Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method
Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This pap...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Pavan Kumar Naik, S. [verfasserIn] Santosh, M. [verfasserIn] Swarup Raju, P. M. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2017 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of superconductivity - Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988, 31(2017), 5 vom: 01. Sept., Seite 1279-1286 |
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| Übergeordnetes Werk: |
volume:31 ; year:2017 ; number:5 ; day:01 ; month:09 ; pages:1279-1286 |
| Links: |
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| DOI / URN: |
10.1007/s10948-017-4306-z |
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| 520 | |a Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. | ||
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10.1007/s10948-017-4306-z doi (DE-627)SPR014910152 (SPR)s10948-017-4306-z-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Pavan Kumar Naik, S. verfasserin aut Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. Y (dpeaa)DE-He213 Ba (dpeaa)DE-He213 Cu (dpeaa)DE-He213 O (dpeaa)DE-He213 Rietveld refinement (dpeaa)DE-He213 TG-DTA (dpeaa)DE-He213 Santosh, M. verfasserin aut Swarup Raju, P. M. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 31(2017), 5 vom: 01. Sept., Seite 1279-1286 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:31 year:2017 number:5 day:01 month:09 pages:1279-1286 https://dx.doi.org/10.1007/s10948-017-4306-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 31 2017 5 01 09 1279-1286 |
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10.1007/s10948-017-4306-z doi (DE-627)SPR014910152 (SPR)s10948-017-4306-z-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Pavan Kumar Naik, S. verfasserin aut Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. Y (dpeaa)DE-He213 Ba (dpeaa)DE-He213 Cu (dpeaa)DE-He213 O (dpeaa)DE-He213 Rietveld refinement (dpeaa)DE-He213 TG-DTA (dpeaa)DE-He213 Santosh, M. verfasserin aut Swarup Raju, P. M. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 31(2017), 5 vom: 01. Sept., Seite 1279-1286 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:31 year:2017 number:5 day:01 month:09 pages:1279-1286 https://dx.doi.org/10.1007/s10948-017-4306-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 31 2017 5 01 09 1279-1286 |
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10.1007/s10948-017-4306-z doi (DE-627)SPR014910152 (SPR)s10948-017-4306-z-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Pavan Kumar Naik, S. verfasserin aut Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. Y (dpeaa)DE-He213 Ba (dpeaa)DE-He213 Cu (dpeaa)DE-He213 O (dpeaa)DE-He213 Rietveld refinement (dpeaa)DE-He213 TG-DTA (dpeaa)DE-He213 Santosh, M. verfasserin aut Swarup Raju, P. M. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 31(2017), 5 vom: 01. Sept., Seite 1279-1286 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:31 year:2017 number:5 day:01 month:09 pages:1279-1286 https://dx.doi.org/10.1007/s10948-017-4306-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 31 2017 5 01 09 1279-1286 |
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10.1007/s10948-017-4306-z doi (DE-627)SPR014910152 (SPR)s10948-017-4306-z-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Pavan Kumar Naik, S. verfasserin aut Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. Y (dpeaa)DE-He213 Ba (dpeaa)DE-He213 Cu (dpeaa)DE-He213 O (dpeaa)DE-He213 Rietveld refinement (dpeaa)DE-He213 TG-DTA (dpeaa)DE-He213 Santosh, M. verfasserin aut Swarup Raju, P. M. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 31(2017), 5 vom: 01. Sept., Seite 1279-1286 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:31 year:2017 number:5 day:01 month:09 pages:1279-1286 https://dx.doi.org/10.1007/s10948-017-4306-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 31 2017 5 01 09 1279-1286 |
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10.1007/s10948-017-4306-z doi (DE-627)SPR014910152 (SPR)s10948-017-4306-z-e DE-627 ger DE-627 rakwb eng 530 ASE 33.74 bkl Pavan Kumar Naik, S. verfasserin aut Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. Y (dpeaa)DE-He213 Ba (dpeaa)DE-He213 Cu (dpeaa)DE-He213 O (dpeaa)DE-He213 Rietveld refinement (dpeaa)DE-He213 TG-DTA (dpeaa)DE-He213 Santosh, M. verfasserin aut Swarup Raju, P. M. verfasserin aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 31(2017), 5 vom: 01. Sept., Seite 1279-1286 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:31 year:2017 number:5 day:01 month:09 pages:1279-1286 https://dx.doi.org/10.1007/s10948-017-4306-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 33.74 ASE AR 31 2017 5 01 09 1279-1286 |
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Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. 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Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method |
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structural and thermal validations of $ y_{3} %$ ba_{5} %$ cu_{8} %$ o_{18} $ composites synthesized via citrate sol-gel spontaneous combustion method |
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Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method |
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Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. |
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Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. |
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Abstract The fabrication of single-phase superconductors enabled promising advancements in a wide range of technological applications. Numerous parameters including processing temperature, thermal cycle, chemical composition, doping, and atmosphere will be carefully addressed and optimized. This paper investigates phase stability and compound formation of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{y} $ (Y-358) preform powders which were sintered at different temperatures. The precursor powder synthesized via chemical route and employing spontaneous combustion technique, respectively. The presence of Y-358 and $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (Y-123) phases in composites sintered at different temperatures with varied phase fractions were further confirmed through Rietveld refinement. The formation of Y-123 phase is dominant in all samples and composite was sintered at 900 °C, which was exhibited higher as compared to Y-358 phase content. The decomposition of different phases present in the composites and reaction temperatures were investigated with simultaneous differential thermal and thermogravimetry analysis. |
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Structural and Thermal Validations of $ Y_{3} %$ Ba_{5} %$ Cu_{8} %$ O_{18} $ Composites Synthesized via Citrate Sol-Gel Spontaneous Combustion Method |
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