Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)

Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis....
Ausführliche Beschreibung

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Autor*in:	Taydakov, I. V. [verfasserIn] Zaitsev, B. E. Krasnosel’sky, S. S. Polyakova, I. N. Sergienko, V. S.

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2011

Schlagwörter:	Pyrazol Complex Anion Pyrazol Ring APEX2 Automatic Diffractometer Diketonate Moiety

Anmerkung:	© Pleiades Publishing, Ltd. 2011

Übergeordnetes Werk:	Enthalten in: Russian journal of inorganic chemistry - Moscow : MAIK Nauka/Interperiodica Publ., 2006, 56(2011), 3 vom: März, Seite 345-349
Übergeordnetes Werk:	volume:56 ; year:2011 ; number:3 ; month:03 ; pages:345-349

Links:	Volltext

DOI / URN:	10.1134/S0036023611030211

Katalog-ID:	SPR020295065

Internformat


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100	1		\|a Taydakov, I. V. \|e verfasserin \|4 aut
245	1	0	\|a Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)
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520			\|a Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $.
650		4	\|a Pyrazol \|7 (dpeaa)DE-He213
650		4	\|a Complex Anion \|7 (dpeaa)DE-He213
650		4	\|a Pyrazol Ring \|7 (dpeaa)DE-He213
650		4	\|a APEX2 Automatic Diffractometer \|7 (dpeaa)DE-He213
650		4	\|a Diketonate Moiety \|7 (dpeaa)DE-He213
700	1		\|a Zaitsev, B. E. \|4 aut
700	1		\|a Krasnosel’sky, S. S. \|4 aut
700	1		\|a Polyakova, I. N. \|4 aut
700	1		\|a Sergienko, V. S. \|4 aut
773	0	8	\|i Enthalten in \|t Russian journal of inorganic chemistry \|d Moscow : MAIK Nauka/Interperiodica Publ., 2006 \|g 56(2011), 3 vom: März, Seite 345-349 \|w (DE-627)508334675 \|w (DE-600)2223897-9 \|x 1531-8613 \|7 nnns
773	1	8	\|g volume:56 \|g year:2011 \|g number:3 \|g month:03 \|g pages:345-349
856	4	0	\|u https://dx.doi.org/10.1134/S0036023611030211 \|z lizenzpflichtig \|3 Volltext
912			\|a GBV_USEFLAG_A
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912			\|a GBV_ILN_20
912			\|a GBV_ILN_22
912			\|a GBV_ILN_23
912			\|a GBV_ILN_24
912			\|a GBV_ILN_31
912			\|a GBV_ILN_32
912			\|a GBV_ILN_39
912			\|a GBV_ILN_40
912			\|a GBV_ILN_60
912			\|a GBV_ILN_62
912			\|a GBV_ILN_63
912			\|a GBV_ILN_65
912			\|a GBV_ILN_69
912			\|a GBV_ILN_70
912			\|a GBV_ILN_73
912			\|a GBV_ILN_74
912			\|a GBV_ILN_90
912			\|a GBV_ILN_95
912			\|a GBV_ILN_100
912			\|a GBV_ILN_101
912			\|a GBV_ILN_105
912			\|a GBV_ILN_110
912			\|a GBV_ILN_120
912			\|a GBV_ILN_138
912			\|a GBV_ILN_150
912			\|a GBV_ILN_151
912			\|a GBV_ILN_152
912			\|a GBV_ILN_161
912			\|a GBV_ILN_170
912			\|a GBV_ILN_171
912			\|a GBV_ILN_187
912			\|a GBV_ILN_213
912			\|a GBV_ILN_224
912			\|a GBV_ILN_230
912			\|a GBV_ILN_250
912			\|a GBV_ILN_281
912			\|a GBV_ILN_285
912			\|a GBV_ILN_293
912			\|a GBV_ILN_370
912			\|a GBV_ILN_602
912			\|a GBV_ILN_636
912			\|a GBV_ILN_702
912			\|a GBV_ILN_2001
912			\|a GBV_ILN_2003
912			\|a GBV_ILN_2004
912			\|a GBV_ILN_2005
912			\|a GBV_ILN_2006
912			\|a GBV_ILN_2007
912			\|a GBV_ILN_2008
912			\|a GBV_ILN_2009
912			\|a GBV_ILN_2010
912			\|a GBV_ILN_2011
912			\|a GBV_ILN_2014
912			\|a GBV_ILN_2015
912			\|a GBV_ILN_2020
912			\|a GBV_ILN_2021
912			\|a GBV_ILN_2025
912			\|a GBV_ILN_2026
912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2031
912			\|a GBV_ILN_2034
912			\|a GBV_ILN_2037
912			\|a GBV_ILN_2038
912			\|a GBV_ILN_2039
912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2050
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2057
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
912			\|a GBV_ILN_2064
912			\|a GBV_ILN_2065
912			\|a GBV_ILN_2068
912			\|a GBV_ILN_2070
912			\|a GBV_ILN_2086
912			\|a GBV_ILN_2088
912			\|a GBV_ILN_2093
912			\|a GBV_ILN_2106
912			\|a GBV_ILN_2107
912			\|a GBV_ILN_2108
912			\|a GBV_ILN_2110
912			\|a GBV_ILN_2111
912			\|a GBV_ILN_2112
912			\|a GBV_ILN_2113
912			\|a GBV_ILN_2116
912			\|a GBV_ILN_2118
912			\|a GBV_ILN_2119
912			\|a GBV_ILN_2122
912			\|a GBV_ILN_2129
912			\|a GBV_ILN_2143
912			\|a GBV_ILN_2144
912			\|a GBV_ILN_2147
912			\|a GBV_ILN_2148
912			\|a GBV_ILN_2152
912			\|a GBV_ILN_2153
912			\|a GBV_ILN_2188
912			\|a GBV_ILN_2190
912			\|a GBV_ILN_2232
912			\|a GBV_ILN_2336
912			\|a GBV_ILN_2446
912			\|a GBV_ILN_2470
912			\|a GBV_ILN_2472
912			\|a GBV_ILN_2507
912			\|a GBV_ILN_2522
912			\|a GBV_ILN_2548
912			\|a GBV_ILN_4035
912			\|a GBV_ILN_4037
912			\|a GBV_ILN_4046
912			\|a GBV_ILN_4112
912			\|a GBV_ILN_4125
912			\|a GBV_ILN_4242
912			\|a GBV_ILN_4246
912			\|a GBV_ILN_4249
912			\|a GBV_ILN_4251
912			\|a GBV_ILN_4305
912			\|a GBV_ILN_4306
912			\|a GBV_ILN_4307
912			\|a GBV_ILN_4313
912			\|a GBV_ILN_4322
912			\|a GBV_ILN_4323
912			\|a GBV_ILN_4324
912			\|a GBV_ILN_4325
912			\|a GBV_ILN_4326
912			\|a GBV_ILN_4333
912			\|a GBV_ILN_4334
912			\|a GBV_ILN_4335
912			\|a GBV_ILN_4336
912			\|a GBV_ILN_4338
912			\|a GBV_ILN_4393
912			\|a GBV_ILN_4700
951			\|a AR
952			\|d 56 \|j 2011 \|e 3 \|c 03 \|h 345-349

Indexfelder

author_variant	i v t iv ivt b e z be bez s s k ss ssk i n p in inp v s s vs vss
matchkey_str	article:15318613:2011----::yteiadrsasrcuefa_oel475h2l2l3i1dmty1
hierarchy_sort_str	2011
publishDate	2011
allfields	10.1134/S0036023611030211 doi (DE-627)SPR020295065 (SPR)S0036023611030211-e DE-627 ger DE-627 rakwb eng Taydakov, I. V. verfasserin aut Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $. Pyrazol (dpeaa)DE-He213 Complex Anion (dpeaa)DE-He213 Pyrazol Ring (dpeaa)DE-He213 APEX2 Automatic Diffractometer (dpeaa)DE-He213 Diketonate Moiety (dpeaa)DE-He213 Zaitsev, B. E. aut Krasnosel’sky, S. S. aut Polyakova, I. N. aut Sergienko, V. S. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 3 vom: März, Seite 345-349 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:3 month:03 pages:345-349 https://dx.doi.org/10.1134/S0036023611030211 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 3 03 345-349
spelling	10.1134/S0036023611030211 doi (DE-627)SPR020295065 (SPR)S0036023611030211-e DE-627 ger DE-627 rakwb eng Taydakov, I. V. verfasserin aut Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $. Pyrazol (dpeaa)DE-He213 Complex Anion (dpeaa)DE-He213 Pyrazol Ring (dpeaa)DE-He213 APEX2 Automatic Diffractometer (dpeaa)DE-He213 Diketonate Moiety (dpeaa)DE-He213 Zaitsev, B. E. aut Krasnosel’sky, S. S. aut Polyakova, I. N. aut Sergienko, V. S. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 3 vom: März, Seite 345-349 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:3 month:03 pages:345-349 https://dx.doi.org/10.1134/S0036023611030211 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 3 03 345-349
allfields_unstemmed	10.1134/S0036023611030211 doi (DE-627)SPR020295065 (SPR)S0036023611030211-e DE-627 ger DE-627 rakwb eng Taydakov, I. V. verfasserin aut Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $. Pyrazol (dpeaa)DE-He213 Complex Anion (dpeaa)DE-He213 Pyrazol Ring (dpeaa)DE-He213 APEX2 Automatic Diffractometer (dpeaa)DE-He213 Diketonate Moiety (dpeaa)DE-He213 Zaitsev, B. E. aut Krasnosel’sky, S. S. aut Polyakova, I. N. aut Sergienko, V. S. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 3 vom: März, Seite 345-349 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:3 month:03 pages:345-349 https://dx.doi.org/10.1134/S0036023611030211 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 3 03 345-349
allfieldsGer	10.1134/S0036023611030211 doi (DE-627)SPR020295065 (SPR)S0036023611030211-e DE-627 ger DE-627 rakwb eng Taydakov, I. V. verfasserin aut Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $. Pyrazol (dpeaa)DE-He213 Complex Anion (dpeaa)DE-He213 Pyrazol Ring (dpeaa)DE-He213 APEX2 Automatic Diffractometer (dpeaa)DE-He213 Diketonate Moiety (dpeaa)DE-He213 Zaitsev, B. E. aut Krasnosel’sky, S. S. aut Polyakova, I. N. aut Sergienko, V. S. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 3 vom: März, Seite 345-349 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:3 month:03 pages:345-349 https://dx.doi.org/10.1134/S0036023611030211 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 3 03 345-349
allfieldsSound	10.1134/S0036023611030211 doi (DE-627)SPR020295065 (SPR)S0036023611030211-e DE-627 ger DE-627 rakwb eng Taydakov, I. V. verfasserin aut Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $. Pyrazol (dpeaa)DE-He213 Complex Anion (dpeaa)DE-He213 Pyrazol Ring (dpeaa)DE-He213 APEX2 Automatic Diffractometer (dpeaa)DE-He213 Diketonate Moiety (dpeaa)DE-He213 Zaitsev, B. E. aut Krasnosel’sky, S. S. aut Polyakova, I. N. aut Sergienko, V. S. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 3 vom: März, Seite 345-349 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:3 month:03 pages:345-349 https://dx.doi.org/10.1134/S0036023611030211 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 3 03 345-349
language	English
source	Enthalten in Russian journal of inorganic chemistry 56(2011), 3 vom: März, Seite 345-349 volume:56 year:2011 number:3 month:03 pages:345-349
sourceStr	Enthalten in Russian journal of inorganic chemistry 56(2011), 3 vom: März, Seite 345-349 volume:56 year:2011 number:3 month:03 pages:345-349
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Pyrazol Complex Anion Pyrazol Ring APEX2 Automatic Diffractometer Diketonate Moiety
isfreeaccess_bool	false
container_title	Russian journal of inorganic chemistry
authorswithroles_txt_mv	Taydakov, I. V. @@aut@@ Zaitsev, B. E. @@aut@@ Krasnosel’sky, S. S. @@aut@@ Polyakova, I. N. @@aut@@ Sergienko, V. S. @@aut@@
publishDateDaySort_date	2011-03-01T00:00:00Z
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author	Taydakov, I. V.
spellingShingle	Taydakov, I. V. misc Pyrazol misc Complex Anion misc Pyrazol Ring misc APEX2 Automatic Diffractometer misc Diketonate Moiety Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)
authorStr	Taydakov, I. V.
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topic_title	Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione) Pyrazol (dpeaa)DE-He213 Complex Anion (dpeaa)DE-He213 Pyrazol Ring (dpeaa)DE-He213 APEX2 Automatic Diffractometer (dpeaa)DE-He213 Diketonate Moiety (dpeaa)DE-He213
topic	misc Pyrazol misc Complex Anion misc Pyrazol Ring misc APEX2 Automatic Diffractometer misc Diketonate Moiety
topic_unstemmed	misc Pyrazol misc Complex Anion misc Pyrazol Ring misc APEX2 Automatic Diffractometer misc Diketonate Moiety
topic_browse	misc Pyrazol misc Complex Anion misc Pyrazol Ring misc APEX2 Automatic Diffractometer misc Diketonate Moiety
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title	Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)
ctrlnum	(DE-627)SPR020295065 (SPR)S0036023611030211-e
title_full	Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)
author_sort	Taydakov, I. V.
journal	Russian journal of inorganic chemistry
journalStr	Russian journal of inorganic chemistry
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container_start_page	345
author_browse	Taydakov, I. V. Zaitsev, B. E. Krasnosel’sky, S. S. Polyakova, I. N. Sergienko, V. S.
container_volume	56
format_se	Elektronische Aufsätze
author-letter	Taydakov, I. V.
doi_str_mv	10.1134/S0036023611030211
title_sort	synthesis and crystal structure of [na($ h_{2} $o)4][$ eul_{4} $] · 0.$ 775ch_{2} %$ cl_{2} $ (hl = 1,3-bis(1,3-dimethyl-1h-pyrazol-4-yl)-1,3-propanedione)
title_auth	Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)
abstract	Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $. © Pleiades Publishing, Ltd. 2011
abstractGer	Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $. © Pleiades Publishing, Ltd. 2011
abstract_unstemmed	Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. The coordination polyhedron of the Eu atom is an Archimedean antiprism formed by the O atoms of four bidentate chelate ligands $ L^{−} $. © Pleiades Publishing, Ltd. 2011
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title_short	Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)
url	https://dx.doi.org/10.1134/S0036023611030211
remote_bool	true
author2	Zaitsev, B. E. Krasnosel’sky, S. S. Polyakova, I. N. Sergienko, V. S.
author2Str	Zaitsev, B. E. Krasnosel’sky, S. S. Polyakova, I. N. Sergienko, V. S.
ppnlink	508334675
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isOA_txt	false
hochschulschrift_bool	false
doi_str	10.1134/S0036023611030211
up_date	2024-07-03T15:08:28.255Z
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V.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2011</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Pleiades Publishing, Ltd. 2011</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (I) has been synthesized by the reaction of Eu($ NO_{3} $)3 · $ 6H_{2} $O with 1,3-bis(1,3-dimethyl-1H-pyrasol-4-yl)-1,3-propanedione (HL) in the presence of NaOH. Its crystal structure has been solved by X-ray diffraction analysis. Crystals are tetragonal; a = 16.2401(5) Å, c = 11.9113(4) Å, V= 3141.50(17) $ Å^{3} $, $ ρ_{calcd} $ = 1.427 g/$ cm^{3} $, μ(MoKα) = 1.140 $ mm^{−1} $, space group P4/n, Z = 2. The structural units forming a crystal of compound I are [$ EuL_{4} $]− complex anions, [Na($ H_{2} $O)4]+ cations, and $ CH_{2} %$ Cl_{2} $ molecules. 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Synthesis and crystal structure of [Na($ H_{2} $O)4][$ EuL_{4} $] · 0.$ 775CH_{2} %$ Cl_{2} $ (HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione)

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