Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction

Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was charact...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Rahbari, Zahra Vosoughi [verfasserIn] Khosravan, Mehrji [verfasserIn] Kharat, Ali Nemati [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2017

Übergeordnetes Werk:	Enthalten in: Russian journal of applied chemistry - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1996, 90(2017), 5 vom: Mai, Seite 818-825
Übergeordnetes Werk:	volume:90 ; year:2017 ; number:5 ; month:05 ; pages:818-825

Links:	Volltext

DOI / URN:	10.1134/S107042721705024X

Katalog-ID:	SPR017248892

Internformat


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520			\|a Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio.
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allfields	10.1134/S107042721705024X doi (DE-627)SPR017248892 (SPR)S107042721705024X-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl 58.10 bkl 58.00 bkl Rahbari, Zahra Vosoughi verfasserin aut Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio. Khosravan, Mehrji verfasserin aut Kharat, Ali Nemati verfasserin aut Enthalten in Russian journal of applied chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V, 1996 90(2017), 5 vom: Mai, Seite 818-825 (DE-627)336798393 (DE-600)2061899-2 1608-3296 nnns volume:90 year:2017 number:5 month:05 pages:818-825 https://dx.doi.org/10.1134/S107042721705024X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE 58.10 ASE 58.00 ASE AR 90 2017 5 05 818-825
spelling	10.1134/S107042721705024X doi (DE-627)SPR017248892 (SPR)S107042721705024X-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl 58.10 bkl 58.00 bkl Rahbari, Zahra Vosoughi verfasserin aut Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio. Khosravan, Mehrji verfasserin aut Kharat, Ali Nemati verfasserin aut Enthalten in Russian journal of applied chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V, 1996 90(2017), 5 vom: Mai, Seite 818-825 (DE-627)336798393 (DE-600)2061899-2 1608-3296 nnns volume:90 year:2017 number:5 month:05 pages:818-825 https://dx.doi.org/10.1134/S107042721705024X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE 58.10 ASE 58.00 ASE AR 90 2017 5 05 818-825
allfields_unstemmed	10.1134/S107042721705024X doi (DE-627)SPR017248892 (SPR)S107042721705024X-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl 58.10 bkl 58.00 bkl Rahbari, Zahra Vosoughi verfasserin aut Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio. Khosravan, Mehrji verfasserin aut Kharat, Ali Nemati verfasserin aut Enthalten in Russian journal of applied chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V, 1996 90(2017), 5 vom: Mai, Seite 818-825 (DE-627)336798393 (DE-600)2061899-2 1608-3296 nnns volume:90 year:2017 number:5 month:05 pages:818-825 https://dx.doi.org/10.1134/S107042721705024X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE 58.10 ASE 58.00 ASE AR 90 2017 5 05 818-825
allfieldsGer	10.1134/S107042721705024X doi (DE-627)SPR017248892 (SPR)S107042721705024X-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl 58.10 bkl 58.00 bkl Rahbari, Zahra Vosoughi verfasserin aut Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio. Khosravan, Mehrji verfasserin aut Kharat, Ali Nemati verfasserin aut Enthalten in Russian journal of applied chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V, 1996 90(2017), 5 vom: Mai, Seite 818-825 (DE-627)336798393 (DE-600)2061899-2 1608-3296 nnns volume:90 year:2017 number:5 month:05 pages:818-825 https://dx.doi.org/10.1134/S107042721705024X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE 58.10 ASE 58.00 ASE AR 90 2017 5 05 818-825
allfieldsSound	10.1134/S107042721705024X doi (DE-627)SPR017248892 (SPR)S107042721705024X-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl 58.10 bkl 58.00 bkl Rahbari, Zahra Vosoughi verfasserin aut Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio. Khosravan, Mehrji verfasserin aut Kharat, Ali Nemati verfasserin aut Enthalten in Russian journal of applied chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V, 1996 90(2017), 5 vom: Mai, Seite 818-825 (DE-627)336798393 (DE-600)2061899-2 1608-3296 nnns volume:90 year:2017 number:5 month:05 pages:818-825 https://dx.doi.org/10.1134/S107042721705024X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE 58.10 ASE 58.00 ASE AR 90 2017 5 05 818-825
language	English
source	Enthalten in Russian journal of applied chemistry 90(2017), 5 vom: Mai, Seite 818-825 volume:90 year:2017 number:5 month:05 pages:818-825
sourceStr	Enthalten in Russian journal of applied chemistry 90(2017), 5 vom: Mai, Seite 818-825 volume:90 year:2017 number:5 month:05 pages:818-825
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container_title	Russian journal of applied chemistry
authorswithroles_txt_mv	Rahbari, Zahra Vosoughi @@aut@@ Khosravan, Mehrji @@aut@@ Kharat, Ali Nemati @@aut@@
publishDateDaySort_date	2017-05-01T00:00:00Z
hierarchy_top_id	336798393
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The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. 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author	Rahbari, Zahra Vosoughi
spellingShingle	Rahbari, Zahra Vosoughi ddc 540 bkl 35.00 bkl 58.10 bkl 58.00 Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction
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topic_title	540 ASE 35.00 bkl 58.10 bkl 58.00 bkl Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction
topic	ddc 540 bkl 35.00 bkl 58.10 bkl 58.00
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title	Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction
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title_full	Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction
author_sort	Rahbari, Zahra Vosoughi
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author_browse	Rahbari, Zahra Vosoughi Khosravan, Mehrji Kharat, Ali Nemati
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author-letter	Rahbari, Zahra Vosoughi
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title_sort	effect of synthesis parameters on the crystallinity of eu-1 zeolite for the m-xylene isomerization reaction
title_auth	Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction
abstract	Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio.
abstractGer	Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio.
abstract_unstemmed	Abstract The EU-1 zeolite with Si/Al = 25 was synthesized by hexamethonium bromide as a template. The effects of crystallization time, synthesis temperature, and the pH of the synthesis gel on the structure and crystallinity of EU-1 zeolite were investigated. The synthesized EU-1 zeolite was characterized by X-ray powder diffraction, BET, Fourier transforms infrared spectroscopy, scanning electron microscope, and inductively coupled plasma. The most effective conditions for synthesis of EU-1 were identified as follow: synthesis time 72 h, temperature 200°C, pH of gel ≃ 13, and aging time of 12 h. The catalytic performance of this catalyst was investigated for meta-xylene isomerization reaction in a fixed bed reactor under the following conditions: pressure of 10 bars, the temperature of 380°C, feed space velocity of 3.35 $ h^{–1} $ and 4 g of the EU-1 catalyst. In comparison to other reported catalysts our synthetic EU-1 showed good m-xylene conversion and high PX/OX ratio.
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container_issue	5
title_short	Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction
url	https://dx.doi.org/10.1134/S107042721705024X
remote_bool	true
author2	Khosravan, Mehrji Kharat, Ali Nemati
author2Str	Khosravan, Mehrji Kharat, Ali Nemati
ppnlink	336798393
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isOA_txt	false
hochschulschrift_bool	false
doi_str	10.1134/S107042721705024X
up_date	2024-07-04T02:43:21.106Z
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Effect of synthesis parameters on the crystallinity of EU-1 zeolite for the m-xylene isomerization reaction

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