Vacuum oxidation of freshly deposited iron nanofilms

Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microsc...
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Autor*in:	Kotenev, V. A. [verfasserIn] Petrunin, M. A. [verfasserIn] Maksaeva, L. B. [verfasserIn] Timofeeva, V. A. [verfasserIn] Tsivadze, A. Yu. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2013

Schlagwörter:	Magnetite Hematite Wustite Iron Layer Oxide Shell

Übergeordnetes Werk:	Enthalten in: Protection of metals - Moscow : MAIK Nauka/Interperiodica Publ., 2000, 49(2013), 4 vom: Juli, Seite 479-484
Übergeordnetes Werk:	volume:49 ; year:2013 ; number:4 ; month:07 ; pages:479-484

Links:	Volltext

DOI / URN:	10.1134/S2070205113040072

Katalog-ID:	SPR016849353

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520			\|a Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air).
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allfields	10.1134/S2070205113040072 doi (DE-627)SPR016849353 (SPR)S2070205113040072-e DE-627 ger DE-627 rakwb eng 670 ASE 52.78 bkl Kotenev, V. A. verfasserin aut Vacuum oxidation of freshly deposited iron nanofilms 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air). Magnetite (dpeaa)DE-He213 Hematite (dpeaa)DE-He213 Wustite (dpeaa)DE-He213 Iron Layer (dpeaa)DE-He213 Oxide Shell (dpeaa)DE-He213 Petrunin, M. A. verfasserin aut Maksaeva, L. B. verfasserin aut Timofeeva, V. A. verfasserin aut Tsivadze, A. Yu. verfasserin aut Enthalten in Protection of metals Moscow : MAIK Nauka/Interperiodica Publ., 2000 49(2013), 4 vom: Juli, Seite 479-484 (DE-627)334712300 (DE-600)2058128-2 1608-327X nnns volume:49 year:2013 number:4 month:07 pages:479-484 https://dx.doi.org/10.1134/S2070205113040072 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 52.78 ASE AR 49 2013 4 07 479-484
spelling	10.1134/S2070205113040072 doi (DE-627)SPR016849353 (SPR)S2070205113040072-e DE-627 ger DE-627 rakwb eng 670 ASE 52.78 bkl Kotenev, V. A. verfasserin aut Vacuum oxidation of freshly deposited iron nanofilms 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air). Magnetite (dpeaa)DE-He213 Hematite (dpeaa)DE-He213 Wustite (dpeaa)DE-He213 Iron Layer (dpeaa)DE-He213 Oxide Shell (dpeaa)DE-He213 Petrunin, M. A. verfasserin aut Maksaeva, L. B. verfasserin aut Timofeeva, V. A. verfasserin aut Tsivadze, A. Yu. verfasserin aut Enthalten in Protection of metals Moscow : MAIK Nauka/Interperiodica Publ., 2000 49(2013), 4 vom: Juli, Seite 479-484 (DE-627)334712300 (DE-600)2058128-2 1608-327X nnns volume:49 year:2013 number:4 month:07 pages:479-484 https://dx.doi.org/10.1134/S2070205113040072 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 52.78 ASE AR 49 2013 4 07 479-484
allfields_unstemmed	10.1134/S2070205113040072 doi (DE-627)SPR016849353 (SPR)S2070205113040072-e DE-627 ger DE-627 rakwb eng 670 ASE 52.78 bkl Kotenev, V. A. verfasserin aut Vacuum oxidation of freshly deposited iron nanofilms 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air). Magnetite (dpeaa)DE-He213 Hematite (dpeaa)DE-He213 Wustite (dpeaa)DE-He213 Iron Layer (dpeaa)DE-He213 Oxide Shell (dpeaa)DE-He213 Petrunin, M. A. verfasserin aut Maksaeva, L. B. verfasserin aut Timofeeva, V. A. verfasserin aut Tsivadze, A. Yu. verfasserin aut Enthalten in Protection of metals Moscow : MAIK Nauka/Interperiodica Publ., 2000 49(2013), 4 vom: Juli, Seite 479-484 (DE-627)334712300 (DE-600)2058128-2 1608-327X nnns volume:49 year:2013 number:4 month:07 pages:479-484 https://dx.doi.org/10.1134/S2070205113040072 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 52.78 ASE AR 49 2013 4 07 479-484
allfieldsGer	10.1134/S2070205113040072 doi (DE-627)SPR016849353 (SPR)S2070205113040072-e DE-627 ger DE-627 rakwb eng 670 ASE 52.78 bkl Kotenev, V. A. verfasserin aut Vacuum oxidation of freshly deposited iron nanofilms 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air). Magnetite (dpeaa)DE-He213 Hematite (dpeaa)DE-He213 Wustite (dpeaa)DE-He213 Iron Layer (dpeaa)DE-He213 Oxide Shell (dpeaa)DE-He213 Petrunin, M. A. verfasserin aut Maksaeva, L. B. verfasserin aut Timofeeva, V. A. verfasserin aut Tsivadze, A. Yu. verfasserin aut Enthalten in Protection of metals Moscow : MAIK Nauka/Interperiodica Publ., 2000 49(2013), 4 vom: Juli, Seite 479-484 (DE-627)334712300 (DE-600)2058128-2 1608-327X nnns volume:49 year:2013 number:4 month:07 pages:479-484 https://dx.doi.org/10.1134/S2070205113040072 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 52.78 ASE AR 49 2013 4 07 479-484
allfieldsSound	10.1134/S2070205113040072 doi (DE-627)SPR016849353 (SPR)S2070205113040072-e DE-627 ger DE-627 rakwb eng 670 ASE 52.78 bkl Kotenev, V. A. verfasserin aut Vacuum oxidation of freshly deposited iron nanofilms 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air). Magnetite (dpeaa)DE-He213 Hematite (dpeaa)DE-He213 Wustite (dpeaa)DE-He213 Iron Layer (dpeaa)DE-He213 Oxide Shell (dpeaa)DE-He213 Petrunin, M. A. verfasserin aut Maksaeva, L. B. verfasserin aut Timofeeva, V. A. verfasserin aut Tsivadze, A. Yu. verfasserin aut Enthalten in Protection of metals Moscow : MAIK Nauka/Interperiodica Publ., 2000 49(2013), 4 vom: Juli, Seite 479-484 (DE-627)334712300 (DE-600)2058128-2 1608-327X nnns volume:49 year:2013 number:4 month:07 pages:479-484 https://dx.doi.org/10.1134/S2070205113040072 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 52.78 ASE AR 49 2013 4 07 479-484
language	English
source	Enthalten in Protection of metals 49(2013), 4 vom: Juli, Seite 479-484 volume:49 year:2013 number:4 month:07 pages:479-484
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author	Kotenev, V. A.
spellingShingle	Kotenev, V. A. ddc 670 bkl 52.78 misc Magnetite misc Hematite misc Wustite misc Iron Layer misc Oxide Shell Vacuum oxidation of freshly deposited iron nanofilms
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topic_title	670 ASE 52.78 bkl Vacuum oxidation of freshly deposited iron nanofilms Magnetite (dpeaa)DE-He213 Hematite (dpeaa)DE-He213 Wustite (dpeaa)DE-He213 Iron Layer (dpeaa)DE-He213 Oxide Shell (dpeaa)DE-He213
topic	ddc 670 bkl 52.78 misc Magnetite misc Hematite misc Wustite misc Iron Layer misc Oxide Shell
topic_unstemmed	ddc 670 bkl 52.78 misc Magnetite misc Hematite misc Wustite misc Iron Layer misc Oxide Shell
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title	Vacuum oxidation of freshly deposited iron nanofilms
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title_full	Vacuum oxidation of freshly deposited iron nanofilms
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title_sort	vacuum oxidation of freshly deposited iron nanofilms
title_auth	Vacuum oxidation of freshly deposited iron nanofilms
abstract	Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air).
abstractGer	Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air).
abstract_unstemmed	Abstract The interaction between freshly deposited iron films and oxygen at different evacuation degrees (from $ 10^{−5} $ to 760 mmHg) and room temperature is studied with the use of gravimetry (weighing with quartz nanobalance) and atomic force microscopy. According to data of atomic force microscopy, upon deposition of the metal on a glass substrate and during its subsequent oxidation, a metal-oxide composite film composed of metal-oxide nanoparticles with sizes of 20–30 nm where a metal core is covered with an oxide shell is formed. The reaction between freshly deposited iron and oxygen is shown to proceed quickly already at a pressure of $ 10^{−5} $ mmHg. An increase in the pressure is found to result in an increase in the bulk oxidation degree of the film. The growth kinetics of the film is two-stage. The initial oxidation stage can approximately be described with a linear-logarithmic dependence. The thinner the deposited iron nanolayer, the higher the bulk oxidation degree. The large value of the rate of initial oxidation of freshly deposited layer at a pressure of $ 10^{−5} $ mmHg, can be related to redox processes at the magnetite-hematite interfaces of multilayer nanoparticles that constitute the deposited nanocomposite layer. Upon passivation of the layer, the inherent nanoporosity makes the metal-oxide nanocomposite an adsorbent that can accumulate and store the adsorbed components of the environment (air).
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title_short	Vacuum oxidation of freshly deposited iron nanofilms
url	https://dx.doi.org/10.1134/S2070205113040072
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author2	Petrunin, M. A. Maksaeva, L. B. Timofeeva, V. A. Tsivadze, A. Yu
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