Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry
Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain struc...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Brodskii, E. S. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2014 |
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| Schlagwörter: |
group type composition of heavy distillates and residual petroleum products |
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| Anmerkung: |
© Pleiades Publishing, Ltd. 2014 |
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| Übergeordnetes Werk: |
Enthalten in: Petroleum chemistry - Berlin : Springer, 1962, 54(2014), 1 vom: Jan., Seite 28-36 |
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| Übergeordnetes Werk: |
volume:54 ; year:2014 ; number:1 ; month:01 ; pages:28-36 |
| Links: |
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| DOI / URN: |
10.1134/S0965544114010022 |
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SPR02019031X |
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| 520 | |a Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. | ||
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| 700 | 1 | |a Zhil’nikov, V. G. |4 aut | |
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10.1134/S0965544114010022 doi (DE-627)SPR02019031X (SPR)S0965544114010022-e DE-627 ger DE-627 rakwb eng Brodskii, E. S. verfasserin aut Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2014 Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. group type composition of heavy distillates and residual petroleum products (dpeaa)DE-He213 gas chromatography/mass spectrometry (dpeaa)DE-He213 three-dimensional chromatographic peaks (dpeaa)DE-He213 Shelepchikov, A. A. aut Kalinkevich, G. A. aut Mir-Kadyrova, E. Ya. aut Zhil’nikov, V. G. aut Enthalten in Petroleum chemistry Berlin : Springer, 1962 54(2014), 1 vom: Jan., Seite 28-36 (DE-627)331503778 (DE-600)2051391-4 1555-6239 nnns volume:54 year:2014 number:1 month:01 pages:28-36 https://dx.doi.org/10.1134/S0965544114010022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 54 2014 1 01 28-36 |
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10.1134/S0965544114010022 doi (DE-627)SPR02019031X (SPR)S0965544114010022-e DE-627 ger DE-627 rakwb eng Brodskii, E. S. verfasserin aut Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2014 Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. group type composition of heavy distillates and residual petroleum products (dpeaa)DE-He213 gas chromatography/mass spectrometry (dpeaa)DE-He213 three-dimensional chromatographic peaks (dpeaa)DE-He213 Shelepchikov, A. A. aut Kalinkevich, G. A. aut Mir-Kadyrova, E. Ya. aut Zhil’nikov, V. G. aut Enthalten in Petroleum chemistry Berlin : Springer, 1962 54(2014), 1 vom: Jan., Seite 28-36 (DE-627)331503778 (DE-600)2051391-4 1555-6239 nnns volume:54 year:2014 number:1 month:01 pages:28-36 https://dx.doi.org/10.1134/S0965544114010022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 54 2014 1 01 28-36 |
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10.1134/S0965544114010022 doi (DE-627)SPR02019031X (SPR)S0965544114010022-e DE-627 ger DE-627 rakwb eng Brodskii, E. S. verfasserin aut Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2014 Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. group type composition of heavy distillates and residual petroleum products (dpeaa)DE-He213 gas chromatography/mass spectrometry (dpeaa)DE-He213 three-dimensional chromatographic peaks (dpeaa)DE-He213 Shelepchikov, A. A. aut Kalinkevich, G. A. aut Mir-Kadyrova, E. Ya. aut Zhil’nikov, V. G. aut Enthalten in Petroleum chemistry Berlin : Springer, 1962 54(2014), 1 vom: Jan., Seite 28-36 (DE-627)331503778 (DE-600)2051391-4 1555-6239 nnns volume:54 year:2014 number:1 month:01 pages:28-36 https://dx.doi.org/10.1134/S0965544114010022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 54 2014 1 01 28-36 |
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10.1134/S0965544114010022 doi (DE-627)SPR02019031X (SPR)S0965544114010022-e DE-627 ger DE-627 rakwb eng Brodskii, E. S. verfasserin aut Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2014 Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. group type composition of heavy distillates and residual petroleum products (dpeaa)DE-He213 gas chromatography/mass spectrometry (dpeaa)DE-He213 three-dimensional chromatographic peaks (dpeaa)DE-He213 Shelepchikov, A. A. aut Kalinkevich, G. A. aut Mir-Kadyrova, E. Ya. aut Zhil’nikov, V. G. aut Enthalten in Petroleum chemistry Berlin : Springer, 1962 54(2014), 1 vom: Jan., Seite 28-36 (DE-627)331503778 (DE-600)2051391-4 1555-6239 nnns volume:54 year:2014 number:1 month:01 pages:28-36 https://dx.doi.org/10.1134/S0965544114010022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 54 2014 1 01 28-36 |
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10.1134/S0965544114010022 doi (DE-627)SPR02019031X (SPR)S0965544114010022-e DE-627 ger DE-627 rakwb eng Brodskii, E. S. verfasserin aut Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2014 Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. group type composition of heavy distillates and residual petroleum products (dpeaa)DE-He213 gas chromatography/mass spectrometry (dpeaa)DE-He213 three-dimensional chromatographic peaks (dpeaa)DE-He213 Shelepchikov, A. A. aut Kalinkevich, G. A. aut Mir-Kadyrova, E. Ya. aut Zhil’nikov, V. G. aut Enthalten in Petroleum chemistry Berlin : Springer, 1962 54(2014), 1 vom: Jan., Seite 28-36 (DE-627)331503778 (DE-600)2051391-4 1555-6239 nnns volume:54 year:2014 number:1 month:01 pages:28-36 https://dx.doi.org/10.1134/S0965544114010022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 54 2014 1 01 28-36 |
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Enthalten in Petroleum chemistry 54(2014), 1 vom: Jan., Seite 28-36 volume:54 year:2014 number:1 month:01 pages:28-36 |
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Brodskii, E. S. @@aut@@ Shelepchikov, A. A. @@aut@@ Kalinkevich, G. A. @@aut@@ Mir-Kadyrova, E. Ya. @@aut@@ Zhil’nikov, V. G. @@aut@@ |
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| author |
Brodskii, E. S. |
| spellingShingle |
Brodskii, E. S. misc group type composition of heavy distillates and residual petroleum products misc gas chromatography/mass spectrometry misc three-dimensional chromatographic peaks Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry |
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Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry group type composition of heavy distillates and residual petroleum products (dpeaa)DE-He213 gas chromatography/mass spectrometry (dpeaa)DE-He213 three-dimensional chromatographic peaks (dpeaa)DE-He213 |
| topic |
misc group type composition of heavy distillates and residual petroleum products misc gas chromatography/mass spectrometry misc three-dimensional chromatographic peaks |
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misc group type composition of heavy distillates and residual petroleum products misc gas chromatography/mass spectrometry misc three-dimensional chromatographic peaks |
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misc group type composition of heavy distillates and residual petroleum products misc gas chromatography/mass spectrometry misc three-dimensional chromatographic peaks |
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Elektronische Aufsätze Aufsätze Elektronische Ressource |
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Petroleum chemistry |
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Petroleum chemistry |
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Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry |
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(DE-627)SPR02019031X (SPR)S0965544114010022-e |
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Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry |
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Brodskii, E. S. |
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Petroleum chemistry |
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Petroleum chemistry |
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eng |
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2014 |
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Brodskii, E. S. Shelepchikov, A. A. Kalinkevich, G. A. Mir-Kadyrova, E. Ya. Zhil’nikov, V. G. |
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Elektronische Aufsätze |
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Brodskii, E. S. |
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10.1134/S0965544114010022 |
| title_sort |
type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry |
| title_auth |
Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry |
| abstract |
Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. © Pleiades Publishing, Ltd. 2014 |
| abstractGer |
Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. © Pleiades Publishing, Ltd. 2014 |
| abstract_unstemmed |
Abstract The potential use of gas chromatography/electron ionization mass spectrometry with high-energy electrons for detailed type analysis of heavy distillates and residual petroleum products has been shown. The method is based on the selection of characteristic ions corresponding to certain structural groups in the mass spectra presented as tables of homologous-series ions. In a set of ion mass chromatograms of a homologous series, these ions produce chromatographic peaks that can be represented as sections of a certain three-dimensional pseudo-peak. These three-dimensional peaks characterize both mass and retention time intervals for characteristic ions of compounds of a particular type. The overlap of the characteristic ion peaks of a given type of compounds with other types is much less than in the absence of chromatographic separation, since it is limited to compounds that elute in the given interval of retention times. The contribution of each group of compounds to the total ion current is determined from the sum of abundances of characteristic ions with allowance for the overlap of the mass spectra and differences in the ionization efficiency. The type analysis by this method can be performed without preliminary separation into saturates and aromatics. © Pleiades Publishing, Ltd. 2014 |
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Type analysis of petroleum heavy distillates and residua by gas chromatography/mass spectrometry |
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https://dx.doi.org/10.1134/S0965544114010022 |
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Shelepchikov, A. A. Kalinkevich, G. A. Mir-Kadyrova, E. Ya Zhil’nikov, V. G. |
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Shelepchikov, A. A. Kalinkevich, G. A. Mir-Kadyrova, E. Ya Zhil’nikov, V. G. |
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10.1134/S0965544114010022 |
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2024-07-03T14:27:39.674Z |
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| score |
7.4007177 |