Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution
Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Kiciński, Wojciech [verfasserIn] Szala, Mateusz [verfasserIn] Nita, Marcin [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2010 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of sol gel science and technology - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993, 58(2010), 1 vom: 18. Nov., Seite 102-113 |
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| Übergeordnetes Werk: |
volume:58 ; year:2010 ; number:1 ; day:18 ; month:11 ; pages:102-113 |
| Links: |
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| DOI / URN: |
10.1007/s10971-010-2362-y |
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| Katalog-ID: |
SPR015246264 |
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| 245 | 1 | 0 | |a Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution |
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| 520 | |a Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. | ||
| 650 | 4 | |a Carbon xerogel |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Organic xerogel |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Sol–gel process |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Carbonization |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Microcellular carbon |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Phase separation |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Szala, Mateusz |e verfasserin |4 aut | |
| 700 | 1 | |a Nita, Marcin |e verfasserin |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Journal of sol gel science and technology |d Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 |g 58(2010), 1 vom: 18. Nov., Seite 102-113 |w (DE-627)268757607 |w (DE-600)1472726-2 |x 1573-4846 |7 nnns |
| 773 | 1 | 8 | |g volume:58 |g year:2010 |g number:1 |g day:18 |g month:11 |g pages:102-113 |
| 856 | 4 | 0 | |u https://dx.doi.org/10.1007/s10971-010-2362-y |z kostenfrei |3 Volltext |
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10.1007/s10971-010-2362-y doi (DE-627)SPR015246264 (SPR)s10971-010-2362-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Kiciński, Wojciech verfasserin aut Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. Carbon xerogel (dpeaa)DE-He213 Organic xerogel (dpeaa)DE-He213 Sol–gel process (dpeaa)DE-He213 Carbonization (dpeaa)DE-He213 Microcellular carbon (dpeaa)DE-He213 Phase separation (dpeaa)DE-He213 Szala, Mateusz verfasserin aut Nita, Marcin verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 58(2010), 1 vom: 18. Nov., Seite 102-113 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:58 year:2010 number:1 day:18 month:11 pages:102-113 https://dx.doi.org/10.1007/s10971-010-2362-y kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 58 2010 1 18 11 102-113 |
| spelling |
10.1007/s10971-010-2362-y doi (DE-627)SPR015246264 (SPR)s10971-010-2362-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Kiciński, Wojciech verfasserin aut Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. Carbon xerogel (dpeaa)DE-He213 Organic xerogel (dpeaa)DE-He213 Sol–gel process (dpeaa)DE-He213 Carbonization (dpeaa)DE-He213 Microcellular carbon (dpeaa)DE-He213 Phase separation (dpeaa)DE-He213 Szala, Mateusz verfasserin aut Nita, Marcin verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 58(2010), 1 vom: 18. Nov., Seite 102-113 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:58 year:2010 number:1 day:18 month:11 pages:102-113 https://dx.doi.org/10.1007/s10971-010-2362-y kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 58 2010 1 18 11 102-113 |
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10.1007/s10971-010-2362-y doi (DE-627)SPR015246264 (SPR)s10971-010-2362-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Kiciński, Wojciech verfasserin aut Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. Carbon xerogel (dpeaa)DE-He213 Organic xerogel (dpeaa)DE-He213 Sol–gel process (dpeaa)DE-He213 Carbonization (dpeaa)DE-He213 Microcellular carbon (dpeaa)DE-He213 Phase separation (dpeaa)DE-He213 Szala, Mateusz verfasserin aut Nita, Marcin verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 58(2010), 1 vom: 18. Nov., Seite 102-113 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:58 year:2010 number:1 day:18 month:11 pages:102-113 https://dx.doi.org/10.1007/s10971-010-2362-y kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 58 2010 1 18 11 102-113 |
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10.1007/s10971-010-2362-y doi (DE-627)SPR015246264 (SPR)s10971-010-2362-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Kiciński, Wojciech verfasserin aut Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. Carbon xerogel (dpeaa)DE-He213 Organic xerogel (dpeaa)DE-He213 Sol–gel process (dpeaa)DE-He213 Carbonization (dpeaa)DE-He213 Microcellular carbon (dpeaa)DE-He213 Phase separation (dpeaa)DE-He213 Szala, Mateusz verfasserin aut Nita, Marcin verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 58(2010), 1 vom: 18. Nov., Seite 102-113 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:58 year:2010 number:1 day:18 month:11 pages:102-113 https://dx.doi.org/10.1007/s10971-010-2362-y kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 58 2010 1 18 11 102-113 |
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10.1007/s10971-010-2362-y doi (DE-627)SPR015246264 (SPR)s10971-010-2362-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Kiciński, Wojciech verfasserin aut Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution 2010 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. Carbon xerogel (dpeaa)DE-He213 Organic xerogel (dpeaa)DE-He213 Sol–gel process (dpeaa)DE-He213 Carbonization (dpeaa)DE-He213 Microcellular carbon (dpeaa)DE-He213 Phase separation (dpeaa)DE-He213 Szala, Mateusz verfasserin aut Nita, Marcin verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 58(2010), 1 vom: 18. Nov., Seite 102-113 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:58 year:2010 number:1 day:18 month:11 pages:102-113 https://dx.doi.org/10.1007/s10971-010-2362-y kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 58 2010 1 18 11 102-113 |
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English |
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Enthalten in Journal of sol gel science and technology 58(2010), 1 vom: 18. Nov., Seite 102-113 volume:58 year:2010 number:1 day:18 month:11 pages:102-113 |
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Carbon xerogel Organic xerogel Sol–gel process Carbonization Microcellular carbon Phase separation |
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Journal of sol gel science and technology |
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Kiciński, Wojciech @@aut@@ Szala, Mateusz @@aut@@ Nita, Marcin @@aut@@ |
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Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. 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|
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Kiciński, Wojciech |
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Kiciński, Wojciech ddc 600 bkl 35.18 bkl 51.60 misc Carbon xerogel misc Organic xerogel misc Sol–gel process misc Carbonization misc Microcellular carbon misc Phase separation Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution |
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1573-4846 |
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600 670 ASE 35.18 bkl 51.60 bkl Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution Carbon xerogel (dpeaa)DE-He213 Organic xerogel (dpeaa)DE-He213 Sol–gel process (dpeaa)DE-He213 Carbonization (dpeaa)DE-He213 Microcellular carbon (dpeaa)DE-He213 Phase separation (dpeaa)DE-He213 |
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ddc 600 bkl 35.18 bkl 51.60 misc Carbon xerogel misc Organic xerogel misc Sol–gel process misc Carbonization misc Microcellular carbon misc Phase separation |
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ddc 600 bkl 35.18 bkl 51.60 misc Carbon xerogel misc Organic xerogel misc Sol–gel process misc Carbonization misc Microcellular carbon misc Phase separation |
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ddc 600 bkl 35.18 bkl 51.60 misc Carbon xerogel misc Organic xerogel misc Sol–gel process misc Carbonization misc Microcellular carbon misc Phase separation |
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Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution |
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Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution |
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Kiciński, Wojciech |
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Kiciński, Wojciech Szala, Mateusz Nita, Marcin |
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structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution |
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Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution |
| abstract |
Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. |
| abstractGer |
Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. |
| abstract_unstemmed |
Abstract The impact of solvent composition as well as inorganic salt content and type on carbon xerogel structure was investigated. Carbon xerogels were derived from the sol–gel polycondensation of resorcinol with furfural in a water–methanol–inorganic salt solution. As inorganic salts, NaCl, $ NH_{4} %$ ClO_{4} $ and $ FeCl_{3} $ were used. In order to conduct an accurate examination of the carbon xerogel structures and textures, inorganic salts were removed prior to carbonization. The xerogel structures can be tailored according to the water/methanol ratio and, to a lesser extent, according to the inorganic salt content and type in the starting solution. As a result, a significant amount of salt can be introduced to the gel network of the desired structure. The morphology and physical properties of the organic xerogels, carbon xerogels and their composites were characterized by means of SEM, $ N_{2} $ sorption and XRD. It was found that samples derived from mixtures with $ FeCl_{3} $ manifest well developed mesoporosity and depleated microporosity in comparison to samples prepared from mixtures with NaCl and $ NH_{4} %$ ClO_{4} $. Iron ions chemically bond to the xerogel matrix and cause its partial graphitization during the carbonization process, resulting in enhanced mesoporosity. |
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| container_issue |
1 |
| title_short |
Structurally tailored carbon xerogels produced through a sol–gel process in a water–methanol–inorganic salt solution |
| url |
https://dx.doi.org/10.1007/s10971-010-2362-y |
| remote_bool |
true |
| author2 |
Szala, Mateusz Nita, Marcin |
| author2Str |
Szala, Mateusz Nita, Marcin |
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| doi_str |
10.1007/s10971-010-2362-y |
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2024-07-03T14:55:32.831Z |
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|
| score |
7.401888 |