Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process
Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (T...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Huang, Kai [verfasserIn] Cai, Zhenyu [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of sol gel science and technology - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993, 87(2018), 2 vom: 30. Juni, Seite 264-268 |
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| Übergeordnetes Werk: |
volume:87 ; year:2018 ; number:2 ; day:30 ; month:06 ; pages:264-268 |
| Links: |
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| DOI / URN: |
10.1007/s10971-018-4734-7 |
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| Katalog-ID: |
SPR015269922 |
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| 520 | |a Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. | ||
| 520 | |a Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. | ||
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| 650 | 4 | |a Si/Al ratio |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Cai, Zhenyu |e verfasserin |4 aut | |
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10.1007/s10971-018-4734-7 doi (DE-627)SPR015269922 (SPR)s10971-018-4734-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Huang, Kai verfasserin aut Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. 3DOM (dpeaa)DE-He213 Sol–gel preparation (dpeaa)DE-He213 Composite (dpeaa)DE-He213 APTES (dpeaa)DE-He213 Si/Al ratio (dpeaa)DE-He213 Cai, Zhenyu verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 87(2018), 2 vom: 30. Juni, Seite 264-268 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:87 year:2018 number:2 day:30 month:06 pages:264-268 https://dx.doi.org/10.1007/s10971-018-4734-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 87 2018 2 30 06 264-268 |
| spelling |
10.1007/s10971-018-4734-7 doi (DE-627)SPR015269922 (SPR)s10971-018-4734-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Huang, Kai verfasserin aut Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. 3DOM (dpeaa)DE-He213 Sol–gel preparation (dpeaa)DE-He213 Composite (dpeaa)DE-He213 APTES (dpeaa)DE-He213 Si/Al ratio (dpeaa)DE-He213 Cai, Zhenyu verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 87(2018), 2 vom: 30. Juni, Seite 264-268 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:87 year:2018 number:2 day:30 month:06 pages:264-268 https://dx.doi.org/10.1007/s10971-018-4734-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 87 2018 2 30 06 264-268 |
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10.1007/s10971-018-4734-7 doi (DE-627)SPR015269922 (SPR)s10971-018-4734-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Huang, Kai verfasserin aut Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. 3DOM (dpeaa)DE-He213 Sol–gel preparation (dpeaa)DE-He213 Composite (dpeaa)DE-He213 APTES (dpeaa)DE-He213 Si/Al ratio (dpeaa)DE-He213 Cai, Zhenyu verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 87(2018), 2 vom: 30. Juni, Seite 264-268 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:87 year:2018 number:2 day:30 month:06 pages:264-268 https://dx.doi.org/10.1007/s10971-018-4734-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 87 2018 2 30 06 264-268 |
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10.1007/s10971-018-4734-7 doi (DE-627)SPR015269922 (SPR)s10971-018-4734-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Huang, Kai verfasserin aut Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. 3DOM (dpeaa)DE-He213 Sol–gel preparation (dpeaa)DE-He213 Composite (dpeaa)DE-He213 APTES (dpeaa)DE-He213 Si/Al ratio (dpeaa)DE-He213 Cai, Zhenyu verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 87(2018), 2 vom: 30. Juni, Seite 264-268 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:87 year:2018 number:2 day:30 month:06 pages:264-268 https://dx.doi.org/10.1007/s10971-018-4734-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 87 2018 2 30 06 264-268 |
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10.1007/s10971-018-4734-7 doi (DE-627)SPR015269922 (SPR)s10971-018-4734-7-e DE-627 ger DE-627 rakwb eng 600 670 ASE 35.18 bkl 51.60 bkl Huang, Kai verfasserin aut Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. 3DOM (dpeaa)DE-He213 Sol–gel preparation (dpeaa)DE-He213 Composite (dpeaa)DE-He213 APTES (dpeaa)DE-He213 Si/Al ratio (dpeaa)DE-He213 Cai, Zhenyu verfasserin aut Enthalten in Journal of sol gel science and technology Dordrecht [u.a.] : Springer Science + Business Media B.V, 1993 87(2018), 2 vom: 30. Juni, Seite 264-268 (DE-627)268757607 (DE-600)1472726-2 1573-4846 nnns volume:87 year:2018 number:2 day:30 month:06 pages:264-268 https://dx.doi.org/10.1007/s10971-018-4734-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.18 ASE 51.60 ASE AR 87 2018 2 30 06 264-268 |
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Huang, Kai |
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Huang, Kai ddc 600 bkl 35.18 bkl 51.60 misc 3DOM misc Sol–gel preparation misc Composite misc APTES misc Si/Al ratio Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process |
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600 670 ASE 35.18 bkl 51.60 bkl Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process 3DOM (dpeaa)DE-He213 Sol–gel preparation (dpeaa)DE-He213 Composite (dpeaa)DE-He213 APTES (dpeaa)DE-He213 Si/Al ratio (dpeaa)DE-He213 |
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ddc 600 bkl 35.18 bkl 51.60 misc 3DOM misc Sol–gel preparation misc Composite misc APTES misc Si/Al ratio |
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Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process |
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synthesis and characterization of three-dimensional ordered macroporous si–al compound oxide by sol–gel process |
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Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process |
| abstract |
Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. |
| abstractGer |
Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. |
| abstract_unstemmed |
Abstract A series of three-dimensional ordered macropore (3DOM) Si–Al compound oxide with different ratios of Si/Al were synthesized using a simple colloidal crystal template method. The synthesized material was characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The results show that the addition of 3-Aminpropyltriethoxysilane (APTES) and the concentration of aluminum in the precursor had remarkable impact on the structure but were not observed the transformation of the aluminosilicate crystalline form of the material. The facile synthetic method as well as the ability to control the Si/Al ratio will make 3DOM Si–Al compound oxide have great potential application value as catalyst. Highlights The three-dimensional ordered macroporous Si–Al compound oxide were synthesized by the colloidal crystal template method with sol–gel process for the first time.We used APTES as “molecular bridge” due to its cementing effect.The Si/Al ratio of samples have great impact on its specific surface area. |
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Synthesis and characterization of three-dimensional ordered macroporous Si–Al compound oxide by sol–gel process |
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https://dx.doi.org/10.1007/s10971-018-4734-7 |
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Cai, Zhenyu |
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10.1007/s10971-018-4734-7 |
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2024-07-03T15:05:54.050Z |
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| score |
7.4012938 |