Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system
Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of p...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Karthikeyan, S. [verfasserIn] Sikkanthar, S. [verfasserIn] Selvasekarapandian, S. [verfasserIn] Arunkumar, D. [verfasserIn] Nithya, H. [verfasserIn] Kawamura, J. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2016 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of polymer research - Dordrecht : Springer Science + Business Media B.V., 1994, 23(2016), 3 vom: 18. Feb. |
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| Übergeordnetes Werk: |
volume:23 ; year:2016 ; number:3 ; day:18 ; month:02 |
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| DOI / URN: |
10.1007/s10965-016-0952-2 |
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| Katalog-ID: |
SPR015137228 |
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| 520 | |a Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. | ||
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| 650 | 4 | |a Ammonium hexafluorophosphate |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Proton conduction |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Polymer electrolyte |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Electrochemical impedance spectroscopy |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Dielectric Spectra |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Proton battery |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Sikkanthar, S. |e verfasserin |4 aut | |
| 700 | 1 | |a Selvasekarapandian, S. |e verfasserin |4 aut | |
| 700 | 1 | |a Arunkumar, D. |e verfasserin |4 aut | |
| 700 | 1 | |a Nithya, H. |e verfasserin |4 aut | |
| 700 | 1 | |a Kawamura, J. |e verfasserin |4 aut | |
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10.1007/s10965-016-0952-2 doi (DE-627)SPR015137228 (SPR)s10965-016-0952-2-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Karthikeyan, S. verfasserin aut Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. PAN (dpeaa)DE-He213 Ammonium hexafluorophosphate (dpeaa)DE-He213 Proton conduction (dpeaa)DE-He213 Polymer electrolyte (dpeaa)DE-He213 Electrochemical impedance spectroscopy (dpeaa)DE-He213 Dielectric Spectra (dpeaa)DE-He213 Proton battery (dpeaa)DE-He213 Sikkanthar, S. verfasserin aut Selvasekarapandian, S. verfasserin aut Arunkumar, D. verfasserin aut Nithya, H. verfasserin aut Kawamura, J. verfasserin aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 23(2016), 3 vom: 18. Feb. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:23 year:2016 number:3 day:18 month:02 https://dx.doi.org/10.1007/s10965-016-0952-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 23 2016 3 18 02 |
| spelling |
10.1007/s10965-016-0952-2 doi (DE-627)SPR015137228 (SPR)s10965-016-0952-2-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Karthikeyan, S. verfasserin aut Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. PAN (dpeaa)DE-He213 Ammonium hexafluorophosphate (dpeaa)DE-He213 Proton conduction (dpeaa)DE-He213 Polymer electrolyte (dpeaa)DE-He213 Electrochemical impedance spectroscopy (dpeaa)DE-He213 Dielectric Spectra (dpeaa)DE-He213 Proton battery (dpeaa)DE-He213 Sikkanthar, S. verfasserin aut Selvasekarapandian, S. verfasserin aut Arunkumar, D. verfasserin aut Nithya, H. verfasserin aut Kawamura, J. verfasserin aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 23(2016), 3 vom: 18. Feb. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:23 year:2016 number:3 day:18 month:02 https://dx.doi.org/10.1007/s10965-016-0952-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 23 2016 3 18 02 |
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10.1007/s10965-016-0952-2 doi (DE-627)SPR015137228 (SPR)s10965-016-0952-2-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Karthikeyan, S. verfasserin aut Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. PAN (dpeaa)DE-He213 Ammonium hexafluorophosphate (dpeaa)DE-He213 Proton conduction (dpeaa)DE-He213 Polymer electrolyte (dpeaa)DE-He213 Electrochemical impedance spectroscopy (dpeaa)DE-He213 Dielectric Spectra (dpeaa)DE-He213 Proton battery (dpeaa)DE-He213 Sikkanthar, S. verfasserin aut Selvasekarapandian, S. verfasserin aut Arunkumar, D. verfasserin aut Nithya, H. verfasserin aut Kawamura, J. verfasserin aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 23(2016), 3 vom: 18. Feb. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:23 year:2016 number:3 day:18 month:02 https://dx.doi.org/10.1007/s10965-016-0952-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 23 2016 3 18 02 |
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10.1007/s10965-016-0952-2 doi (DE-627)SPR015137228 (SPR)s10965-016-0952-2-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Karthikeyan, S. verfasserin aut Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. PAN (dpeaa)DE-He213 Ammonium hexafluorophosphate (dpeaa)DE-He213 Proton conduction (dpeaa)DE-He213 Polymer electrolyte (dpeaa)DE-He213 Electrochemical impedance spectroscopy (dpeaa)DE-He213 Dielectric Spectra (dpeaa)DE-He213 Proton battery (dpeaa)DE-He213 Sikkanthar, S. verfasserin aut Selvasekarapandian, S. verfasserin aut Arunkumar, D. verfasserin aut Nithya, H. verfasserin aut Kawamura, J. verfasserin aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 23(2016), 3 vom: 18. Feb. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:23 year:2016 number:3 day:18 month:02 https://dx.doi.org/10.1007/s10965-016-0952-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 23 2016 3 18 02 |
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10.1007/s10965-016-0952-2 doi (DE-627)SPR015137228 (SPR)s10965-016-0952-2-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Karthikeyan, S. verfasserin aut Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. PAN (dpeaa)DE-He213 Ammonium hexafluorophosphate (dpeaa)DE-He213 Proton conduction (dpeaa)DE-He213 Polymer electrolyte (dpeaa)DE-He213 Electrochemical impedance spectroscopy (dpeaa)DE-He213 Dielectric Spectra (dpeaa)DE-He213 Proton battery (dpeaa)DE-He213 Sikkanthar, S. verfasserin aut Selvasekarapandian, S. verfasserin aut Arunkumar, D. verfasserin aut Nithya, H. verfasserin aut Kawamura, J. verfasserin aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 23(2016), 3 vom: 18. Feb. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:23 year:2016 number:3 day:18 month:02 https://dx.doi.org/10.1007/s10965-016-0952-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 23 2016 3 18 02 |
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Enthalten in Journal of polymer research 23(2016), 3 vom: 18. Feb. volume:23 year:2016 number:3 day:18 month:02 |
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Karthikeyan, S. @@aut@@ Sikkanthar, S. @@aut@@ Selvasekarapandian, S. @@aut@@ Arunkumar, D. @@aut@@ Nithya, H. @@aut@@ Kawamura, J. @@aut@@ |
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Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">PAN</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Ammonium hexafluorophosphate</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Proton conduction</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Polymer electrolyte</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Electrochemical impedance spectroscopy</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Dielectric Spectra</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Proton battery</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Sikkanthar, S.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Selvasekarapandian, S.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Arunkumar, D.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Nithya, H.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Kawamura, J.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of polymer research</subfield><subfield code="d">Dordrecht : Springer Science + Business Media B.V., 1994</subfield><subfield code="g">23(2016), 3 vom: 18. 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Karthikeyan, S. |
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Karthikeyan, S. ddc 540 bkl 35.00 misc PAN misc Ammonium hexafluorophosphate misc Proton conduction misc Polymer electrolyte misc Electrochemical impedance spectroscopy misc Dielectric Spectra misc Proton battery Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system |
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540 ASE 35.00 bkl Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system PAN (dpeaa)DE-He213 Ammonium hexafluorophosphate (dpeaa)DE-He213 Proton conduction (dpeaa)DE-He213 Polymer electrolyte (dpeaa)DE-He213 Electrochemical impedance spectroscopy (dpeaa)DE-He213 Dielectric Spectra (dpeaa)DE-He213 Proton battery (dpeaa)DE-He213 |
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ddc 540 bkl 35.00 misc PAN misc Ammonium hexafluorophosphate misc Proton conduction misc Polymer electrolyte misc Electrochemical impedance spectroscopy misc Dielectric Spectra misc Proton battery |
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ddc 540 bkl 35.00 misc PAN misc Ammonium hexafluorophosphate misc Proton conduction misc Polymer electrolyte misc Electrochemical impedance spectroscopy misc Dielectric Spectra misc Proton battery |
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ddc 540 bkl 35.00 misc PAN misc Ammonium hexafluorophosphate misc Proton conduction misc Polymer electrolyte misc Electrochemical impedance spectroscopy misc Dielectric Spectra misc Proton battery |
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Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system |
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(DE-627)SPR015137228 (SPR)s10965-016-0952-2-e |
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Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system |
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Karthikeyan, S. |
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Journal of polymer research |
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Karthikeyan, S. Sikkanthar, S. Selvasekarapandian, S. Arunkumar, D. Nithya, H. Kawamura, J. |
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Karthikeyan, S. |
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10.1007/s10965-016-0952-2 |
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structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system |
| title_auth |
Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system |
| abstract |
Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. |
| abstractGer |
Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. |
| abstract_unstemmed |
Abstract Polyacrylonitrile (PAN) based polymer electrolyte membranes complexed with Ammonium hexafluorophosphate ($ NH_{4} %$ PF_{6} $) with different molar concentration are prepared by solution casting method. Increase in the amorphous nature by the addition of Ammonium salt and the formation of polymer-salt complex are confirmed by X ray diffraction studies and infrared spectroscopy respectively. The glass transition temperature is measured for all membranes and it showed a lowest value for the PAN complexed with 20 mol% of $ NH_{4} %$ PF_{6} $. Electrical properties are studied by AC impedance spectroscopy. An ionic conductivity of the order of $ 10^{−3} $ $ Scm^{−1} $ is obtained for the 80 PAN / 20 $ NH_{4} %$ PF_{6} $ polymer electrolyte. Conductivity, dielectric and modulus spectra from the impedance data are analysed to understand the ionic transport mechanism. Transference number measurement is done to study the ionic contribution to the charge transport. A proton battery with the configuration, Zn+ $ ZnSO_{4} $. $ 7H_{2} $O /80 PAN / 20 $ NH_{4} %$ PF_{6} $ / $ PbO_{2} $ +$ V_{2} %$ O_{5} $ has been constructed and its discharge characteristics are studied. |
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Structural, electrical and electrochemical properties of polyacrylonitrile-ammonium hexaflurophosphate polymer electrolyte system |
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Sikkanthar, S. Selvasekarapandian, S. Arunkumar, D. Nithya, H. Kawamura, J. |
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| score |
7.399288 |