Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles
Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively....
Ausführliche Beschreibung
Autor*in: |
Li, Pingyun [verfasserIn] Jiang, Wei [verfasserIn] Li, Fengsheng [verfasserIn] |
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Format: |
E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2012 |
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Schlagwörter: |
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Übergeordnetes Werk: |
Enthalten in: Journal of sol gel science and technology - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993, 65(2012), 3 vom: 27. Dez., Seite 359-366 |
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Übergeordnetes Werk: |
volume:65 ; year:2012 ; number:3 ; day:27 ; month:12 ; pages:359-366 |
Links: |
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DOI / URN: |
10.1007/s10971-012-2944-y |
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Katalog-ID: |
SPR015252159 |
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520 | |a Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles. | ||
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700 | 1 | |a Jiang, Wei |e verfasserin |4 aut | |
700 | 1 | |a Li, Fengsheng |e verfasserin |4 aut | |
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10.1007/s10971-012-2944-y doi (DE-627)SPR015252159 (SPR)s10971-012-2944-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Li, Pingyun verfasserin aut Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles. Sol–gel preparation (dpeaa)DE-He213 Colloidal processing (dpeaa)DE-He213 Nanoparticles (dpeaa)DE-He213 Magnetic materials (dpeaa)DE-He213 Jiang, Wei verfasserin aut Li, Fengsheng verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 65(2012), 3 vom: 27. Dez., Seite 359-366 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:65 year:2012 number:3 day:27 month:12 pages:359-366 https://dx.doi.org/10.1007/s10971-012-2944-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 65 2012 3 27 12 359-366 |
spelling |
10.1007/s10971-012-2944-y doi (DE-627)SPR015252159 (SPR)s10971-012-2944-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Li, Pingyun verfasserin aut Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles. Sol–gel preparation (dpeaa)DE-He213 Colloidal processing (dpeaa)DE-He213 Nanoparticles (dpeaa)DE-He213 Magnetic materials (dpeaa)DE-He213 Jiang, Wei verfasserin aut Li, Fengsheng verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 65(2012), 3 vom: 27. Dez., Seite 359-366 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:65 year:2012 number:3 day:27 month:12 pages:359-366 https://dx.doi.org/10.1007/s10971-012-2944-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 65 2012 3 27 12 359-366 |
allfields_unstemmed |
10.1007/s10971-012-2944-y doi (DE-627)SPR015252159 (SPR)s10971-012-2944-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Li, Pingyun verfasserin aut Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles. Sol–gel preparation (dpeaa)DE-He213 Colloidal processing (dpeaa)DE-He213 Nanoparticles (dpeaa)DE-He213 Magnetic materials (dpeaa)DE-He213 Jiang, Wei verfasserin aut Li, Fengsheng verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 65(2012), 3 vom: 27. Dez., Seite 359-366 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:65 year:2012 number:3 day:27 month:12 pages:359-366 https://dx.doi.org/10.1007/s10971-012-2944-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 65 2012 3 27 12 359-366 |
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10.1007/s10971-012-2944-y doi (DE-627)SPR015252159 (SPR)s10971-012-2944-y-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Li, Pingyun verfasserin aut Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles. Sol–gel preparation (dpeaa)DE-He213 Colloidal processing (dpeaa)DE-He213 Nanoparticles (dpeaa)DE-He213 Magnetic materials (dpeaa)DE-He213 Jiang, Wei verfasserin aut Li, Fengsheng verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 65(2012), 3 vom: 27. Dez., Seite 359-366 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:65 year:2012 number:3 day:27 month:12 pages:359-366 https://dx.doi.org/10.1007/s10971-012-2944-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 65 2012 3 27 12 359-366 |
language |
English |
source |
Enthalten in Journal of sol gel science and technology 65(2012), 3 vom: 27. Dez., Seite 359-366 volume:65 year:2012 number:3 day:27 month:12 pages:359-366 |
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container_title |
Journal of sol gel science and technology |
authorswithroles_txt_mv |
Li, Pingyun @@aut@@ Jiang, Wei @@aut@@ Li, Fengsheng @@aut@@ |
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2012-12-27T00:00:00Z |
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Li, Pingyun |
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Li, Pingyun ddc 600 bkl 35.18 bkl 51.60 misc Sol–gel preparation misc Colloidal processing misc Nanoparticles misc Magnetic materials Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles |
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600 670 ASE 35.18 bkl 51.60 bkl Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles Sol–gel preparation (dpeaa)DE-He213 Colloidal processing (dpeaa)DE-He213 Nanoparticles (dpeaa)DE-He213 Magnetic materials (dpeaa)DE-He213 |
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ddc 600 bkl 35.18 bkl 51.60 misc Sol–gel preparation misc Colloidal processing misc Nanoparticles misc Magnetic materials |
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ddc 600 bkl 35.18 bkl 51.60 misc Sol–gel preparation misc Colloidal processing misc Nanoparticles misc Magnetic materials |
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ddc 600 bkl 35.18 bkl 51.60 misc Sol–gel preparation misc Colloidal processing misc Nanoparticles misc Magnetic materials |
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Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles |
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Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles |
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Li, Pingyun Jiang, Wei Li, Fengsheng |
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non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles |
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Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles |
abstract |
Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles. |
abstractGer |
Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles. |
abstract_unstemmed |
Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles. |
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title_short |
Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles |
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https://dx.doi.org/10.1007/s10971-012-2944-y |
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Jiang, Wei Li, Fengsheng |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR015252159</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20220111015343.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">201006s2012 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10971-012-2944-y</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR015252159</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s10971-012-2944-y-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">600</subfield><subfield code="a">670</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">35.18</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">51.60</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Li, Pingyun</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Non-aqueous sol–gel preparation of carbon-supported nickel nanoparticles</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2012</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract This work addresses the novel non-aqueous sol–gel process preparation of carbon-supported nickel nanoparticles. In the sol–gel process, ethanol, nickel nitrate or nickel (П) acetylacetonate, and citric acid were used as solvent, source of metallic element, and chelating agent, respectively. Hexadecylamine (HDA), oleic acid and oleylamine were used as surfactants. The calcination process was performed under protecting Ar or $ N_{2} $ flowing. Carbon supported nickel nanoparticles can be prepared by this sol–gel process. Moreover, no grain growth occurs in a temperature range of 200 K, meaning that the grain size of the nickel nanoparticles can be controlled in this sol–gel process. The nickel nanoparticles can display typical superparamagnetic behavior at room temperature when HDA has been used. This novel method is expected to have wide applications in the field of metallic nanoparticles.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Sol–gel preparation</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Colloidal processing</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Nanoparticles</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Magnetic materials</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Jiang, Wei</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Li, Fengsheng</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of sol gel science and technology</subfield><subfield code="d">Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993</subfield><subfield code="g">65(2012), 3 vom: 27. Dez., Seite 359-366</subfield><subfield code="w">(DE-627)268757607</subfield><subfield code="w">(DE-600)1472726-2</subfield><subfield code="x">1573-4846</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:65</subfield><subfield code="g">year:2012</subfield><subfield code="g">number:3</subfield><subfield code="g">day:27</subfield><subfield code="g">month:12</subfield><subfield code="g">pages:359-366</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">https://dx.doi.org/10.1007/s10971-012-2944-y</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_SPRINGER</subfield></datafield><datafield tag="912" 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