Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization

Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk a...
Ausführliche Beschreibung

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Autor*in:	Gupta, Rainy [verfasserIn] Bhardwaj, Pooja [verfasserIn] Mishra, Deepti [verfasserIn] Prasad, Murari [verfasserIn] Amritphale, S. S. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2016

Schlagwörter:	Mechanochemically Solution chemistry Solid state route Geopolymerization

Übergeordnetes Werk:	Enthalten in: Journal of inorganic and organometallic polymers and materials - Dordrecht [u.a.] : Springer Science + Business Media B.V., 1991, 27(2016), 2 vom: 15. Dez., Seite 385-398
Übergeordnetes Werk:	volume:27 ; year:2016 ; number:2 ; day:15 ; month:12 ; pages:385-398

Links:	Volltext

DOI / URN:	10.1007/s10904-016-0461-0

Katalog-ID:	SPR014850060

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520			\|a Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement.
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matchkey_str	article:15741451:2016----::omltoomcaohmclyvlefysbsdyrdnraiognceplmr
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allfields	10.1007/s10904-016-0461-0 doi (DE-627)SPR014850060 (SPR)s10904-016-0461-0-e DE-627 ger DE-627 rakwb eng 660 ASE 35.80 bkl 51.70 bkl Gupta, Rainy verfasserin aut Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement. Mechanochemically (dpeaa)DE-He213 Solution chemistry (dpeaa)DE-He213 Solid state route (dpeaa)DE-He213 Geopolymerization (dpeaa)DE-He213 Bhardwaj, Pooja verfasserin aut Mishra, Deepti verfasserin aut Prasad, Murari verfasserin aut Amritphale, S. S. verfasserin aut Enthalten in Journal of inorganic and organometallic polymers and materials Dordrecht [u.a.] : Springer Science + Business Media B.V., 1991 27(2016), 2 vom: 15. Dez., Seite 385-398 (DE-627)320575101 (DE-600)2016951-6 1574-1451 nnns volume:27 year:2016 number:2 day:15 month:12 pages:385-398 https://dx.doi.org/10.1007/s10904-016-0461-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.80 ASE 51.70 ASE AR 27 2016 2 15 12 385-398
spelling	10.1007/s10904-016-0461-0 doi (DE-627)SPR014850060 (SPR)s10904-016-0461-0-e DE-627 ger DE-627 rakwb eng 660 ASE 35.80 bkl 51.70 bkl Gupta, Rainy verfasserin aut Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement. Mechanochemically (dpeaa)DE-He213 Solution chemistry (dpeaa)DE-He213 Solid state route (dpeaa)DE-He213 Geopolymerization (dpeaa)DE-He213 Bhardwaj, Pooja verfasserin aut Mishra, Deepti verfasserin aut Prasad, Murari verfasserin aut Amritphale, S. S. verfasserin aut Enthalten in Journal of inorganic and organometallic polymers and materials Dordrecht [u.a.] : Springer Science + Business Media B.V., 1991 27(2016), 2 vom: 15. Dez., Seite 385-398 (DE-627)320575101 (DE-600)2016951-6 1574-1451 nnns volume:27 year:2016 number:2 day:15 month:12 pages:385-398 https://dx.doi.org/10.1007/s10904-016-0461-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.80 ASE 51.70 ASE AR 27 2016 2 15 12 385-398
allfields_unstemmed	10.1007/s10904-016-0461-0 doi (DE-627)SPR014850060 (SPR)s10904-016-0461-0-e DE-627 ger DE-627 rakwb eng 660 ASE 35.80 bkl 51.70 bkl Gupta, Rainy verfasserin aut Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement. Mechanochemically (dpeaa)DE-He213 Solution chemistry (dpeaa)DE-He213 Solid state route (dpeaa)DE-He213 Geopolymerization (dpeaa)DE-He213 Bhardwaj, Pooja verfasserin aut Mishra, Deepti verfasserin aut Prasad, Murari verfasserin aut Amritphale, S. S. verfasserin aut Enthalten in Journal of inorganic and organometallic polymers and materials Dordrecht [u.a.] : Springer Science + Business Media B.V., 1991 27(2016), 2 vom: 15. Dez., Seite 385-398 (DE-627)320575101 (DE-600)2016951-6 1574-1451 nnns volume:27 year:2016 number:2 day:15 month:12 pages:385-398 https://dx.doi.org/10.1007/s10904-016-0461-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.80 ASE 51.70 ASE AR 27 2016 2 15 12 385-398
allfieldsGer	10.1007/s10904-016-0461-0 doi (DE-627)SPR014850060 (SPR)s10904-016-0461-0-e DE-627 ger DE-627 rakwb eng 660 ASE 35.80 bkl 51.70 bkl Gupta, Rainy verfasserin aut Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement. Mechanochemically (dpeaa)DE-He213 Solution chemistry (dpeaa)DE-He213 Solid state route (dpeaa)DE-He213 Geopolymerization (dpeaa)DE-He213 Bhardwaj, Pooja verfasserin aut Mishra, Deepti verfasserin aut Prasad, Murari verfasserin aut Amritphale, S. S. verfasserin aut Enthalten in Journal of inorganic and organometallic polymers and materials Dordrecht [u.a.] : Springer Science + Business Media B.V., 1991 27(2016), 2 vom: 15. Dez., Seite 385-398 (DE-627)320575101 (DE-600)2016951-6 1574-1451 nnns volume:27 year:2016 number:2 day:15 month:12 pages:385-398 https://dx.doi.org/10.1007/s10904-016-0461-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.80 ASE 51.70 ASE AR 27 2016 2 15 12 385-398
allfieldsSound	10.1007/s10904-016-0461-0 doi (DE-627)SPR014850060 (SPR)s10904-016-0461-0-e DE-627 ger DE-627 rakwb eng 660 ASE 35.80 bkl 51.70 bkl Gupta, Rainy verfasserin aut Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement. Mechanochemically (dpeaa)DE-He213 Solution chemistry (dpeaa)DE-He213 Solid state route (dpeaa)DE-He213 Geopolymerization (dpeaa)DE-He213 Bhardwaj, Pooja verfasserin aut Mishra, Deepti verfasserin aut Prasad, Murari verfasserin aut Amritphale, S. S. verfasserin aut Enthalten in Journal of inorganic and organometallic polymers and materials Dordrecht [u.a.] : Springer Science + Business Media B.V., 1991 27(2016), 2 vom: 15. Dez., Seite 385-398 (DE-627)320575101 (DE-600)2016951-6 1574-1451 nnns volume:27 year:2016 number:2 day:15 month:12 pages:385-398 https://dx.doi.org/10.1007/s10904-016-0461-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.80 ASE 51.70 ASE AR 27 2016 2 15 12 385-398
language	English
source	Enthalten in Journal of inorganic and organometallic polymers and materials 27(2016), 2 vom: 15. Dez., Seite 385-398 volume:27 year:2016 number:2 day:15 month:12 pages:385-398
sourceStr	Enthalten in Journal of inorganic and organometallic polymers and materials 27(2016), 2 vom: 15. Dez., Seite 385-398 volume:27 year:2016 number:2 day:15 month:12 pages:385-398
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Mechanochemically Solution chemistry Solid state route Geopolymerization
dewey-raw	660
isfreeaccess_bool	false
container_title	Journal of inorganic and organometallic polymers and materials
authorswithroles_txt_mv	Gupta, Rainy @@aut@@ Bhardwaj, Pooja @@aut@@ Mishra, Deepti @@aut@@ Prasad, Murari @@aut@@ Amritphale, S. S. @@aut@@
publishDateDaySort_date	2016-12-15T00:00:00Z
hierarchy_top_id	320575101
dewey-sort	3660
id	SPR014850060
language_de	englisch
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author	Gupta, Rainy
spellingShingle	Gupta, Rainy ddc 660 bkl 35.80 bkl 51.70 misc Mechanochemically misc Solution chemistry misc Solid state route misc Geopolymerization Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization
authorStr	Gupta, Rainy
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topic_title	660 ASE 35.80 bkl 51.70 bkl Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization Mechanochemically (dpeaa)DE-He213 Solution chemistry (dpeaa)DE-He213 Solid state route (dpeaa)DE-He213 Geopolymerization (dpeaa)DE-He213
topic	ddc 660 bkl 35.80 bkl 51.70 misc Mechanochemically misc Solution chemistry misc Solid state route misc Geopolymerization
topic_unstemmed	ddc 660 bkl 35.80 bkl 51.70 misc Mechanochemically misc Solution chemistry misc Solid state route misc Geopolymerization
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title	Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization
ctrlnum	(DE-627)SPR014850060 (SPR)s10904-016-0461-0-e
title_full	Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization
author_sort	Gupta, Rainy
journal	Journal of inorganic and organometallic polymers and materials
journalStr	Journal of inorganic and organometallic polymers and materials
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author_browse	Gupta, Rainy Bhardwaj, Pooja Mishra, Deepti Prasad, Murari Amritphale, S. S.
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author-letter	Gupta, Rainy
doi_str_mv	10.1007/s10904-016-0461-0
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title_sort	formulation of mechanochemically evolved fly ash based hybrid inorganic–organic geopolymers with multilevel characterization
title_auth	Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization
abstract	Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement.
abstractGer	Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement.
abstract_unstemmed	Abstract In this research, advanced hybrid inorganic–organic geopolymeric material is developed by environmentally and user friendlier approach. The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. XRD, FTIR and SEM characterization data of developed geopolymeric precursor powder and hybrid inorganic–organic geopolymeric material are reported and discussed in detail. As the results of the investigations, the relationship between geopolymer composition, grinding mechanism and material properties established. The composition which exhibited synergistic effect of both rice husk and SMS is found to be excellent in performance. The study showed that it is practical and better to adopt this greener solid state approach for preparation of geopolymer instead of user-unfriendlier hazardous alkaline solution based approach, to achieve sustainable growth in geopolymers as like Portland cement.
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title_short	Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization
url	https://dx.doi.org/10.1007/s10904-016-0461-0
remote_bool	true
author2	Bhardwaj, Pooja Mishra, Deepti Prasad, Murari Amritphale, S. S.
author2Str	Bhardwaj, Pooja Mishra, Deepti Prasad, Murari Amritphale, S. S.
ppnlink	320575101
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doi_str	10.1007/s10904-016-0461-0
up_date	2024-07-04T03:16:16.246Z
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The presented novel approach for geopolymer formation certainly overcomes the existing drawbacks of geopolymerization technology. The effect of rice husk ash and $ Na_{2} $O/$ SiO_{2} $ ratios on geopolymer gel formation and mechanical strength has been previously identified via solution chemistry route; however, development of geopolymeric material having hybrid inorganic–organic characters via together mechanochemical grinding of raw materials and effect of mechanochemically activated $ Na_{2} %$ SiO_{3} $ on geopolymeric properties via solid state route has never before been explored. Together mechanochemical grinding of raw materials of varying compositions in solid state resulted in the formation of ready to use geopolymeric precursors; which on just addition of water led to development of advanced hybrid inorganic–organic geopolymeric material with considerably enhanced properties. 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Formulation of Mechanochemically Evolved Fly Ash Based Hybrid Inorganic–Organic Geopolymers with Multilevel Characterization

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