Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6]
Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 1...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Gumbris, E. G. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2012 |
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| Schlagwörter: |
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| Anmerkung: |
© Pleiades Publishing, Ltd. 2012 |
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| Übergeordnetes Werk: |
Enthalten in: Russian journal of inorganic chemistry - Moscow : MAIK Nauka/Interperiodica Publ., 2006, 57(2012), 3 vom: März, Seite 337-342 |
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| Übergeordnetes Werk: |
volume:57 ; year:2012 ; number:3 ; month:03 ; pages:337-342 |
| Links: |
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| DOI / URN: |
10.1134/S0036023612030084 |
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| Katalog-ID: |
SPR020298366 |
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| 100 | 1 | |a Gumbris, E. G. |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] |
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| 520 | |a Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). | ||
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| 650 | 4 | |a Terpyridine |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Peresypkina, E. V. |4 aut | |
| 700 | 1 | |a Virovets, A. V. |4 aut | |
| 700 | 1 | |a Cherkasova, T. G. |4 aut | |
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10.1134/S0036023612030084 doi (DE-627)SPR020298366 (SPR)S0036023612030084-e DE-627 ger DE-627 rakwb eng Gumbris, E. G. verfasserin aut Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2012 Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). Bismuth (dpeaa)DE-He213 Acetone Solution (dpeaa)DE-He213 Cambridge Structural Database (dpeaa)DE-He213 BiOCl (dpeaa)DE-He213 Terpyridine (dpeaa)DE-He213 Peresypkina, E. V. aut Virovets, A. V. aut Cherkasova, T. G. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 57(2012), 3 vom: März, Seite 337-342 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:57 year:2012 number:3 month:03 pages:337-342 https://dx.doi.org/10.1134/S0036023612030084 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 57 2012 3 03 337-342 |
| spelling |
10.1134/S0036023612030084 doi (DE-627)SPR020298366 (SPR)S0036023612030084-e DE-627 ger DE-627 rakwb eng Gumbris, E. G. verfasserin aut Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2012 Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). Bismuth (dpeaa)DE-He213 Acetone Solution (dpeaa)DE-He213 Cambridge Structural Database (dpeaa)DE-He213 BiOCl (dpeaa)DE-He213 Terpyridine (dpeaa)DE-He213 Peresypkina, E. V. aut Virovets, A. V. aut Cherkasova, T. G. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 57(2012), 3 vom: März, Seite 337-342 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:57 year:2012 number:3 month:03 pages:337-342 https://dx.doi.org/10.1134/S0036023612030084 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 57 2012 3 03 337-342 |
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10.1134/S0036023612030084 doi (DE-627)SPR020298366 (SPR)S0036023612030084-e DE-627 ger DE-627 rakwb eng Gumbris, E. G. verfasserin aut Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2012 Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). Bismuth (dpeaa)DE-He213 Acetone Solution (dpeaa)DE-He213 Cambridge Structural Database (dpeaa)DE-He213 BiOCl (dpeaa)DE-He213 Terpyridine (dpeaa)DE-He213 Peresypkina, E. V. aut Virovets, A. V. aut Cherkasova, T. G. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 57(2012), 3 vom: März, Seite 337-342 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:57 year:2012 number:3 month:03 pages:337-342 https://dx.doi.org/10.1134/S0036023612030084 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 57 2012 3 03 337-342 |
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10.1134/S0036023612030084 doi (DE-627)SPR020298366 (SPR)S0036023612030084-e DE-627 ger DE-627 rakwb eng Gumbris, E. G. verfasserin aut Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2012 Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). Bismuth (dpeaa)DE-He213 Acetone Solution (dpeaa)DE-He213 Cambridge Structural Database (dpeaa)DE-He213 BiOCl (dpeaa)DE-He213 Terpyridine (dpeaa)DE-He213 Peresypkina, E. V. aut Virovets, A. V. aut Cherkasova, T. G. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 57(2012), 3 vom: März, Seite 337-342 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:57 year:2012 number:3 month:03 pages:337-342 https://dx.doi.org/10.1134/S0036023612030084 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 57 2012 3 03 337-342 |
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10.1134/S0036023612030084 doi (DE-627)SPR020298366 (SPR)S0036023612030084-e DE-627 ger DE-627 rakwb eng Gumbris, E. G. verfasserin aut Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2012 Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). Bismuth (dpeaa)DE-He213 Acetone Solution (dpeaa)DE-He213 Cambridge Structural Database (dpeaa)DE-He213 BiOCl (dpeaa)DE-He213 Terpyridine (dpeaa)DE-He213 Peresypkina, E. V. aut Virovets, A. V. aut Cherkasova, T. G. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 57(2012), 3 vom: März, Seite 337-342 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:57 year:2012 number:3 month:03 pages:337-342 https://dx.doi.org/10.1134/S0036023612030084 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 57 2012 3 03 337-342 |
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Enthalten in Russian journal of inorganic chemistry 57(2012), 3 vom: März, Seite 337-342 volume:57 year:2012 number:3 month:03 pages:337-342 |
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Gumbris, E. G. @@aut@@ Peresypkina, E. V. @@aut@@ Virovets, A. V. @@aut@@ Cherkasova, T. G. @@aut@@ |
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G.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6]</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2012</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Pleiades Publishing, Ltd. 2012</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). 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Gumbris, E. G. |
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Gumbris, E. G. misc Bismuth misc Acetone Solution misc Cambridge Structural Database misc BiOCl misc Terpyridine Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] |
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Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] Bismuth (dpeaa)DE-He213 Acetone Solution (dpeaa)DE-He213 Cambridge Structural Database (dpeaa)DE-He213 BiOCl (dpeaa)DE-He213 Terpyridine (dpeaa)DE-He213 |
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Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] |
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Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] |
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Gumbris, E. G. Peresypkina, E. V. Virovets, A. V. Cherkasova, T. G. |
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syntheses and crystal structures of [bi(dmso)8][fe(ncs)6] and [al(dmso)6][al(ncs)6] |
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Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] |
| abstract |
Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). © Pleiades Publishing, Ltd. 2012 |
| abstractGer |
Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). © Pleiades Publishing, Ltd. 2012 |
| abstract_unstemmed |
Abstract New complexes of composition [Bi(DMSO)8][Fe(NCS)6] (1) and [Al(DMSO)6][Al(NCS)6] (2) have been prepared, and an octahedral hexarodanoaluminate anion has been structurally characterized for the first time. Crystals of compound 1 are triclinic, space group %$P\bar 1%$, a = 11.2368(4) Å, b = 11.4063(4) Å, c = 21.0711(9) Å, α = 92.9520(10)°, β = 99.9430(10)°, γ = 111.9290(10)°, V = 2447.69(16) $ Å^{3} $, Z = 2, $ ρ_{calc} $ = 1.680 g/$ cm^{3} $, R1 = 0.0564; crystals of compound 2 are cubic, space group %$Pa\bar 3%$, a = 15.8201(4) Å, V = 3959.39(17) $ Å^{3} $, Z = 4, $ ρ_{calc} $ = 1.462 g/$ cm^{3} $, R1 = 0.0475. The bismuth coordination polyhedron $ BiO_{8} $ in compound 1 is a distorted square antiprism with broken square faces (Bi-O, 2.368-2.582 Å). In the structure of 2, the cation disordered in a complex manner has an octahedral configuration (Al-O, 1.888(11)-1.912(11) Å). © Pleiades Publishing, Ltd. 2012 |
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3 |
| title_short |
Syntheses and crystal structures of [Bi(DMSO)8][Fe(NCS)6] and [Al(DMSO)6][Al(NCS)6] |
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https://dx.doi.org/10.1134/S0036023612030084 |
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Peresypkina, E. V. Virovets, A. V. Cherkasova, T. G. |
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Peresypkina, E. V. Virovets, A. V. Cherkasova, T. G. |
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| doi_str |
10.1134/S0036023612030084 |
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2024-07-03T15:09:54.309Z |
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| score |
7.399646 |