Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)

Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a digly...
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Autor*in:	Titov, L. V. [verfasserIn] Gavrilova, L. A. Petrovskii, P. V.

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2008

Schlagwörter:	Neodymium Alkali Metal Salt Diglyme Sodium Tetrahydroborate Hydride Hydrogen

Anmerkung:	© MAIK Nauka 2008

Übergeordnetes Werk:	Enthalten in: Russian journal of inorganic chemistry - Moscow : MAIK Nauka/Interperiodica Publ., 2006, 53(2008), 4 vom: Apr., Seite 565-567
Übergeordnetes Werk:	volume:53 ; year:2008 ; number:4 ; month:04 ; pages:565-567

Links:	Volltext

DOI / URN:	10.1134/S0036023608040141

Katalog-ID:	SPR02028442X

Internformat


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100	1		\|a Titov, L. V. \|e verfasserin \|4 aut
245	1	0	\|a Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)
264		1	\|c 2008
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520			\|a Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm).
650		4	\|a Neodymium \|7 (dpeaa)DE-He213
650		4	\|a Alkali Metal Salt \|7 (dpeaa)DE-He213
650		4	\|a Diglyme \|7 (dpeaa)DE-He213
650		4	\|a Sodium Tetrahydroborate \|7 (dpeaa)DE-He213
650		4	\|a Hydride Hydrogen \|7 (dpeaa)DE-He213
700	1		\|a Gavrilova, L. A. \|4 aut
700	1		\|a Petrovskii, P. V. \|4 aut
773	0	8	\|i Enthalten in \|t Russian journal of inorganic chemistry \|d Moscow : MAIK Nauka/Interperiodica Publ., 2006 \|g 53(2008), 4 vom: Apr., Seite 565-567 \|w (DE-627)508334675 \|w (DE-600)2223897-9 \|x 1531-8613 \|7 nnns
773	1	8	\|g volume:53 \|g year:2008 \|g number:4 \|g month:04 \|g pages:565-567
856	4	0	\|u https://dx.doi.org/10.1134/S0036023608040141 \|z lizenzpflichtig \|3 Volltext
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912			\|a GBV_ILN_23
912			\|a GBV_ILN_24
912			\|a GBV_ILN_31
912			\|a GBV_ILN_32
912			\|a GBV_ILN_39
912			\|a GBV_ILN_40
912			\|a GBV_ILN_60
912			\|a GBV_ILN_62
912			\|a GBV_ILN_63
912			\|a GBV_ILN_65
912			\|a GBV_ILN_69
912			\|a GBV_ILN_70
912			\|a GBV_ILN_73
912			\|a GBV_ILN_74
912			\|a GBV_ILN_90
912			\|a GBV_ILN_95
912			\|a GBV_ILN_100
912			\|a GBV_ILN_101
912			\|a GBV_ILN_105
912			\|a GBV_ILN_110
912			\|a GBV_ILN_120
912			\|a GBV_ILN_138
912			\|a GBV_ILN_150
912			\|a GBV_ILN_151
912			\|a GBV_ILN_152
912			\|a GBV_ILN_161
912			\|a GBV_ILN_170
912			\|a GBV_ILN_171
912			\|a GBV_ILN_187
912			\|a GBV_ILN_213
912			\|a GBV_ILN_224
912			\|a GBV_ILN_230
912			\|a GBV_ILN_250
912			\|a GBV_ILN_281
912			\|a GBV_ILN_285
912			\|a GBV_ILN_293
912			\|a GBV_ILN_370
912			\|a GBV_ILN_602
912			\|a GBV_ILN_636
912			\|a GBV_ILN_702
912			\|a GBV_ILN_2001
912			\|a GBV_ILN_2003
912			\|a GBV_ILN_2004
912			\|a GBV_ILN_2005
912			\|a GBV_ILN_2006
912			\|a GBV_ILN_2007
912			\|a GBV_ILN_2008
912			\|a GBV_ILN_2009
912			\|a GBV_ILN_2010
912			\|a GBV_ILN_2011
912			\|a GBV_ILN_2014
912			\|a GBV_ILN_2015
912			\|a GBV_ILN_2020
912			\|a GBV_ILN_2021
912			\|a GBV_ILN_2025
912			\|a GBV_ILN_2026
912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2031
912			\|a GBV_ILN_2034
912			\|a GBV_ILN_2037
912			\|a GBV_ILN_2038
912			\|a GBV_ILN_2039
912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2050
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2057
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
912			\|a GBV_ILN_2064
912			\|a GBV_ILN_2065
912			\|a GBV_ILN_2068
912			\|a GBV_ILN_2070
912			\|a GBV_ILN_2086
912			\|a GBV_ILN_2088
912			\|a GBV_ILN_2093
912			\|a GBV_ILN_2106
912			\|a GBV_ILN_2107
912			\|a GBV_ILN_2108
912			\|a GBV_ILN_2110
912			\|a GBV_ILN_2111
912			\|a GBV_ILN_2112
912			\|a GBV_ILN_2113
912			\|a GBV_ILN_2116
912			\|a GBV_ILN_2118
912			\|a GBV_ILN_2119
912			\|a GBV_ILN_2122
912			\|a GBV_ILN_2129
912			\|a GBV_ILN_2143
912			\|a GBV_ILN_2144
912			\|a GBV_ILN_2147
912			\|a GBV_ILN_2148
912			\|a GBV_ILN_2152
912			\|a GBV_ILN_2153
912			\|a GBV_ILN_2188
912			\|a GBV_ILN_2190
912			\|a GBV_ILN_2232
912			\|a GBV_ILN_2336
912			\|a GBV_ILN_2446
912			\|a GBV_ILN_2470
912			\|a GBV_ILN_2472
912			\|a GBV_ILN_2507
912			\|a GBV_ILN_2522
912			\|a GBV_ILN_2548
912			\|a GBV_ILN_4035
912			\|a GBV_ILN_4037
912			\|a GBV_ILN_4046
912			\|a GBV_ILN_4112
912			\|a GBV_ILN_4125
912			\|a GBV_ILN_4242
912			\|a GBV_ILN_4246
912			\|a GBV_ILN_4249
912			\|a GBV_ILN_4251
912			\|a GBV_ILN_4305
912			\|a GBV_ILN_4306
912			\|a GBV_ILN_4307
912			\|a GBV_ILN_4313
912			\|a GBV_ILN_4322
912			\|a GBV_ILN_4323
912			\|a GBV_ILN_4324
912			\|a GBV_ILN_4325
912			\|a GBV_ILN_4326
912			\|a GBV_ILN_4333
912			\|a GBV_ILN_4334
912			\|a GBV_ILN_4335
912			\|a GBV_ILN_4336
912			\|a GBV_ILN_4338
912			\|a GBV_ILN_4393
912			\|a GBV_ILN_4700
951			\|a AR
952			\|d 53 \|j 2008 \|e 4 \|c 04 \|h 565-567

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author_variant	l v t lv lvt l a g la lag p v p pv pvp
matchkey_str	article:15318613:2008----::yteiadoerprisfd_1_4
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allfields	10.1134/S0036023608040141 doi (DE-627)SPR02028442X (SPR)S0036023608040141-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme) 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © MAIK Nauka 2008 Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm). Neodymium (dpeaa)DE-He213 Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Hydride Hydrogen (dpeaa)DE-He213 Gavrilova, L. A. aut Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 53(2008), 4 vom: Apr., Seite 565-567 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:53 year:2008 number:4 month:04 pages:565-567 https://dx.doi.org/10.1134/S0036023608040141 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 53 2008 4 04 565-567
spelling	10.1134/S0036023608040141 doi (DE-627)SPR02028442X (SPR)S0036023608040141-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme) 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © MAIK Nauka 2008 Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm). Neodymium (dpeaa)DE-He213 Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Hydride Hydrogen (dpeaa)DE-He213 Gavrilova, L. A. aut Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 53(2008), 4 vom: Apr., Seite 565-567 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:53 year:2008 number:4 month:04 pages:565-567 https://dx.doi.org/10.1134/S0036023608040141 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 53 2008 4 04 565-567
allfields_unstemmed	10.1134/S0036023608040141 doi (DE-627)SPR02028442X (SPR)S0036023608040141-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme) 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © MAIK Nauka 2008 Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm). Neodymium (dpeaa)DE-He213 Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Hydride Hydrogen (dpeaa)DE-He213 Gavrilova, L. A. aut Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 53(2008), 4 vom: Apr., Seite 565-567 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:53 year:2008 number:4 month:04 pages:565-567 https://dx.doi.org/10.1134/S0036023608040141 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 53 2008 4 04 565-567
allfieldsGer	10.1134/S0036023608040141 doi (DE-627)SPR02028442X (SPR)S0036023608040141-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme) 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © MAIK Nauka 2008 Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm). Neodymium (dpeaa)DE-He213 Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Hydride Hydrogen (dpeaa)DE-He213 Gavrilova, L. A. aut Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 53(2008), 4 vom: Apr., Seite 565-567 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:53 year:2008 number:4 month:04 pages:565-567 https://dx.doi.org/10.1134/S0036023608040141 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 53 2008 4 04 565-567
allfieldsSound	10.1134/S0036023608040141 doi (DE-627)SPR02028442X (SPR)S0036023608040141-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme) 2008 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © MAIK Nauka 2008 Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm). Neodymium (dpeaa)DE-He213 Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Hydride Hydrogen (dpeaa)DE-He213 Gavrilova, L. A. aut Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 53(2008), 4 vom: Apr., Seite 565-567 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:53 year:2008 number:4 month:04 pages:565-567 https://dx.doi.org/10.1134/S0036023608040141 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 53 2008 4 04 565-567
language	English
source	Enthalten in Russian journal of inorganic chemistry 53(2008), 4 vom: Apr., Seite 565-567 volume:53 year:2008 number:4 month:04 pages:565-567
sourceStr	Enthalten in Russian journal of inorganic chemistry 53(2008), 4 vom: Apr., Seite 565-567 volume:53 year:2008 number:4 month:04 pages:565-567
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Neodymium Alkali Metal Salt Diglyme Sodium Tetrahydroborate Hydride Hydrogen
isfreeaccess_bool	false
container_title	Russian journal of inorganic chemistry
authorswithroles_txt_mv	Titov, L. V. @@aut@@ Gavrilova, L. A. @@aut@@ Petrovskii, P. V. @@aut@@
publishDateDaySort_date	2008-04-01T00:00:00Z
hierarchy_top_id	508334675
id	SPR02028442X
language_de	englisch
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author	Titov, L. V.
spellingShingle	Titov, L. V. misc Neodymium misc Alkali Metal Salt misc Diglyme misc Sodium Tetrahydroborate misc Hydride Hydrogen Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)
authorStr	Titov, L. V.
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topic_title	Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme) Neodymium (dpeaa)DE-He213 Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Hydride Hydrogen (dpeaa)DE-He213
topic	misc Neodymium misc Alkali Metal Salt misc Diglyme misc Sodium Tetrahydroborate misc Hydride Hydrogen
topic_unstemmed	misc Neodymium misc Alkali Metal Salt misc Diglyme misc Sodium Tetrahydroborate misc Hydride Hydrogen
topic_browse	misc Neodymium misc Alkali Metal Salt misc Diglyme misc Sodium Tetrahydroborate misc Hydride Hydrogen
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title	Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)
ctrlnum	(DE-627)SPR02028442X (SPR)S0036023608040141-e
title_full	Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)
author_sort	Titov, L. V.
journal	Russian journal of inorganic chemistry
journalStr	Russian journal of inorganic chemistry
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author_browse	Titov, L. V. Gavrilova, L. A. Petrovskii, P. V.
container_volume	53
format_se	Elektronische Aufsätze
author-letter	Titov, L. V.
doi_str_mv	10.1134/S0036023608040141
title_sort	synthesis and some properties of nd($ b_{11} %$ h_{14} $)3 · 4dg (dg is diglyme)
title_auth	Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)
abstract	Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm). © MAIK Nauka 2008
abstractGer	Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm). © MAIK Nauka 2008
abstract_unstemmed	Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm). © MAIK Nauka 2008
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container_issue	4
title_short	Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)
url	https://dx.doi.org/10.1134/S0036023608040141
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author2	Gavrilova, L. A. Petrovskii, P. V.
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up_date	2024-07-03T15:04:23.878Z
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V.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2008</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© MAIK Nauka 2008</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract The reaction of Nd($ BH_{4} $)3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd($ B_{11} %$ H_{14} $)3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd($ BH_{4} $)3 · 3THF to $ B_{10} %$ H_{14} $ is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an inert atmosphere, Nd($ B_{11} %$ H_{14} $)3 · 4Dg is stable to 150°C and decomposes with an exotherm at 160–190°C. The IR spectrum of Nd($ B_{11} %$ H_{14} $)3 · 4Dg in the region of B-H stretching vibrations contains an intense band at 2530 $ cm^{−1} $. The 11B {1H} NMR spectra of the synthesized compound in diglyme solutions contain signals of the tetradecahydro-nido-undecaborate anion $ B_{11} $H14− (δ = -14.0, -15.6, and -16.5 ppm).</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Neodymium</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Alkali Metal Salt</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Diglyme</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Sodium Tetrahydroborate</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Hydride Hydrogen</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Gavrilova, L. 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Synthesis and some properties of Nd($ B_{11} %$ H_{14} $)3 · 4Dg (Dg is diglyme)

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