Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC
Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Zhong, Yanjun [verfasserIn] Li, Xuecong [verfasserIn] Gu, Zhanyong [verfasserIn] Wang, Xinlong [verfasserIn] Yang, Lin [verfasserIn] Yang, Xiushan [verfasserIn] Zhang, Zhiye [verfasserIn] Zhong, Benhe [verfasserIn] |
|---|
| Format: |
E-Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2017 |
|---|
| Schlagwörter: |
|---|
| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969, 131(2017), 2 vom: 30. Aug., Seite 1287-1293 |
|---|---|
| Übergeordnetes Werk: |
volume:131 ; year:2017 ; number:2 ; day:30 ; month:08 ; pages:1287-1293 |
| Links: |
|---|
| DOI / URN: |
10.1007/s10973-017-6640-6 |
|---|
| Katalog-ID: |
SPR015607186 |
|---|
| LEADER | 01000caa a22002652 4500 | ||
|---|---|---|---|
| 001 | SPR015607186 | ||
| 003 | DE-627 | ||
| 005 | 20230519144910.0 | ||
| 007 | cr uuu---uuuuu | ||
| 008 | 201006s2017 xx |||||o 00| ||eng c | ||
| 024 | 7 | |a 10.1007/s10973-017-6640-6 |2 doi | |
| 035 | |a (DE-627)SPR015607186 | ||
| 035 | |a (SPR)s10973-017-6640-6-e | ||
| 040 | |a DE-627 |b ger |c DE-627 |e rakwb | ||
| 041 | |a eng | ||
| 082 | 0 | 4 | |a 660 |q ASE |
| 084 | |a 35.00 |2 bkl | ||
| 100 | 1 | |a Zhong, Yanjun |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC |
| 264 | 1 | |c 2017 | |
| 336 | |a Text |b txt |2 rdacontent | ||
| 337 | |a Computermedien |b c |2 rdamedia | ||
| 338 | |a Online-Ressource |b cr |2 rdacarrier | ||
| 520 | |a Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). | ||
| 650 | 4 | |a Li(CH |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a CN) |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a PF |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Li(C |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a H |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a O |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a ) |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a PF |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Thermal decomposition |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a TG–MS–DTA |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a DSC |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Li, Xuecong |e verfasserin |4 aut | |
| 700 | 1 | |a Gu, Zhanyong |e verfasserin |4 aut | |
| 700 | 1 | |a Wang, Xinlong |e verfasserin |4 aut | |
| 700 | 1 | |a Yang, Lin |e verfasserin |4 aut | |
| 700 | 1 | |a Yang, Xiushan |e verfasserin |4 aut | |
| 700 | 1 | |a Zhang, Zhiye |e verfasserin |4 aut | |
| 700 | 1 | |a Zhong, Benhe |e verfasserin |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Journal of thermal analysis and calorimetry |d Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 |g 131(2017), 2 vom: 30. Aug., Seite 1287-1293 |w (DE-627)315295422 |w (DE-600)2017304-0 |x 1572-8943 |7 nnns |
| 773 | 1 | 8 | |g volume:131 |g year:2017 |g number:2 |g day:30 |g month:08 |g pages:1287-1293 |
| 856 | 4 | 0 | |u https://dx.doi.org/10.1007/s10973-017-6640-6 |z lizenzpflichtig |3 Volltext |
| 912 | |a GBV_USEFLAG_A | ||
| 912 | |a SYSFLAG_A | ||
| 912 | |a GBV_SPRINGER | ||
| 912 | |a SSG-OLC-PHA | ||
| 912 | |a GBV_ILN_11 | ||
| 912 | |a GBV_ILN_20 | ||
| 912 | |a GBV_ILN_22 | ||
| 912 | |a GBV_ILN_23 | ||
| 912 | |a GBV_ILN_24 | ||
| 912 | |a GBV_ILN_31 | ||
| 912 | |a GBV_ILN_32 | ||
| 912 | |a GBV_ILN_39 | ||
| 912 | |a GBV_ILN_40 | ||
| 912 | |a GBV_ILN_60 | ||
| 912 | |a GBV_ILN_62 | ||
| 912 | |a GBV_ILN_63 | ||
| 912 | |a GBV_ILN_69 | ||
| 912 | |a GBV_ILN_70 | ||
| 912 | |a GBV_ILN_73 | ||
| 912 | |a GBV_ILN_74 | ||
| 912 | |a GBV_ILN_90 | ||
| 912 | |a GBV_ILN_95 | ||
| 912 | |a GBV_ILN_100 | ||
| 912 | |a GBV_ILN_105 | ||
| 912 | |a GBV_ILN_110 | ||
| 912 | |a GBV_ILN_120 | ||
| 912 | |a GBV_ILN_138 | ||
| 912 | |a GBV_ILN_150 | ||
| 912 | |a GBV_ILN_151 | ||
| 912 | |a GBV_ILN_152 | ||
| 912 | |a GBV_ILN_161 | ||
| 912 | |a GBV_ILN_170 | ||
| 912 | |a GBV_ILN_171 | ||
| 912 | |a GBV_ILN_187 | ||
| 912 | |a GBV_ILN_206 | ||
| 912 | |a GBV_ILN_213 | ||
| 912 | |a GBV_ILN_224 | ||
| 912 | |a GBV_ILN_230 | ||
| 912 | |a GBV_ILN_250 | ||
| 912 | |a GBV_ILN_281 | ||
| 912 | |a GBV_ILN_285 | ||
| 912 | |a GBV_ILN_293 | ||
| 912 | |a GBV_ILN_370 | ||
| 912 | |a GBV_ILN_602 | ||
| 912 | |a GBV_ILN_636 | ||
| 912 | |a GBV_ILN_702 | ||
| 912 | |a GBV_ILN_2001 | ||
| 912 | |a GBV_ILN_2003 | ||
| 912 | |a GBV_ILN_2004 | ||
| 912 | |a GBV_ILN_2005 | ||
| 912 | |a GBV_ILN_2006 | ||
| 912 | |a GBV_ILN_2007 | ||
| 912 | |a GBV_ILN_2008 | ||
| 912 | |a GBV_ILN_2009 | ||
| 912 | |a GBV_ILN_2010 | ||
| 912 | |a GBV_ILN_2011 | ||
| 912 | |a GBV_ILN_2014 | ||
| 912 | |a GBV_ILN_2015 | ||
| 912 | |a GBV_ILN_2020 | ||
| 912 | |a GBV_ILN_2021 | ||
| 912 | |a GBV_ILN_2025 | ||
| 912 | |a GBV_ILN_2026 | ||
| 912 | |a GBV_ILN_2027 | ||
| 912 | |a GBV_ILN_2031 | ||
| 912 | |a GBV_ILN_2034 | ||
| 912 | |a GBV_ILN_2037 | ||
| 912 | |a GBV_ILN_2038 | ||
| 912 | |a GBV_ILN_2039 | ||
| 912 | |a GBV_ILN_2044 | ||
| 912 | |a GBV_ILN_2048 | ||
| 912 | |a GBV_ILN_2049 | ||
| 912 | |a GBV_ILN_2050 | ||
| 912 | |a GBV_ILN_2055 | ||
| 912 | |a GBV_ILN_2056 | ||
| 912 | |a GBV_ILN_2057 | ||
| 912 | |a GBV_ILN_2059 | ||
| 912 | |a GBV_ILN_2061 | ||
| 912 | |a GBV_ILN_2064 | ||
| 912 | |a GBV_ILN_2065 | ||
| 912 | |a GBV_ILN_2068 | ||
| 912 | |a GBV_ILN_2070 | ||
| 912 | |a GBV_ILN_2086 | ||
| 912 | |a GBV_ILN_2088 | ||
| 912 | |a GBV_ILN_2093 | ||
| 912 | |a GBV_ILN_2106 | ||
| 912 | |a GBV_ILN_2107 | ||
| 912 | |a GBV_ILN_2108 | ||
| 912 | |a GBV_ILN_2110 | ||
| 912 | |a GBV_ILN_2111 | ||
| 912 | |a GBV_ILN_2112 | ||
| 912 | |a GBV_ILN_2113 | ||
| 912 | |a GBV_ILN_2116 | ||
| 912 | |a GBV_ILN_2118 | ||
| 912 | |a GBV_ILN_2119 | ||
| 912 | |a GBV_ILN_2122 | ||
| 912 | |a GBV_ILN_2129 | ||
| 912 | |a GBV_ILN_2143 | ||
| 912 | |a GBV_ILN_2144 | ||
| 912 | |a GBV_ILN_2147 | ||
| 912 | |a GBV_ILN_2148 | ||
| 912 | |a GBV_ILN_2152 | ||
| 912 | |a GBV_ILN_2153 | ||
| 912 | |a GBV_ILN_2188 | ||
| 912 | |a GBV_ILN_2190 | ||
| 912 | |a GBV_ILN_2232 | ||
| 912 | |a GBV_ILN_2336 | ||
| 912 | |a GBV_ILN_2446 | ||
| 912 | |a GBV_ILN_2470 | ||
| 912 | |a GBV_ILN_2472 | ||
| 912 | |a GBV_ILN_2507 | ||
| 912 | |a GBV_ILN_2522 | ||
| 912 | |a GBV_ILN_2548 | ||
| 912 | |a GBV_ILN_4035 | ||
| 912 | |a GBV_ILN_4037 | ||
| 912 | |a GBV_ILN_4046 | ||
| 912 | |a GBV_ILN_4112 | ||
| 912 | |a GBV_ILN_4125 | ||
| 912 | |a GBV_ILN_4242 | ||
| 912 | |a GBV_ILN_4246 | ||
| 912 | |a GBV_ILN_4249 | ||
| 912 | |a GBV_ILN_4251 | ||
| 912 | |a GBV_ILN_4305 | ||
| 912 | |a GBV_ILN_4306 | ||
| 912 | |a GBV_ILN_4307 | ||
| 912 | |a GBV_ILN_4313 | ||
| 912 | |a GBV_ILN_4322 | ||
| 912 | |a GBV_ILN_4323 | ||
| 912 | |a GBV_ILN_4324 | ||
| 912 | |a GBV_ILN_4325 | ||
| 912 | |a GBV_ILN_4326 | ||
| 912 | |a GBV_ILN_4328 | ||
| 912 | |a GBV_ILN_4333 | ||
| 912 | |a GBV_ILN_4334 | ||
| 912 | |a GBV_ILN_4335 | ||
| 912 | |a GBV_ILN_4336 | ||
| 912 | |a GBV_ILN_4338 | ||
| 912 | |a GBV_ILN_4393 | ||
| 912 | |a GBV_ILN_4700 | ||
| 936 | b | k | |a 35.00 |q ASE |
| 951 | |a AR | ||
| 952 | |d 131 |j 2017 |e 2 |b 30 |c 08 |h 1287-1293 | ||
| author_variant |
y z yz x l xl z g zg x w xw l y ly x y xy z z zz b z bz |
|---|---|
| matchkey_str |
article:15728943:2017----::hrasuisnih3np_adi_h1o2p_cmlx |
| hierarchy_sort_str |
2017 |
| bklnumber |
35.00 |
| publishDate |
2017 |
| allfields |
10.1007/s10973-017-6640-6 doi (DE-627)SPR015607186 (SPR)s10973-017-6640-6-e DE-627 ger DE-627 rakwb eng 660 ASE 35.00 bkl Zhong, Yanjun verfasserin aut Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). Li(CH (dpeaa)DE-He213 CN) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Li(C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 ) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Thermal decomposition (dpeaa)DE-He213 TG–MS–DTA (dpeaa)DE-He213 DSC (dpeaa)DE-He213 Li, Xuecong verfasserin aut Gu, Zhanyong verfasserin aut Wang, Xinlong verfasserin aut Yang, Lin verfasserin aut Yang, Xiushan verfasserin aut Zhang, Zhiye verfasserin aut Zhong, Benhe verfasserin aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 131(2017), 2 vom: 30. Aug., Seite 1287-1293 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:131 year:2017 number:2 day:30 month:08 pages:1287-1293 https://dx.doi.org/10.1007/s10973-017-6640-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 131 2017 2 30 08 1287-1293 |
| spelling |
10.1007/s10973-017-6640-6 doi (DE-627)SPR015607186 (SPR)s10973-017-6640-6-e DE-627 ger DE-627 rakwb eng 660 ASE 35.00 bkl Zhong, Yanjun verfasserin aut Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). Li(CH (dpeaa)DE-He213 CN) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Li(C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 ) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Thermal decomposition (dpeaa)DE-He213 TG–MS–DTA (dpeaa)DE-He213 DSC (dpeaa)DE-He213 Li, Xuecong verfasserin aut Gu, Zhanyong verfasserin aut Wang, Xinlong verfasserin aut Yang, Lin verfasserin aut Yang, Xiushan verfasserin aut Zhang, Zhiye verfasserin aut Zhong, Benhe verfasserin aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 131(2017), 2 vom: 30. Aug., Seite 1287-1293 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:131 year:2017 number:2 day:30 month:08 pages:1287-1293 https://dx.doi.org/10.1007/s10973-017-6640-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 131 2017 2 30 08 1287-1293 |
| allfields_unstemmed |
10.1007/s10973-017-6640-6 doi (DE-627)SPR015607186 (SPR)s10973-017-6640-6-e DE-627 ger DE-627 rakwb eng 660 ASE 35.00 bkl Zhong, Yanjun verfasserin aut Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). Li(CH (dpeaa)DE-He213 CN) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Li(C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 ) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Thermal decomposition (dpeaa)DE-He213 TG–MS–DTA (dpeaa)DE-He213 DSC (dpeaa)DE-He213 Li, Xuecong verfasserin aut Gu, Zhanyong verfasserin aut Wang, Xinlong verfasserin aut Yang, Lin verfasserin aut Yang, Xiushan verfasserin aut Zhang, Zhiye verfasserin aut Zhong, Benhe verfasserin aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 131(2017), 2 vom: 30. Aug., Seite 1287-1293 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:131 year:2017 number:2 day:30 month:08 pages:1287-1293 https://dx.doi.org/10.1007/s10973-017-6640-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 131 2017 2 30 08 1287-1293 |
| allfieldsGer |
10.1007/s10973-017-6640-6 doi (DE-627)SPR015607186 (SPR)s10973-017-6640-6-e DE-627 ger DE-627 rakwb eng 660 ASE 35.00 bkl Zhong, Yanjun verfasserin aut Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). Li(CH (dpeaa)DE-He213 CN) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Li(C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 ) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Thermal decomposition (dpeaa)DE-He213 TG–MS–DTA (dpeaa)DE-He213 DSC (dpeaa)DE-He213 Li, Xuecong verfasserin aut Gu, Zhanyong verfasserin aut Wang, Xinlong verfasserin aut Yang, Lin verfasserin aut Yang, Xiushan verfasserin aut Zhang, Zhiye verfasserin aut Zhong, Benhe verfasserin aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 131(2017), 2 vom: 30. Aug., Seite 1287-1293 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:131 year:2017 number:2 day:30 month:08 pages:1287-1293 https://dx.doi.org/10.1007/s10973-017-6640-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 131 2017 2 30 08 1287-1293 |
| allfieldsSound |
10.1007/s10973-017-6640-6 doi (DE-627)SPR015607186 (SPR)s10973-017-6640-6-e DE-627 ger DE-627 rakwb eng 660 ASE 35.00 bkl Zhong, Yanjun verfasserin aut Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). Li(CH (dpeaa)DE-He213 CN) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Li(C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 ) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Thermal decomposition (dpeaa)DE-He213 TG–MS–DTA (dpeaa)DE-He213 DSC (dpeaa)DE-He213 Li, Xuecong verfasserin aut Gu, Zhanyong verfasserin aut Wang, Xinlong verfasserin aut Yang, Lin verfasserin aut Yang, Xiushan verfasserin aut Zhang, Zhiye verfasserin aut Zhong, Benhe verfasserin aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 131(2017), 2 vom: 30. Aug., Seite 1287-1293 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:131 year:2017 number:2 day:30 month:08 pages:1287-1293 https://dx.doi.org/10.1007/s10973-017-6640-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 131 2017 2 30 08 1287-1293 |
| language |
English |
| source |
Enthalten in Journal of thermal analysis and calorimetry 131(2017), 2 vom: 30. Aug., Seite 1287-1293 volume:131 year:2017 number:2 day:30 month:08 pages:1287-1293 |
| sourceStr |
Enthalten in Journal of thermal analysis and calorimetry 131(2017), 2 vom: 30. Aug., Seite 1287-1293 volume:131 year:2017 number:2 day:30 month:08 pages:1287-1293 |
| format_phy_str_mv |
Article |
| institution |
findex.gbv.de |
| topic_facet |
Li(CH CN) PF Li(C H O ) Thermal decomposition TG–MS–DTA DSC |
| dewey-raw |
660 |
| isfreeaccess_bool |
false |
| container_title |
Journal of thermal analysis and calorimetry |
| authorswithroles_txt_mv |
Zhong, Yanjun @@aut@@ Li, Xuecong @@aut@@ Gu, Zhanyong @@aut@@ Wang, Xinlong @@aut@@ Yang, Lin @@aut@@ Yang, Xiushan @@aut@@ Zhang, Zhiye @@aut@@ Zhong, Benhe @@aut@@ |
| publishDateDaySort_date |
2017-08-30T00:00:00Z |
| hierarchy_top_id |
315295422 |
| dewey-sort |
3660 |
| id |
SPR015607186 |
| language_de |
englisch |
| fullrecord |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR015607186</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230519144910.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">201006s2017 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10973-017-6640-6</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR015607186</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s10973-017-6640-6-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">35.00</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Zhong, Yanjun</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2017</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC).</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Li(CH</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">CN)</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">PF</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Li(C</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">H</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">O</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">)</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">PF</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Thermal decomposition</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">TG–MS–DTA</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">DSC</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Li, Xuecong</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Gu, Zhanyong</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wang, Xinlong</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Yang, Lin</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Yang, Xiushan</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Zhang, Zhiye</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Zhong, Benhe</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of thermal analysis and calorimetry</subfield><subfield code="d">Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969</subfield><subfield code="g">131(2017), 2 vom: 30. Aug., Seite 1287-1293</subfield><subfield code="w">(DE-627)315295422</subfield><subfield code="w">(DE-600)2017304-0</subfield><subfield code="x">1572-8943</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:131</subfield><subfield code="g">year:2017</subfield><subfield code="g">number:2</subfield><subfield code="g">day:30</subfield><subfield code="g">month:08</subfield><subfield code="g">pages:1287-1293</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">https://dx.doi.org/10.1007/s10973-017-6640-6</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_SPRINGER</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_11</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_20</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_22</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_23</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_24</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_31</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_32</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_39</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_40</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_60</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_62</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_63</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_69</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_73</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_74</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_90</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_95</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_100</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_105</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_110</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_120</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_138</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_150</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_151</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_152</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_161</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_170</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_171</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_187</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_206</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_213</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_224</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_230</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_250</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_281</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_285</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_293</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_370</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_602</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_636</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_702</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2001</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2003</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2004</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2005</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2006</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2007</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2008</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2009</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2010</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2011</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2014</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2015</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2020</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2021</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2025</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2026</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2027</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2031</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2034</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2037</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2038</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2039</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2044</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2048</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2049</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2050</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2055</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2056</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2057</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2059</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2061</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2064</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2065</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2068</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2070</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2086</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2088</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2093</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2106</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2107</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2108</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2110</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2111</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2112</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2113</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2116</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2118</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2119</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2122</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2129</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2143</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2144</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2147</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2148</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2152</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2153</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2188</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2190</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2232</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2336</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2446</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2470</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2472</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2507</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2522</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2548</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4035</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4037</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4046</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4112</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4125</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4242</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4246</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4249</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4251</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4305</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4306</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4307</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4313</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4322</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4323</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4324</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4325</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4326</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4328</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4333</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4334</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4335</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4336</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4338</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4393</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4700</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">35.00</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">131</subfield><subfield code="j">2017</subfield><subfield code="e">2</subfield><subfield code="b">30</subfield><subfield code="c">08</subfield><subfield code="h">1287-1293</subfield></datafield></record></collection>
|
| author |
Zhong, Yanjun |
| spellingShingle |
Zhong, Yanjun ddc 660 bkl 35.00 misc Li(CH misc CN) misc PF misc Li(C misc H misc O misc ) misc Thermal decomposition misc TG–MS–DTA misc DSC Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC |
| authorStr |
Zhong, Yanjun |
| ppnlink_with_tag_str_mv |
@@773@@(DE-627)315295422 |
| format |
electronic Article |
| dewey-ones |
660 - Chemical engineering |
| delete_txt_mv |
keep |
| author_role |
aut aut aut aut aut aut aut aut |
| collection |
springer |
| remote_str |
true |
| illustrated |
Not Illustrated |
| issn |
1572-8943 |
| topic_title |
660 ASE 35.00 bkl Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC Li(CH (dpeaa)DE-He213 CN) (dpeaa)DE-He213 PF (dpeaa)DE-He213 Li(C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 ) (dpeaa)DE-He213 Thermal decomposition (dpeaa)DE-He213 TG–MS–DTA (dpeaa)DE-He213 DSC (dpeaa)DE-He213 |
| topic |
ddc 660 bkl 35.00 misc Li(CH misc CN) misc PF misc Li(C misc H misc O misc ) misc Thermal decomposition misc TG–MS–DTA misc DSC |
| topic_unstemmed |
ddc 660 bkl 35.00 misc Li(CH misc CN) misc PF misc Li(C misc H misc O misc ) misc Thermal decomposition misc TG–MS–DTA misc DSC |
| topic_browse |
ddc 660 bkl 35.00 misc Li(CH misc CN) misc PF misc Li(C misc H misc O misc ) misc Thermal decomposition misc TG–MS–DTA misc DSC |
| format_facet |
Elektronische Aufsätze Aufsätze Elektronische Ressource |
| format_main_str_mv |
Text Zeitschrift/Artikel |
| carriertype_str_mv |
cr |
| hierarchy_parent_title |
Journal of thermal analysis and calorimetry |
| hierarchy_parent_id |
315295422 |
| dewey-tens |
660 - Chemical engineering |
| hierarchy_top_title |
Journal of thermal analysis and calorimetry |
| isfreeaccess_txt |
false |
| familylinks_str_mv |
(DE-627)315295422 (DE-600)2017304-0 |
| title |
Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC |
| ctrlnum |
(DE-627)SPR015607186 (SPR)s10973-017-6640-6-e |
| title_full |
Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC |
| author_sort |
Zhong, Yanjun |
| journal |
Journal of thermal analysis and calorimetry |
| journalStr |
Journal of thermal analysis and calorimetry |
| lang_code |
eng |
| isOA_bool |
false |
| dewey-hundreds |
600 - Technology |
| recordtype |
marc |
| publishDateSort |
2017 |
| contenttype_str_mv |
txt |
| container_start_page |
1287 |
| author_browse |
Zhong, Yanjun Li, Xuecong Gu, Zhanyong Wang, Xinlong Yang, Lin Yang, Xiushan Zhang, Zhiye Zhong, Benhe |
| container_volume |
131 |
| class |
660 ASE 35.00 bkl |
| format_se |
Elektronische Aufsätze |
| author-letter |
Zhong, Yanjun |
| doi_str_mv |
10.1007/s10973-017-6640-6 |
| dewey-full |
660 |
| author2-role |
verfasserin |
| title_sort |
thermal studies on li($ ch_{3} $cn)4$ pf_{6} $ and li($ c_{4} %$ h_{10} %$ o_{2} $)2$ pf_{6} $ complexes by the tg–dta–ms and dsc |
| title_auth |
Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC |
| abstract |
Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). |
| abstractGer |
Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). |
| abstract_unstemmed |
Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC). |
| collection_details |
GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 |
| container_issue |
2 |
| title_short |
Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC |
| url |
https://dx.doi.org/10.1007/s10973-017-6640-6 |
| remote_bool |
true |
| author2 |
Li, Xuecong Gu, Zhanyong Wang, Xinlong Yang, Lin Yang, Xiushan Zhang, Zhiye Zhong, Benhe |
| author2Str |
Li, Xuecong Gu, Zhanyong Wang, Xinlong Yang, Lin Yang, Xiushan Zhang, Zhiye Zhong, Benhe |
| ppnlink |
315295422 |
| mediatype_str_mv |
c |
| isOA_txt |
false |
| hochschulschrift_bool |
false |
| doi_str |
10.1007/s10973-017-6640-6 |
| up_date |
2024-07-03T17:20:14.500Z |
| _version_ |
1803579256484134912 |
| fullrecord_marcxml |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR015607186</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230519144910.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">201006s2017 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10973-017-6640-6</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR015607186</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s10973-017-6640-6-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">35.00</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Zhong, Yanjun</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Thermal studies on Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes by the TG–DTA–MS and DSC</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2017</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes are important intermediates created in the synthetic process of high-purity $ LiPF_{6} $ electrolyte via transformation method. The thermal decomposition behavior of as-prepared Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystals in pure nitrogen atmosphere has been studied by means of thermogravimetric–differential thermal analysis coupled with mass spectrometry (TG–DTA–MS). Results suggest that the decomposition of Li($ CH_{3} $CN)4$ PF_{6} $ complex can be roughly divided into a three-stage process, and $ CH_{3} $CN is the primary gas product of decomposition process for Li($ CH_{3} $CN)4$ PF_{6} $ in open $ Al_{2} %$ O_{3} $ pans. Further insight into Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ crystal indicates that it undergoes a similar decomposition process to Li($ CH_{3} $CN)4$ PF_{6} $. Accordingly, the detailed deduction of the thermal decomposition mechanism formulas for them was presented in this paper. Besides, the thermal behaviors of Li($ CH_{3} $CN)4$ PF_{6} $ and Li($ C_{4} %$ H_{10} %$ O_{2} $)2$ PF_{6} $ complexes in hermetic aluminum pan were also investigated by differential scanning calorimetry (DSC).</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Li(CH</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">CN)</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">PF</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Li(C</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">H</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">O</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">)</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">PF</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Thermal decomposition</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">TG–MS–DTA</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">DSC</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Li, Xuecong</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Gu, Zhanyong</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wang, Xinlong</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Yang, Lin</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Yang, Xiushan</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Zhang, Zhiye</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Zhong, Benhe</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of thermal analysis and calorimetry</subfield><subfield code="d">Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969</subfield><subfield code="g">131(2017), 2 vom: 30. Aug., Seite 1287-1293</subfield><subfield code="w">(DE-627)315295422</subfield><subfield code="w">(DE-600)2017304-0</subfield><subfield code="x">1572-8943</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:131</subfield><subfield code="g">year:2017</subfield><subfield code="g">number:2</subfield><subfield code="g">day:30</subfield><subfield code="g">month:08</subfield><subfield code="g">pages:1287-1293</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">https://dx.doi.org/10.1007/s10973-017-6640-6</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_SPRINGER</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_11</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_20</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_22</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_23</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_24</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_31</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_32</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_39</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_40</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_60</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_62</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_63</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_69</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_73</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_74</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_90</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_95</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_100</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_105</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_110</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_120</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_138</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_150</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_151</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_152</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_161</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_170</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_171</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_187</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_206</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_213</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_224</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_230</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_250</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_281</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_285</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_293</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_370</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_602</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_636</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_702</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2001</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2003</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2004</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2005</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2006</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2007</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2008</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2009</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2010</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2011</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2014</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2015</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2020</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2021</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2025</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2026</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2027</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2031</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2034</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2037</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2038</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2039</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2044</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2048</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2049</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2050</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2055</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2056</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2057</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2059</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2061</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2064</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2065</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2068</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2070</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2086</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2088</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2093</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2106</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2107</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2108</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2110</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2111</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2112</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2113</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2116</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2118</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2119</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2122</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2129</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2143</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2144</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2147</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2148</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2152</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2153</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2188</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2190</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2232</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2336</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2446</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2470</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2472</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2507</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2522</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2548</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4035</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4037</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4046</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4112</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4125</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4242</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4246</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4249</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4251</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4305</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4306</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4307</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4313</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4322</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4323</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4324</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4325</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4326</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4328</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4333</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4334</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4335</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4336</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4338</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4393</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4700</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">35.00</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">131</subfield><subfield code="j">2017</subfield><subfield code="e">2</subfield><subfield code="b">30</subfield><subfield code="c">08</subfield><subfield code="h">1287-1293</subfield></datafield></record></collection>
|
| score |
7.401865 |