2 month:02 pages:151-160 |
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findex.gbv.de |
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anthra[2,1- ][1,3]dioxole-6,11-dione anthra[2,3- ]furan-5,10-dione anthra[1,2- ]furan-6,11-dione anthra[1,3- ]furan-2,6,11(3H)-trione 2,3-dichloroquinizarine methyl pivaloylacetate condensation modification |
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Chemistry of heterocyclic compounds |
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Shchekotikhin, A. E. @@aut@@ Luzikov, Yu. N. @@aut@@ Buyanov, V. N. @@aut@@ Preobrazhenskaya, M. N. @@aut@@ |
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2009-02-01T00:00:00Z |
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SPR011607068 |
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E.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2009</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. 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|
| author |
Shchekotikhin, A. E. |
| spellingShingle |
Shchekotikhin, A. E. ddc 540 bkl 35.00 misc anthra[2,1- misc ][1,3]dioxole-6,11-dione misc anthra[2,3- misc ]furan-5,10-dione misc anthra[1,2- misc ]furan-6,11-dione misc anthra[1,3- misc ]furan-2,6,11(3H)-trione misc 2,3-dichloroquinizarine misc methyl pivaloylacetate misc condensation misc modification Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones |
| authorStr |
Shchekotikhin, A. E. |
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@@773@@(DE-627)325568561 |
| format |
electronic Article |
| dewey-ones |
540 - Chemistry & allied sciences |
| delete_txt_mv |
keep |
| author_role |
aut aut aut aut |
| collection |
springer |
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true |
| illustrated |
Not Illustrated |
| issn |
1573-8353 |
| topic_title |
540 ASE 35.00 bkl Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones anthra[2,1- (dpeaa)DE-He213 ][1,3]dioxole-6,11-dione (dpeaa)DE-He213 anthra[2,3- (dpeaa)DE-He213 ]furan-5,10-dione (dpeaa)DE-He213 anthra[1,2- (dpeaa)DE-He213 ]furan-6,11-dione (dpeaa)DE-He213 anthra[1,3- (dpeaa)DE-He213 ]furan-2,6,11(3H)-trione (dpeaa)DE-He213 2,3-dichloroquinizarine (dpeaa)DE-He213 methyl pivaloylacetate (dpeaa)DE-He213 condensation (dpeaa)DE-He213 modification (dpeaa)DE-He213 |
| topic |
ddc 540 bkl 35.00 misc anthra[2,1- misc ][1,3]dioxole-6,11-dione misc anthra[2,3- misc ]furan-5,10-dione misc anthra[1,2- misc ]furan-6,11-dione misc anthra[1,3- misc ]furan-2,6,11(3H)-trione misc 2,3-dichloroquinizarine misc methyl pivaloylacetate misc condensation misc modification |
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ddc 540 bkl 35.00 misc anthra[2,1- misc ][1,3]dioxole-6,11-dione misc anthra[2,3- misc ]furan-5,10-dione misc anthra[1,2- misc ]furan-6,11-dione misc anthra[1,3- misc ]furan-2,6,11(3H)-trione misc 2,3-dichloroquinizarine misc methyl pivaloylacetate misc condensation misc modification |
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Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones |
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Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones |
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Shchekotikhin, A. E. |
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Chemistry of heterocyclic compounds |
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Shchekotikhin, A. E. Luzikov, Yu. N. Buyanov, V. N. Preobrazhenskaya, M. N. |
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heterocyclic analogs of 5,12-naphthacenequinone 8.* synthesis of furano-anthraquinones |
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Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones |
| abstract |
During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. |
| abstractGer |
During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. |
| abstract_unstemmed |
During the condensation of 2,3-dichloroquinizarine with methyl pivaloylacetate in the presence of potassium carbonate in dimethyl sulfoxide the main reaction products are derivatives of angular 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione (about 70%) and anthra[2,1-d][1,3]dioxole-6,11-dione (15%), whereas the yield of the targeted linear methyl 2-tert-butyl-4,11-dihydroxyanthra[2,3-b]furan-5,10-dione-3-carboxylate is only 2%. Methods are developed for modification of the obtained 3-pivaloylanthra[1,2-b]furan-2,6,11(3H)-trione, making it possible to use it for the synthesis of the tert-butyl derivatives of linear anthra[2,3-b]furan-5,10-dione or angular anthra[1,2-b]furan-6,11-dione. |
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Heterocyclic analogs of 5,12-naphthacenequinone 8.* Synthesis of furano-anthraquinones |
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| score |
7.4008636 |