Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme)
Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydrou...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Titov, L. V. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2011 |
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| Schlagwörter: |
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| Anmerkung: |
© Pleiades Publishing, Ltd. 2011 |
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| Übergeordnetes Werk: |
Enthalten in: Russian journal of inorganic chemistry - Moscow : MAIK Nauka/Interperiodica Publ., 2006, 56(2011), 7 vom: Juli, Seite 1032-1033 |
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| Übergeordnetes Werk: |
volume:56 ; year:2011 ; number:7 ; month:07 ; pages:1032-1033 |
| Links: |
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| DOI / URN: |
10.1134/S0036023611070308 |
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| Katalog-ID: |
SPR020296231 |
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| 100 | 1 | |a Titov, L. V. |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) |
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| 520 | |a Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. | ||
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| 650 | 4 | |a Diglyme |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Sodium Tetrahydroborate |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Boron Hydride |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Yellow Oily Substance |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Petrovskii, P. V. |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Russian journal of inorganic chemistry |d Moscow : MAIK Nauka/Interperiodica Publ., 2006 |g 56(2011), 7 vom: Juli, Seite 1032-1033 |w (DE-627)508334675 |w (DE-600)2223897-9 |x 1531-8613 |7 nnns |
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10.1134/S0036023611070308 doi (DE-627)SPR020296231 (SPR)S0036023611070308-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Boron Hydride (dpeaa)DE-He213 Yellow Oily Substance (dpeaa)DE-He213 Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 7 vom: Juli, Seite 1032-1033 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:7 month:07 pages:1032-1033 https://dx.doi.org/10.1134/S0036023611070308 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 7 07 1032-1033 |
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10.1134/S0036023611070308 doi (DE-627)SPR020296231 (SPR)S0036023611070308-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Boron Hydride (dpeaa)DE-He213 Yellow Oily Substance (dpeaa)DE-He213 Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 7 vom: Juli, Seite 1032-1033 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:7 month:07 pages:1032-1033 https://dx.doi.org/10.1134/S0036023611070308 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 7 07 1032-1033 |
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10.1134/S0036023611070308 doi (DE-627)SPR020296231 (SPR)S0036023611070308-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Boron Hydride (dpeaa)DE-He213 Yellow Oily Substance (dpeaa)DE-He213 Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 7 vom: Juli, Seite 1032-1033 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:7 month:07 pages:1032-1033 https://dx.doi.org/10.1134/S0036023611070308 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 7 07 1032-1033 |
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10.1134/S0036023611070308 doi (DE-627)SPR020296231 (SPR)S0036023611070308-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Boron Hydride (dpeaa)DE-He213 Yellow Oily Substance (dpeaa)DE-He213 Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 7 vom: Juli, Seite 1032-1033 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:7 month:07 pages:1032-1033 https://dx.doi.org/10.1134/S0036023611070308 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 7 07 1032-1033 |
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10.1134/S0036023611070308 doi (DE-627)SPR020296231 (SPR)S0036023611070308-e DE-627 ger DE-627 rakwb eng Titov, L. V. verfasserin aut Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2011 Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Boron Hydride (dpeaa)DE-He213 Yellow Oily Substance (dpeaa)DE-He213 Petrovskii, P. V. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 56(2011), 7 vom: Juli, Seite 1032-1033 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:56 year:2011 number:7 month:07 pages:1032-1033 https://dx.doi.org/10.1134/S0036023611070308 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 56 2011 7 07 1032-1033 |
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Titov, L. V. |
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Titov, L. V. misc Alkali Metal Salt misc Diglyme misc Sodium Tetrahydroborate misc Boron Hydride misc Yellow Oily Substance Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) |
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Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) Alkali Metal Salt (dpeaa)DE-He213 Diglyme (dpeaa)DE-He213 Sodium Tetrahydroborate (dpeaa)DE-He213 Boron Hydride (dpeaa)DE-He213 Yellow Oily Substance (dpeaa)DE-He213 |
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misc Alkali Metal Salt misc Diglyme misc Sodium Tetrahydroborate misc Boron Hydride misc Yellow Oily Substance |
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Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) |
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Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) |
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synthesis and some properties of calcium tetradecahydroundecaborate ca($ b_{11} %$ h_{14} $)2 · 4dg (dg = diglyme) |
| title_auth |
Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) |
| abstract |
Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. © Pleiades Publishing, Ltd. 2011 |
| abstractGer |
Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. © Pleiades Publishing, Ltd. 2011 |
| abstract_unstemmed |
Abstract The reaction of Ca($ BH_{4} $)2 · 1.5Dg with decaborane-14 in diglyme at 85°C yields Ca($ B_{11} %$ H_{14} $)2 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Ca($ BH_{4} $)2 · 1.5Dg: $ B_{10} %$ H_{14} $ is 1: 3.5. The yield is 84.7%. The synthesized calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg is a stable compound soluble in water and a number of organic solvents. The study of the compound was carried out using elemental analysis and IR and NMR 11B {1H} spectroscopy. Calcium undecaborate can be used for synthesizing other salts with boron hydride nido-borates. © Pleiades Publishing, Ltd. 2011 |
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7 |
| title_short |
Synthesis and some properties of calcium tetradecahydroundecaborate Ca($ B_{11} %$ H_{14} $)2 · 4Dg (Dg = diglyme) |
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https://dx.doi.org/10.1134/S0036023611070308 |
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Petrovskii, P. V. |
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Petrovskii, P. V. |
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| doi_str |
10.1134/S0036023611070308 |
| up_date |
2024-07-03T15:09:01.807Z |
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1803571001356713984 |
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