Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2
Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for e...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Tiekink, Edward R. T. [verfasserIn] Wardell, James L. [verfasserIn] Wardell, Solange M. S. V. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2007 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of chemical crystallography - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1971, 37(2007), 7 vom: 04. Apr., Seite 439-443 |
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| Übergeordnetes Werk: |
volume:37 ; year:2007 ; number:7 ; day:04 ; month:04 ; pages:439-443 |
| Links: |
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| DOI / URN: |
10.1007/s10870-007-9189-6 |
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| Katalog-ID: |
SPR014203065 |
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| 082 | 0 | 4 | |a 540 |q ASE |
| 084 | |a 35.25 |2 bkl | ||
| 084 | |a 35.90 |2 bkl | ||
| 084 | |a 38.31 |2 bkl | ||
| 084 | |a 51.00 |2 bkl | ||
| 100 | 1 | |a Tiekink, Edward R. T. |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 |
| 264 | 1 | |c 2007 | |
| 336 | |a Text |b txt |2 rdacontent | ||
| 337 | |a Computermedien |b c |2 rdamedia | ||
| 338 | |a Online-Ressource |b cr |2 rdacarrier | ||
| 520 | |a Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. | ||
| 650 | 4 | |a Nickel |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Dithiocarbamate |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Metal complex |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Hydrogen-bonding |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Wardell, James L. |e verfasserin |4 aut | |
| 700 | 1 | |a Wardell, Solange M. S. V. |e verfasserin |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Journal of chemical crystallography |d Dordrecht [u.a.] : Springer Science + Business Media B.V, 1971 |g 37(2007), 7 vom: 04. Apr., Seite 439-443 |w (DE-627)302467270 |w (DE-600)1491232-6 |x 1572-8854 |7 nnns |
| 773 | 1 | 8 | |g volume:37 |g year:2007 |g number:7 |g day:04 |g month:04 |g pages:439-443 |
| 856 | 4 | 0 | |u https://dx.doi.org/10.1007/s10870-007-9189-6 |z lizenzpflichtig |3 Volltext |
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| 912 | |a GBV_ILN_2107 | ||
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| 912 | |a GBV_ILN_2116 | ||
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| 936 | b | k | |a 35.25 |q ASE |
| 936 | b | k | |a 35.90 |q ASE |
| 936 | b | k | |a 38.31 |q ASE |
| 936 | b | k | |a 51.00 |q ASE |
| 951 | |a AR | ||
| 952 | |d 37 |j 2007 |e 7 |b 04 |c 04 |h 439-443 | ||
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2007 |
| bklnumber |
35.25 35.90 38.31 51.00 |
| publishDate |
2007 |
| allfields |
10.1007/s10870-007-9189-6 doi (DE-627)SPR014203065 (SPR)s10870-007-9189-6-e DE-627 ger DE-627 rakwb eng 540 ASE 35.25 bkl 35.90 bkl 38.31 bkl 51.00 bkl Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 2007 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel (dpeaa)DE-He213 Dithiocarbamate (dpeaa)DE-He213 Metal complex (dpeaa)DE-He213 Hydrogen-bonding (dpeaa)DE-He213 Wardell, James L. verfasserin aut Wardell, Solange M. S. V. verfasserin aut Enthalten in Journal of chemical crystallography Dordrecht [u.a.] : Springer Science + Business Media B.V, 1971 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)302467270 (DE-600)1491232-6 1572-8854 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://dx.doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA SSG-OPC-GGO SSG-OPC-ASE GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.25 ASE 35.90 ASE 38.31 ASE 51.00 ASE AR 37 2007 7 04 04 439-443 |
| spelling |
10.1007/s10870-007-9189-6 doi (DE-627)SPR014203065 (SPR)s10870-007-9189-6-e DE-627 ger DE-627 rakwb eng 540 ASE 35.25 bkl 35.90 bkl 38.31 bkl 51.00 bkl Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 2007 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel (dpeaa)DE-He213 Dithiocarbamate (dpeaa)DE-He213 Metal complex (dpeaa)DE-He213 Hydrogen-bonding (dpeaa)DE-He213 Wardell, James L. verfasserin aut Wardell, Solange M. S. V. verfasserin aut Enthalten in Journal of chemical crystallography Dordrecht [u.a.] : Springer Science + Business Media B.V, 1971 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)302467270 (DE-600)1491232-6 1572-8854 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://dx.doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA SSG-OPC-GGO SSG-OPC-ASE GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.25 ASE 35.90 ASE 38.31 ASE 51.00 ASE AR 37 2007 7 04 04 439-443 |
| allfields_unstemmed |
10.1007/s10870-007-9189-6 doi (DE-627)SPR014203065 (SPR)s10870-007-9189-6-e DE-627 ger DE-627 rakwb eng 540 ASE 35.25 bkl 35.90 bkl 38.31 bkl 51.00 bkl Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 2007 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel (dpeaa)DE-He213 Dithiocarbamate (dpeaa)DE-He213 Metal complex (dpeaa)DE-He213 Hydrogen-bonding (dpeaa)DE-He213 Wardell, James L. verfasserin aut Wardell, Solange M. S. V. verfasserin aut Enthalten in Journal of chemical crystallography Dordrecht [u.a.] : Springer Science + Business Media B.V, 1971 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)302467270 (DE-600)1491232-6 1572-8854 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://dx.doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA SSG-OPC-GGO SSG-OPC-ASE GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.25 ASE 35.90 ASE 38.31 ASE 51.00 ASE AR 37 2007 7 04 04 439-443 |
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10.1007/s10870-007-9189-6 doi (DE-627)SPR014203065 (SPR)s10870-007-9189-6-e DE-627 ger DE-627 rakwb eng 540 ASE 35.25 bkl 35.90 bkl 38.31 bkl 51.00 bkl Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 2007 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel (dpeaa)DE-He213 Dithiocarbamate (dpeaa)DE-He213 Metal complex (dpeaa)DE-He213 Hydrogen-bonding (dpeaa)DE-He213 Wardell, James L. verfasserin aut Wardell, Solange M. S. V. verfasserin aut Enthalten in Journal of chemical crystallography Dordrecht [u.a.] : Springer Science + Business Media B.V, 1971 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)302467270 (DE-600)1491232-6 1572-8854 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://dx.doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA SSG-OPC-GGO SSG-OPC-ASE GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.25 ASE 35.90 ASE 38.31 ASE 51.00 ASE AR 37 2007 7 04 04 439-443 |
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10.1007/s10870-007-9189-6 doi (DE-627)SPR014203065 (SPR)s10870-007-9189-6-e DE-627 ger DE-627 rakwb eng 540 ASE 35.25 bkl 35.90 bkl 38.31 bkl 51.00 bkl Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 2007 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel (dpeaa)DE-He213 Dithiocarbamate (dpeaa)DE-He213 Metal complex (dpeaa)DE-He213 Hydrogen-bonding (dpeaa)DE-He213 Wardell, James L. verfasserin aut Wardell, Solange M. S. V. verfasserin aut Enthalten in Journal of chemical crystallography Dordrecht [u.a.] : Springer Science + Business Media B.V, 1971 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)302467270 (DE-600)1491232-6 1572-8854 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://dx.doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA SSG-OPC-GGO SSG-OPC-ASE GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.25 ASE 35.90 ASE 38.31 ASE 51.00 ASE AR 37 2007 7 04 04 439-443 |
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English |
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Enthalten in Journal of chemical crystallography 37(2007), 7 vom: 04. Apr., Seite 439-443 volume:37 year:2007 number:7 day:04 month:04 pages:439-443 |
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Enthalten in Journal of chemical crystallography 37(2007), 7 vom: 04. Apr., Seite 439-443 volume:37 year:2007 number:7 day:04 month:04 pages:439-443 |
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Nickel Dithiocarbamate Metal complex Hydrogen-bonding |
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Journal of chemical crystallography |
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Tiekink, Edward R. T. @@aut@@ Wardell, James L. @@aut@@ Wardell, Solange M. S. V. @@aut@@ |
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T.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2007</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Nickel</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Dithiocarbamate</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Metal complex</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Hydrogen-bonding</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wardell, James L.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wardell, Solange M. 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|
| author |
Tiekink, Edward R. T. |
| spellingShingle |
Tiekink, Edward R. T. ddc 540 bkl 35.25 bkl 35.90 bkl 38.31 bkl 51.00 misc Nickel misc Dithiocarbamate misc Metal complex misc Hydrogen-bonding Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 |
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540 - Chemistry & allied sciences |
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1572-8854 |
| topic_title |
540 ASE 35.25 bkl 35.90 bkl 38.31 bkl 51.00 bkl Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 Nickel (dpeaa)DE-He213 Dithiocarbamate (dpeaa)DE-He213 Metal complex (dpeaa)DE-He213 Hydrogen-bonding (dpeaa)DE-He213 |
| topic |
ddc 540 bkl 35.25 bkl 35.90 bkl 38.31 bkl 51.00 misc Nickel misc Dithiocarbamate misc Metal complex misc Hydrogen-bonding |
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ddc 540 bkl 35.25 bkl 35.90 bkl 38.31 bkl 51.00 misc Nickel misc Dithiocarbamate misc Metal complex misc Hydrogen-bonding |
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ddc 540 bkl 35.25 bkl 35.90 bkl 38.31 bkl 51.00 misc Nickel misc Dithiocarbamate misc Metal complex misc Hydrogen-bonding |
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| title |
Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 |
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(DE-627)SPR014203065 (SPR)s10870-007-9189-6-e |
| title_full |
Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 |
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Tiekink, Edward R. T. |
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Journal of chemical crystallography |
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Journal of chemical crystallography |
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eng |
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2007 |
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Tiekink, Edward R. T. Wardell, James L. Wardell, Solange M. S. V. |
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37 |
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540 ASE 35.25 bkl 35.90 bkl 38.31 bkl 51.00 bkl |
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Elektronische Aufsätze |
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Tiekink, Edward R. T. |
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10.1007/s10870-007-9189-6 |
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540 |
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verfasserin |
| title_sort |
hydrogen-bonding interactions in the crystal structure of bis(n-propyl-n-(2-hydroxyethyl)dithiocarbamato-s,s′)nickel(ii): ni[$ s_{2} $cn(npr)($ ch_{2} %$ ch_{2} $oh)]2 |
| title_auth |
Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 |
| abstract |
Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. |
| abstractGer |
Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. |
| abstract_unstemmed |
Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} %$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. |
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7 |
| title_short |
Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} %$ CH_{2} $OH)]2 |
| url |
https://dx.doi.org/10.1007/s10870-007-9189-6 |
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| author2 |
Wardell, James L. Wardell, Solange M. S. V. |
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Wardell, James L. Wardell, Solange M. S. V. |
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| doi_str |
10.1007/s10870-007-9189-6 |
| up_date |
2024-07-04T00:36:34.931Z |
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1803606708647362560 |
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| score |
7.4010057 |