Phase quantification of mullite–zirconia and zircon commercial powders using PAC and XRD techniques
Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, w...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Rendtorff, Nicolás M. [verfasserIn] Conconi, Maria S. [verfasserIn] Aglietti, Esteban F. [verfasserIn] Chain, Cecilia Y. [verfasserIn] Pasquevich, Alberto F. [verfasserIn] Rivas, Patricia C. [verfasserIn] Martínez, Jorge A. [verfasserIn] Caracoche, María C. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2010 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Hyperfine interactions - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1975, 198(2010), 1-3 vom: Juni, Seite 211-218 |
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| Übergeordnetes Werk: |
volume:198 ; year:2010 ; number:1-3 ; month:06 ; pages:211-218 |
| Links: |
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| DOI / URN: |
10.1007/s10751-010-0177-4 |
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| Katalog-ID: |
SPR013003070 |
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| 520 | |a Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. | ||
| 650 | 4 | |a Ceramics |7 (dpeaa)DE-He213 | |
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| 650 | 4 | |a PAC |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Conconi, Maria S. |e verfasserin |4 aut | |
| 700 | 1 | |a Aglietti, Esteban F. |e verfasserin |4 aut | |
| 700 | 1 | |a Chain, Cecilia Y. |e verfasserin |4 aut | |
| 700 | 1 | |a Pasquevich, Alberto F. |e verfasserin |4 aut | |
| 700 | 1 | |a Rivas, Patricia C. |e verfasserin |4 aut | |
| 700 | 1 | |a Martínez, Jorge A. |e verfasserin |4 aut | |
| 700 | 1 | |a Caracoche, María C. |e verfasserin |4 aut | |
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10.1007/s10751-010-0177-4 doi (DE-627)SPR013003070 (SPR)s10751-010-0177-4-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Rendtorff, Nicolás M. verfasserin aut Phase quantification of mullite–zirconia and zircon commercial powders using PAC and XRD techniques 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. Ceramics (dpeaa)DE-He213 XRD techniques (dpeaa)DE-He213 Gamma ray (dpeaa)DE-He213 PAC (dpeaa)DE-He213 Conconi, Maria S. verfasserin aut Aglietti, Esteban F. verfasserin aut Chain, Cecilia Y. verfasserin aut Pasquevich, Alberto F. verfasserin aut Rivas, Patricia C. verfasserin aut Martínez, Jorge A. verfasserin aut Caracoche, María C. verfasserin aut Enthalten in Hyperfine interactions Dordrecht [u.a.] : Springer Science + Business Media B.V, 1975 198(2010), 1-3 vom: Juni, Seite 211-218 (DE-627)320612953 (DE-600)2021614-2 1572-9540 nnns volume:198 year:2010 number:1-3 month:06 pages:211-218 https://dx.doi.org/10.1007/s10751-010-0177-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4313 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4700 33.00 ASE AR 198 2010 1-3 06 211-218 |
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10.1007/s10751-010-0177-4 doi (DE-627)SPR013003070 (SPR)s10751-010-0177-4-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Rendtorff, Nicolás M. verfasserin aut Phase quantification of mullite–zirconia and zircon commercial powders using PAC and XRD techniques 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. Ceramics (dpeaa)DE-He213 XRD techniques (dpeaa)DE-He213 Gamma ray (dpeaa)DE-He213 PAC (dpeaa)DE-He213 Conconi, Maria S. verfasserin aut Aglietti, Esteban F. verfasserin aut Chain, Cecilia Y. verfasserin aut Pasquevich, Alberto F. verfasserin aut Rivas, Patricia C. verfasserin aut Martínez, Jorge A. verfasserin aut Caracoche, María C. verfasserin aut Enthalten in Hyperfine interactions Dordrecht [u.a.] : Springer Science + Business Media B.V, 1975 198(2010), 1-3 vom: Juni, Seite 211-218 (DE-627)320612953 (DE-600)2021614-2 1572-9540 nnns volume:198 year:2010 number:1-3 month:06 pages:211-218 https://dx.doi.org/10.1007/s10751-010-0177-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4313 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4700 33.00 ASE AR 198 2010 1-3 06 211-218 |
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10.1007/s10751-010-0177-4 doi (DE-627)SPR013003070 (SPR)s10751-010-0177-4-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Rendtorff, Nicolás M. verfasserin aut Phase quantification of mullite–zirconia and zircon commercial powders using PAC and XRD techniques 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. Ceramics (dpeaa)DE-He213 XRD techniques (dpeaa)DE-He213 Gamma ray (dpeaa)DE-He213 PAC (dpeaa)DE-He213 Conconi, Maria S. verfasserin aut Aglietti, Esteban F. verfasserin aut Chain, Cecilia Y. verfasserin aut Pasquevich, Alberto F. verfasserin aut Rivas, Patricia C. verfasserin aut Martínez, Jorge A. verfasserin aut Caracoche, María C. verfasserin aut Enthalten in Hyperfine interactions Dordrecht [u.a.] : Springer Science + Business Media B.V, 1975 198(2010), 1-3 vom: Juni, Seite 211-218 (DE-627)320612953 (DE-600)2021614-2 1572-9540 nnns volume:198 year:2010 number:1-3 month:06 pages:211-218 https://dx.doi.org/10.1007/s10751-010-0177-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4313 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4700 33.00 ASE AR 198 2010 1-3 06 211-218 |
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10.1007/s10751-010-0177-4 doi (DE-627)SPR013003070 (SPR)s10751-010-0177-4-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Rendtorff, Nicolás M. verfasserin aut Phase quantification of mullite–zirconia and zircon commercial powders using PAC and XRD techniques 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. Ceramics (dpeaa)DE-He213 XRD techniques (dpeaa)DE-He213 Gamma ray (dpeaa)DE-He213 PAC (dpeaa)DE-He213 Conconi, Maria S. verfasserin aut Aglietti, Esteban F. verfasserin aut Chain, Cecilia Y. verfasserin aut Pasquevich, Alberto F. verfasserin aut Rivas, Patricia C. verfasserin aut Martínez, Jorge A. verfasserin aut Caracoche, María C. verfasserin aut Enthalten in Hyperfine interactions Dordrecht [u.a.] : Springer Science + Business Media B.V, 1975 198(2010), 1-3 vom: Juni, Seite 211-218 (DE-627)320612953 (DE-600)2021614-2 1572-9540 nnns volume:198 year:2010 number:1-3 month:06 pages:211-218 https://dx.doi.org/10.1007/s10751-010-0177-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4313 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4700 33.00 ASE AR 198 2010 1-3 06 211-218 |
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10.1007/s10751-010-0177-4 doi (DE-627)SPR013003070 (SPR)s10751-010-0177-4-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Rendtorff, Nicolás M. verfasserin aut Phase quantification of mullite–zirconia and zircon commercial powders using PAC and XRD techniques 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. Ceramics (dpeaa)DE-He213 XRD techniques (dpeaa)DE-He213 Gamma ray (dpeaa)DE-He213 PAC (dpeaa)DE-He213 Conconi, Maria S. verfasserin aut Aglietti, Esteban F. verfasserin aut Chain, Cecilia Y. verfasserin aut Pasquevich, Alberto F. verfasserin aut Rivas, Patricia C. verfasserin aut Martínez, Jorge A. verfasserin aut Caracoche, María C. verfasserin aut Enthalten in Hyperfine interactions Dordrecht [u.a.] : Springer Science + Business Media B.V, 1975 198(2010), 1-3 vom: Juni, Seite 211-218 (DE-627)320612953 (DE-600)2021614-2 1572-9540 nnns volume:198 year:2010 number:1-3 month:06 pages:211-218 https://dx.doi.org/10.1007/s10751-010-0177-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2061 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4313 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4700 33.00 ASE AR 198 2010 1-3 06 211-218 |
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Enthalten in Hyperfine interactions 198(2010), 1-3 vom: Juni, Seite 211-218 volume:198 year:2010 number:1-3 month:06 pages:211-218 |
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phase quantification of mullite–zirconia and zircon commercial powders using pac and xrd techniques |
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Phase quantification of mullite–zirconia and zircon commercial powders using PAC and XRD techniques |
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Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. |
| abstractGer |
Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. |
| abstract_unstemmed |
Abstract The short range technique of the Perturbed Angular Correlation (PAC) and x-ray diffraction (Rietveld) methods have been employed to determine the phase content in commercial mullite–zirconia and zircon raw materials that are ordinarily used to produce ceramic materials. The PAC technique, which probes zirconium-containing compounds at nanoscopic level, showed that zircon contains crystalline $ ZrSiO_{4 } $ and an important amount of a structurally distorted zircon, which is also observed accompanying monoclinic zirconia in mullite–zirconia. This particular zircon phase was not detected by the long range x-ray diffraction–Rietveld technique. After an annealing treatment, important changes in crystalline contents of the powders allow confirming, by the x-ray diffraction–Rietveld method, the preexistence of this particular zircon phase. This fact must be taken into account when preparing multicomposites based on the present raw materials. |
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