Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors
Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen...
Ausführliche Beschreibung
Autor*in: |
Singh, Kiran [verfasserIn] Mohan, Rajneesh [verfasserIn] Rayaprol, Sudhindra [verfasserIn] Dogra, Anjana [verfasserIn] Prajapat, C. L. [verfasserIn] Bhattacharya, Shovit [verfasserIn] Gaur, N. K. [verfasserIn] Singh, R. K. [verfasserIn] |
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Sprache: |
Englisch |
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2009 |
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Übergeordnetes Werk: |
Enthalten in: Journal of superconductivity - Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988, 22(2009), 7 vom: 02. Mai, Seite 699-704 |
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Übergeordnetes Werk: |
volume:22 ; year:2009 ; number:7 ; day:02 ; month:05 ; pages:699-704 |
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DOI / URN: |
10.1007/s10948-009-0482-9 |
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SPR014866528 |
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520 | |a Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. | ||
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10.1007/s10948-009-0482-9 doi (DE-627)SPR014866528 (SPR)s10948-009-0482-9-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Singh, Kiran verfasserin aut Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. Cuprate superconductors (dpeaa)DE-He213 Hole doping (dpeaa)DE-He213 AgO and HgO addition (dpeaa)DE-He213 Mohan, Rajneesh verfasserin aut Rayaprol, Sudhindra verfasserin aut Dogra, Anjana verfasserin aut Prajapat, C. L. verfasserin aut Bhattacharya, Shovit verfasserin aut Gaur, N. K. verfasserin aut Singh, R. K. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 22(2009), 7 vom: 02. Mai, Seite 699-704 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:22 year:2009 number:7 day:02 month:05 pages:699-704 https://dx.doi.org/10.1007/s10948-009-0482-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 22 2009 7 02 05 699-704 |
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10.1007/s10948-009-0482-9 doi (DE-627)SPR014866528 (SPR)s10948-009-0482-9-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Singh, Kiran verfasserin aut Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. Cuprate superconductors (dpeaa)DE-He213 Hole doping (dpeaa)DE-He213 AgO and HgO addition (dpeaa)DE-He213 Mohan, Rajneesh verfasserin aut Rayaprol, Sudhindra verfasserin aut Dogra, Anjana verfasserin aut Prajapat, C. L. verfasserin aut Bhattacharya, Shovit verfasserin aut Gaur, N. K. verfasserin aut Singh, R. K. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 22(2009), 7 vom: 02. Mai, Seite 699-704 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:22 year:2009 number:7 day:02 month:05 pages:699-704 https://dx.doi.org/10.1007/s10948-009-0482-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 22 2009 7 02 05 699-704 |
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10.1007/s10948-009-0482-9 doi (DE-627)SPR014866528 (SPR)s10948-009-0482-9-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Singh, Kiran verfasserin aut Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. Cuprate superconductors (dpeaa)DE-He213 Hole doping (dpeaa)DE-He213 AgO and HgO addition (dpeaa)DE-He213 Mohan, Rajneesh verfasserin aut Rayaprol, Sudhindra verfasserin aut Dogra, Anjana verfasserin aut Prajapat, C. L. verfasserin aut Bhattacharya, Shovit verfasserin aut Gaur, N. K. verfasserin aut Singh, R. K. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 22(2009), 7 vom: 02. Mai, Seite 699-704 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:22 year:2009 number:7 day:02 month:05 pages:699-704 https://dx.doi.org/10.1007/s10948-009-0482-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 22 2009 7 02 05 699-704 |
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10.1007/s10948-009-0482-9 doi (DE-627)SPR014866528 (SPR)s10948-009-0482-9-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Singh, Kiran verfasserin aut Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. Cuprate superconductors (dpeaa)DE-He213 Hole doping (dpeaa)DE-He213 AgO and HgO addition (dpeaa)DE-He213 Mohan, Rajneesh verfasserin aut Rayaprol, Sudhindra verfasserin aut Dogra, Anjana verfasserin aut Prajapat, C. L. verfasserin aut Bhattacharya, Shovit verfasserin aut Gaur, N. K. verfasserin aut Singh, R. K. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 22(2009), 7 vom: 02. Mai, Seite 699-704 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:22 year:2009 number:7 day:02 month:05 pages:699-704 https://dx.doi.org/10.1007/s10948-009-0482-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 22 2009 7 02 05 699-704 |
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10.1007/s10948-009-0482-9 doi (DE-627)SPR014866528 (SPR)s10948-009-0482-9-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Singh, Kiran verfasserin aut Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. Cuprate superconductors (dpeaa)DE-He213 Hole doping (dpeaa)DE-He213 AgO and HgO addition (dpeaa)DE-He213 Mohan, Rajneesh verfasserin aut Rayaprol, Sudhindra verfasserin aut Dogra, Anjana verfasserin aut Prajapat, C. L. verfasserin aut Bhattacharya, Shovit verfasserin aut Gaur, N. K. verfasserin aut Singh, R. K. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 22(2009), 7 vom: 02. Mai, Seite 699-704 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:22 year:2009 number:7 day:02 month:05 pages:699-704 https://dx.doi.org/10.1007/s10948-009-0482-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 22 2009 7 02 05 699-704 |
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Singh, Kiran @@aut@@ Mohan, Rajneesh @@aut@@ Rayaprol, Sudhindra @@aut@@ Dogra, Anjana @@aut@@ Prajapat, C. L. @@aut@@ Bhattacharya, Shovit @@aut@@ Gaur, N. K. @@aut@@ Singh, R. K. @@aut@@ |
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Singh, Kiran ddc 530 bkl 33.74 misc Cuprate superconductors misc Hole doping misc AgO and HgO addition Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors |
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530 ASE 33.74 bkl Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors Cuprate superconductors (dpeaa)DE-He213 Hole doping (dpeaa)DE-He213 AgO and HgO addition (dpeaa)DE-He213 |
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Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors |
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Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors |
abstract |
Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. |
abstractGer |
Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. |
abstract_unstemmed |
Abstract We have prepared a series of $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ (La2125) compounds by the standard solid-state reaction method. The oxygen stoichiometry in this R-123 type compound has been homogenized by two different methods. The first method is heating the sample in flowing oxygen at 500 °C for 6 hours and then slowly cooling to room temperature. The second method is to provide internal oxygen while sintering the sample by adding HgO or AgO. The addition of HgO or AgO in preparing oxide superconductors is advantageous when preparing them in bulk quantities, as HgO or AgO provide internal oxygen which is a much essential ingredient of the structure of oxide superconductors. Such a method of synthesis eliminates the need of additional oxygen annealing, thus enabling the synthesis in huge quantities at once. The composites referred to as La2125+xHgO and La2125+xAgO respectively, have been characterized by XRD, SEM, resistivity and magnetic measurements for their structural and superconducting properties. We compare the properties of oxygen-annealed and HgO/AgO added compounds and discuss the results in the light of applicability of such method in synthesizing bulk quantities of high-Tc oxide superconductors. |
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Preparation and Characterization of HgO and AgO Added $ La_{2} %$ CaBa_{2} %$ Cu_{5} %$ O_{z} $ Superconductors |
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