Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study
Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal duri...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Shi, Yaoqi [verfasserIn] Hu, Dongkang [verfasserIn] Xin, Zhong [verfasserIn] Zhao, Shicheng [verfasserIn] Zhou, Shuai [verfasserIn] Meng, Xing [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2016 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966, 51(2016), 10 vom: 08. Feb., Seite 4880-4887 |
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| Übergeordnetes Werk: |
volume:51 ; year:2016 ; number:10 ; day:08 ; month:02 ; pages:4880-4887 |
| Links: |
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| DOI / URN: |
10.1007/s10853-016-9793-y |
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| Katalog-ID: |
SPR013909738 |
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| 245 | 1 | 0 | |a Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study |
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| 520 | |a Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. | ||
| 650 | 4 | |a PLLA |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Isothermal Crystallization |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Interchain Interaction |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Neat PLLA |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a PLLA Film |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Hu, Dongkang |e verfasserin |4 aut | |
| 700 | 1 | |a Xin, Zhong |e verfasserin |4 aut | |
| 700 | 1 | |a Zhao, Shicheng |e verfasserin |4 aut | |
| 700 | 1 | |a Zhou, Shuai |e verfasserin |4 aut | |
| 700 | 1 | |a Meng, Xing |e verfasserin |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Journal of materials science |d Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 |g 51(2016), 10 vom: 08. Feb., Seite 4880-4887 |w (DE-627)315293969 |w (DE-600)2015305-3 |x 1573-4803 |7 nnns |
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10.1007/s10853-016-9793-y doi (DE-627)SPR013909738 (SPR)s10853-016-9793-y-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Shi, Yaoqi verfasserin aut Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. PLLA (dpeaa)DE-He213 Isothermal Crystallization (dpeaa)DE-He213 Interchain Interaction (dpeaa)DE-He213 Neat PLLA (dpeaa)DE-He213 PLLA Film (dpeaa)DE-He213 Hu, Dongkang verfasserin aut Xin, Zhong verfasserin aut Zhao, Shicheng verfasserin aut Zhou, Shuai verfasserin aut Meng, Xing verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 51(2016), 10 vom: 08. Feb., Seite 4880-4887 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:51 year:2016 number:10 day:08 month:02 pages:4880-4887 https://dx.doi.org/10.1007/s10853-016-9793-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 51 2016 10 08 02 4880-4887 |
| spelling |
10.1007/s10853-016-9793-y doi (DE-627)SPR013909738 (SPR)s10853-016-9793-y-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Shi, Yaoqi verfasserin aut Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. PLLA (dpeaa)DE-He213 Isothermal Crystallization (dpeaa)DE-He213 Interchain Interaction (dpeaa)DE-He213 Neat PLLA (dpeaa)DE-He213 PLLA Film (dpeaa)DE-He213 Hu, Dongkang verfasserin aut Xin, Zhong verfasserin aut Zhao, Shicheng verfasserin aut Zhou, Shuai verfasserin aut Meng, Xing verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 51(2016), 10 vom: 08. Feb., Seite 4880-4887 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:51 year:2016 number:10 day:08 month:02 pages:4880-4887 https://dx.doi.org/10.1007/s10853-016-9793-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 51 2016 10 08 02 4880-4887 |
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10.1007/s10853-016-9793-y doi (DE-627)SPR013909738 (SPR)s10853-016-9793-y-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Shi, Yaoqi verfasserin aut Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. PLLA (dpeaa)DE-He213 Isothermal Crystallization (dpeaa)DE-He213 Interchain Interaction (dpeaa)DE-He213 Neat PLLA (dpeaa)DE-He213 PLLA Film (dpeaa)DE-He213 Hu, Dongkang verfasserin aut Xin, Zhong verfasserin aut Zhao, Shicheng verfasserin aut Zhou, Shuai verfasserin aut Meng, Xing verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 51(2016), 10 vom: 08. Feb., Seite 4880-4887 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:51 year:2016 number:10 day:08 month:02 pages:4880-4887 https://dx.doi.org/10.1007/s10853-016-9793-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 51 2016 10 08 02 4880-4887 |
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10.1007/s10853-016-9793-y doi (DE-627)SPR013909738 (SPR)s10853-016-9793-y-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Shi, Yaoqi verfasserin aut Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. PLLA (dpeaa)DE-He213 Isothermal Crystallization (dpeaa)DE-He213 Interchain Interaction (dpeaa)DE-He213 Neat PLLA (dpeaa)DE-He213 PLLA Film (dpeaa)DE-He213 Hu, Dongkang verfasserin aut Xin, Zhong verfasserin aut Zhao, Shicheng verfasserin aut Zhou, Shuai verfasserin aut Meng, Xing verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 51(2016), 10 vom: 08. Feb., Seite 4880-4887 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:51 year:2016 number:10 day:08 month:02 pages:4880-4887 https://dx.doi.org/10.1007/s10853-016-9793-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 51 2016 10 08 02 4880-4887 |
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10.1007/s10853-016-9793-y doi (DE-627)SPR013909738 (SPR)s10853-016-9793-y-e DE-627 ger DE-627 rakwb eng 670 ASE 51.00 bkl Shi, Yaoqi verfasserin aut Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. PLLA (dpeaa)DE-He213 Isothermal Crystallization (dpeaa)DE-He213 Interchain Interaction (dpeaa)DE-He213 Neat PLLA (dpeaa)DE-He213 PLLA Film (dpeaa)DE-He213 Hu, Dongkang verfasserin aut Xin, Zhong verfasserin aut Zhao, Shicheng verfasserin aut Zhou, Shuai verfasserin aut Meng, Xing verfasserin aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1966 51(2016), 10 vom: 08. Feb., Seite 4880-4887 (DE-627)315293969 (DE-600)2015305-3 1573-4803 nnns volume:51 year:2016 number:10 day:08 month:02 pages:4880-4887 https://dx.doi.org/10.1007/s10853-016-9793-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 51 2016 10 08 02 4880-4887 |
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Enthalten in Journal of materials science 51(2016), 10 vom: 08. Feb., Seite 4880-4887 volume:51 year:2016 number:10 day:08 month:02 pages:4880-4887 |
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PLLA Isothermal Crystallization Interchain Interaction Neat PLLA PLLA Film |
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Journal of materials science |
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Shi, Yaoqi @@aut@@ Hu, Dongkang @@aut@@ Xin, Zhong @@aut@@ Zhao, Shicheng @@aut@@ Zhou, Shuai @@aut@@ Meng, Xing @@aut@@ |
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2016-02-08T00:00:00Z |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR013909738</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20220111004129.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">201006s2016 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10853-016-9793-y</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR013909738</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s10853-016-9793-y-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">670</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">51.00</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Shi, Yaoqi</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2016</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. 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Shi, Yaoqi |
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Shi, Yaoqi ddc 670 bkl 51.00 misc PLLA misc Isothermal Crystallization misc Interchain Interaction misc Neat PLLA misc PLLA Film Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study |
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670 ASE 51.00 bkl Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study PLLA (dpeaa)DE-He213 Isothermal Crystallization (dpeaa)DE-He213 Interchain Interaction (dpeaa)DE-He213 Neat PLLA (dpeaa)DE-He213 PLLA Film (dpeaa)DE-He213 |
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Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study |
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Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study |
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Shi, Yaoqi Hu, Dongkang Xin, Zhong Zhao, Shicheng Zhou, Shuai Meng, Xing |
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conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study |
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Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study |
| abstract |
Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. |
| abstractGer |
Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. |
| abstract_unstemmed |
Abstract Chain conformation order of poly (l-lactic acid) (PLLA) was investigated by time-lapsed Fourier transform infrared (FTIR) spectroscopy and two-dimensional infrared correlation spectroscopy during the isothermal crystallization at 140 °C. The result showed that the PLLA formed α-crystal during the isothermal crystallization at 140 °C. According to the detailed information in the region of 1000–1500 $ cm^{−1} $ investigated by infrared and 2D correlation spectroscopy, it was found that the conformation of C–O–C groups changed prior to that of $ CH_{3} $ groups. Moreover, the formation of the initial helix chain conformation was interfered by the interchain interactions between the $ CH_{3} $ groups, which consequently resulted in the formation of α-crystal with the distorted $ 10_{3} $ helix conformation. |
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| container_issue |
10 |
| title_short |
Conformation order of poly(l-lactic acid) chains during the melt crystallization process: infrared and two-dimensional infrared correlation spectroscopy study |
| url |
https://dx.doi.org/10.1007/s10853-016-9793-y |
| remote_bool |
true |
| author2 |
Hu, Dongkang Xin, Zhong Zhao, Shicheng Zhou, Shuai Meng, Xing |
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Hu, Dongkang Xin, Zhong Zhao, Shicheng Zhou, Shuai Meng, Xing |
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| doi_str |
10.1007/s10853-016-9793-y |
| up_date |
2024-07-03T22:57:10.294Z |
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| score |
7.4010115 |