Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition

Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (F...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Jin, Zhengwei [verfasserIn] Wang, Xiaodong [verfasserIn] Cui, Xiuguo [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2006

Schlagwörter:	Mesoporous Silica Mesoporous Material Triblock Copolymer Silica Source Mesoporous Silica Material

Übergeordnetes Werk:	Enthalten in: Journal of materials science - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966, 42(2006), 2 vom: 28. Nov., Seite 465-471
Übergeordnetes Werk:	volume:42 ; year:2006 ; number:2 ; day:28 ; month:11 ; pages:465-471

Links:	Volltext

DOI / URN:	10.1007/s10853-006-1170-9

Katalog-ID:	SPR013824783

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520			\|a Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation.
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allfields	10.1007/s10853-006-1170-9 doi (DE-627)SPR013824783 (SPR)s10853-006-1170-9-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Jin, Zhengwei verfasserin aut Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation. Mesoporous Silica (dpeaa)DE-He213 Mesoporous Material (dpeaa)DE-He213 Triblock Copolymer (dpeaa)DE-He213 Silica Source (dpeaa)DE-He213 Mesoporous Silica Material (dpeaa)DE-He213 Wang, Xiaodong verfasserin aut Cui, Xiuguo verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 42(2006), 2 vom: 28. Nov., Seite 465-471 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:42 year:2006 number:2 day:28 month:11 pages:465-471 https://dx.doi.org/10.1007/s10853-006-1170-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 42 2006 2 28 11 465-471
spelling	10.1007/s10853-006-1170-9 doi (DE-627)SPR013824783 (SPR)s10853-006-1170-9-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Jin, Zhengwei verfasserin aut Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation. Mesoporous Silica (dpeaa)DE-He213 Mesoporous Material (dpeaa)DE-He213 Triblock Copolymer (dpeaa)DE-He213 Silica Source (dpeaa)DE-He213 Mesoporous Silica Material (dpeaa)DE-He213 Wang, Xiaodong verfasserin aut Cui, Xiuguo verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 42(2006), 2 vom: 28. Nov., Seite 465-471 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:42 year:2006 number:2 day:28 month:11 pages:465-471 https://dx.doi.org/10.1007/s10853-006-1170-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 42 2006 2 28 11 465-471
allfields_unstemmed	10.1007/s10853-006-1170-9 doi (DE-627)SPR013824783 (SPR)s10853-006-1170-9-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Jin, Zhengwei verfasserin aut Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation. Mesoporous Silica (dpeaa)DE-He213 Mesoporous Material (dpeaa)DE-He213 Triblock Copolymer (dpeaa)DE-He213 Silica Source (dpeaa)DE-He213 Mesoporous Silica Material (dpeaa)DE-He213 Wang, Xiaodong verfasserin aut Cui, Xiuguo verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 42(2006), 2 vom: 28. Nov., Seite 465-471 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:42 year:2006 number:2 day:28 month:11 pages:465-471 https://dx.doi.org/10.1007/s10853-006-1170-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 42 2006 2 28 11 465-471
allfieldsGer	10.1007/s10853-006-1170-9 doi (DE-627)SPR013824783 (SPR)s10853-006-1170-9-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Jin, Zhengwei verfasserin aut Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation. Mesoporous Silica (dpeaa)DE-He213 Mesoporous Material (dpeaa)DE-He213 Triblock Copolymer (dpeaa)DE-He213 Silica Source (dpeaa)DE-He213 Mesoporous Silica Material (dpeaa)DE-He213 Wang, Xiaodong verfasserin aut Cui, Xiuguo verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 42(2006), 2 vom: 28. Nov., Seite 465-471 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:42 year:2006 number:2 day:28 month:11 pages:465-471 https://dx.doi.org/10.1007/s10853-006-1170-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 42 2006 2 28 11 465-471
allfieldsSound	10.1007/s10853-006-1170-9 doi (DE-627)SPR013824783 (SPR)s10853-006-1170-9-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Jin, Zhengwei verfasserin aut Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation. Mesoporous Silica (dpeaa)DE-He213 Mesoporous Material (dpeaa)DE-He213 Triblock Copolymer (dpeaa)DE-He213 Silica Source (dpeaa)DE-He213 Mesoporous Silica Material (dpeaa)DE-He213 Wang, Xiaodong verfasserin aut Cui, Xiuguo verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 42(2006), 2 vom: 28. Nov., Seite 465-471 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:42 year:2006 number:2 day:28 month:11 pages:465-471 https://dx.doi.org/10.1007/s10853-006-1170-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 42 2006 2 28 11 465-471
language	English
source	Enthalten in Journal of materials science 42(2006), 2 vom: 28. Nov., Seite 465-471 volume:42 year:2006 number:2 day:28 month:11 pages:465-471
sourceStr	Enthalten in Journal of materials science 42(2006), 2 vom: 28. Nov., Seite 465-471 volume:42 year:2006 number:2 day:28 month:11 pages:465-471
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Mesoporous Silica Mesoporous Material Triblock Copolymer Silica Source Mesoporous Silica Material
dewey-raw	670
isfreeaccess_bool	false
container_title	Journal of materials science
authorswithroles_txt_mv	Jin, Zhengwei @@aut@@ Wang, Xiaodong @@aut@@ Cui, Xiuguo @@aut@@
publishDateDaySort_date	2006-11-28T00:00:00Z
hierarchy_top_id	315293969
dewey-sort	3670
id	SPR013824783
language_de	englisch
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author	Jin, Zhengwei
spellingShingle	Jin, Zhengwei ddc 670 bkl 51.00 misc Mesoporous Silica misc Mesoporous Material misc Triblock Copolymer misc Silica Source misc Mesoporous Silica Material Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition
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topic_title	670 ASE 51.00 bkl Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition Mesoporous Silica (dpeaa)DE-He213 Mesoporous Material (dpeaa)DE-He213 Triblock Copolymer (dpeaa)DE-He213 Silica Source (dpeaa)DE-He213 Mesoporous Silica Material (dpeaa)DE-He213
topic	ddc 670 bkl 51.00 misc Mesoporous Silica misc Mesoporous Material misc Triblock Copolymer misc Silica Source misc Mesoporous Silica Material
topic_unstemmed	ddc 670 bkl 51.00 misc Mesoporous Silica misc Mesoporous Material misc Triblock Copolymer misc Silica Source misc Mesoporous Silica Material
topic_browse	ddc 670 bkl 51.00 misc Mesoporous Silica misc Mesoporous Material misc Triblock Copolymer misc Silica Source misc Mesoporous Silica Material
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title	Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition
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title_full	Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition
author_sort	Jin, Zhengwei
journal	Journal of materials science
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author_browse	Jin, Zhengwei Wang, Xiaodong Cui, Xiuguo
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title_sort	synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition
title_auth	Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition
abstract	Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation.
abstractGer	Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation.
abstract_unstemmed	Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. The mesoporous silica prepared in this study exhibits potential applications to catalysis, sensoring, and separation.
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title_short	Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition
url	https://dx.doi.org/10.1007/s10853-006-1170-9
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author2	Wang, Xiaodong Cui, Xiuguo
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doi_str	10.1007/s10853-006-1170-9
up_date	2024-07-03T22:23:30.999Z
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fullrecord_marcxml	<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR013824783</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20220111003815.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">201006s2006 xx \|\|\|\|\|o 00\| \|\|eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10853-006-1170-9</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR013824783</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s10853-006-1170-9-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">670</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">51.00</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Jin, Zhengwei</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2006</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Ordered and cubic mesoporous silica materials were synthesized by using poly(ethylene oxide-b-propylene oxide-b-ethylene oxide) triblock copolymer as template under a moderately acidic condition of 0.5 mol/l HCl solution. These mesoporous materials were characterized by Fourier transform (FT) IR spectroscopy, thermo-gravimetric analysis (TGA), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption–desorption measurements. The three-dimensional cage-like microporosity of the prepared mesoporous silica having ordered hexagonal mesoporous structure was evidenced by the well-defined XRD patterns combined with TEM photographs. SEM observation shows a highly regular cubic crystal structure for the prepared mesoporous silica. The size of these crystallites was maintained within the range between 4 and 6 μm, which is fairly important for the application to the stationary phase for separation. The nitrogen adsorption–desorption analysis reveals that the prepared mesoporous silica possesses a small pore diameter of 3.68 nm, a total surface area of 363.648 $ m^{2} $/g, a total pore volume of 0.379 $ cm^{3} $/g, and a pore-wall thickness of 6.63 nm. These features may lead to higher thermal and hydrothermal stability, excellent microporosity, and good connectivity. 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Synthesis and characterization of ordered and cubic mesoporous silica crystals under a moderately acidic condition

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