Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method
Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making f...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Penchal Reddy, M. [verfasserIn] Madhuri, W. [verfasserIn] Sadhana, K. [verfasserIn] Kim, I. G. [verfasserIn] Hui, K. N. [verfasserIn] Hui, K. S. [verfasserIn] Siva Kumar, K. V. [verfasserIn] Ramakrishna Reddy, R. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2014 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of sol gel science and technology - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993, 70(2014), 3 vom: 07. Feb., Seite 400-404 |
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| Übergeordnetes Werk: |
volume:70 ; year:2014 ; number:3 ; day:07 ; month:02 ; pages:400-404 |
| Links: |
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| DOI / URN: |
10.1007/s10971-014-3295-7 |
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| Katalog-ID: |
SPR015255824 |
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| 520 | |a Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. | ||
| 650 | 4 | |a Ferrite |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Nano particles |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Sol–gel synthesis |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Microwave sintering |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a TEM |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Saturation magnetization |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Madhuri, W. |e verfasserin |4 aut | |
| 700 | 1 | |a Sadhana, K. |e verfasserin |4 aut | |
| 700 | 1 | |a Kim, I. G. |e verfasserin |4 aut | |
| 700 | 1 | |a Hui, K. N. |e verfasserin |4 aut | |
| 700 | 1 | |a Hui, K. S. |e verfasserin |4 aut | |
| 700 | 1 | |a Siva Kumar, K. V. |e verfasserin |4 aut | |
| 700 | 1 | |a Ramakrishna Reddy, R. |e verfasserin |4 aut | |
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10.1007/s10971-014-3295-7 doi (DE-627)SPR015255824 (SPR)s10971-014-3295-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Penchal Reddy, M. verfasserin aut Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. Ferrite (dpeaa)DE-He213 Nano particles (dpeaa)DE-He213 Sol–gel synthesis (dpeaa)DE-He213 Microwave sintering (dpeaa)DE-He213 TEM (dpeaa)DE-He213 Saturation magnetization (dpeaa)DE-He213 Madhuri, W. verfasserin aut Sadhana, K. verfasserin aut Kim, I. G. verfasserin aut Hui, K. N. verfasserin aut Hui, K. S. verfasserin aut Siva Kumar, K. V. verfasserin aut Ramakrishna Reddy, R. verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 70(2014), 3 vom: 07. Feb., Seite 400-404 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:70 year:2014 number:3 day:07 month:02 pages:400-404 https://dx.doi.org/10.1007/s10971-014-3295-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 70 2014 3 07 02 400-404 |
| spelling |
10.1007/s10971-014-3295-7 doi (DE-627)SPR015255824 (SPR)s10971-014-3295-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Penchal Reddy, M. verfasserin aut Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. Ferrite (dpeaa)DE-He213 Nano particles (dpeaa)DE-He213 Sol–gel synthesis (dpeaa)DE-He213 Microwave sintering (dpeaa)DE-He213 TEM (dpeaa)DE-He213 Saturation magnetization (dpeaa)DE-He213 Madhuri, W. verfasserin aut Sadhana, K. verfasserin aut Kim, I. G. verfasserin aut Hui, K. N. verfasserin aut Hui, K. S. verfasserin aut Siva Kumar, K. V. verfasserin aut Ramakrishna Reddy, R. verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 70(2014), 3 vom: 07. Feb., Seite 400-404 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:70 year:2014 number:3 day:07 month:02 pages:400-404 https://dx.doi.org/10.1007/s10971-014-3295-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 70 2014 3 07 02 400-404 |
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10.1007/s10971-014-3295-7 doi (DE-627)SPR015255824 (SPR)s10971-014-3295-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Penchal Reddy, M. verfasserin aut Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. Ferrite (dpeaa)DE-He213 Nano particles (dpeaa)DE-He213 Sol–gel synthesis (dpeaa)DE-He213 Microwave sintering (dpeaa)DE-He213 TEM (dpeaa)DE-He213 Saturation magnetization (dpeaa)DE-He213 Madhuri, W. verfasserin aut Sadhana, K. verfasserin aut Kim, I. G. verfasserin aut Hui, K. N. verfasserin aut Hui, K. S. verfasserin aut Siva Kumar, K. V. verfasserin aut Ramakrishna Reddy, R. verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 70(2014), 3 vom: 07. Feb., Seite 400-404 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:70 year:2014 number:3 day:07 month:02 pages:400-404 https://dx.doi.org/10.1007/s10971-014-3295-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 70 2014 3 07 02 400-404 |
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10.1007/s10971-014-3295-7 doi (DE-627)SPR015255824 (SPR)s10971-014-3295-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Penchal Reddy, M. verfasserin aut Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. Ferrite (dpeaa)DE-He213 Nano particles (dpeaa)DE-He213 Sol–gel synthesis (dpeaa)DE-He213 Microwave sintering (dpeaa)DE-He213 TEM (dpeaa)DE-He213 Saturation magnetization (dpeaa)DE-He213 Madhuri, W. verfasserin aut Sadhana, K. verfasserin aut Kim, I. G. verfasserin aut Hui, K. N. verfasserin aut Hui, K. S. verfasserin aut Siva Kumar, K. V. verfasserin aut Ramakrishna Reddy, R. verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 70(2014), 3 vom: 07. Feb., Seite 400-404 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:70 year:2014 number:3 day:07 month:02 pages:400-404 https://dx.doi.org/10.1007/s10971-014-3295-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 70 2014 3 07 02 400-404 |
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10.1007/s10971-014-3295-7 doi (DE-627)SPR015255824 (SPR)s10971-014-3295-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Penchal Reddy, M. verfasserin aut Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. Ferrite (dpeaa)DE-He213 Nano particles (dpeaa)DE-He213 Sol–gel synthesis (dpeaa)DE-He213 Microwave sintering (dpeaa)DE-He213 TEM (dpeaa)DE-He213 Saturation magnetization (dpeaa)DE-He213 Madhuri, W. verfasserin aut Sadhana, K. verfasserin aut Kim, I. G. verfasserin aut Hui, K. N. verfasserin aut Hui, K. S. verfasserin aut Siva Kumar, K. V. verfasserin aut Ramakrishna Reddy, R. verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 70(2014), 3 vom: 07. Feb., Seite 400-404 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:70 year:2014 number:3 day:07 month:02 pages:400-404 https://dx.doi.org/10.1007/s10971-014-3295-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 70 2014 3 07 02 400-404 |
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Penchal Reddy, M. @@aut@@ Madhuri, W. @@aut@@ Sadhana, K. @@aut@@ Kim, I. G. @@aut@@ Hui, K. N. @@aut@@ Hui, K. S. @@aut@@ Siva Kumar, K. V. @@aut@@ Ramakrishna Reddy, R. @@aut@@ |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR015255824</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20220111015424.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">201006s2014 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10971-014-3295-7</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR015255824</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s10971-014-3295-7-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">600</subfield><subfield code="a">670</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">35.18</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">51.60</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Penchal Reddy, M.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2014</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. 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Penchal Reddy, M. |
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Penchal Reddy, M. ddc 600 bkl 35.18 bkl 51.60 misc Ferrite misc Nano particles misc Sol–gel synthesis misc Microwave sintering misc TEM misc Saturation magnetization Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method |
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600 670 ASE 35.18 bkl 51.60 bkl Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method Ferrite (dpeaa)DE-He213 Nano particles (dpeaa)DE-He213 Sol–gel synthesis (dpeaa)DE-He213 Microwave sintering (dpeaa)DE-He213 TEM (dpeaa)DE-He213 Saturation magnetization (dpeaa)DE-He213 |
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Penchal Reddy, M. Madhuri, W. Sadhana, K. Kim, I. G. Hui, K. N. Hui, K. S. Siva Kumar, K. V. Ramakrishna Reddy, R. |
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Elektronische Aufsätze |
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Penchal Reddy, M. |
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10.1007/s10971-014-3295-7 |
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microwave sintering of nickel ferrite nanoparticles processed via sol–gel method |
| title_auth |
Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method |
| abstract |
Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. |
| abstractGer |
Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. |
| abstract_unstemmed |
Abstract Magnetic nickel ferrite ($ NiFe_{2} %$ O_{4} $) was prepared by sol–gel process and calcined in the 2.45 GHz singlemode microwave furnace to synthesize nickel nanopowder. The sol–gel method was used for the processing of the $ NiFe_{2} %$ O_{4} $ powder because of its potential for making fine, pure and homogeneous powders. Sol–gel is a chemical method that has the possibility of synthesizing a reproducible material. Microwave energy is used for the calcining of this powder and the sintering of the $ NiFe_{2} %$ O_{4} $ samples. Its use for calcination has the advantage of reducing the total processing time and the soak temperature. In addition to the above combination of sol–gel and microwave processing yields to nanoscale particles and a more uniform distribution of their sizes. X-ray diffraction, energy dispersive X-ray spectroscopy, transmission electron microscopy and vibrating sample magnetometer were carried out to investigate structural, elemental, morphological and magnetic aspects of $ NiFe_{2} %$ O_{4} $. The results showed that the mean size and the saturation magnetization of the $ NiFe_{2} %$ O_{4} $ nanoparticles are about 30 nm and 55.27 emu/g, respectively. This method could be used as an alternative to other chemical methods in order to obtain $ NiFe_{2} %$ O_{4} $ nanoparticles. |
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Microwave sintering of nickel ferrite nanoparticles processed via sol–gel method |
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| score |
7.4000244 |