Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices
Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Ivicheva, S. N. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Schlagwörter: |
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| Anmerkung: |
© Pleiades Publishing, Ltd. 2015 |
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| Übergeordnetes Werk: |
Enthalten in: Russian journal of inorganic chemistry - Moscow : MAIK Nauka/Interperiodica Publ., 2006, 60(2015), 11 vom: 24. Okt., Seite 1317-1328 |
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| Übergeordnetes Werk: |
volume:60 ; year:2015 ; number:11 ; day:24 ; month:10 ; pages:1317-1328 |
| Links: |
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| DOI / URN: |
10.1134/S003602361511008X |
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| Katalog-ID: |
SPR020306482 |
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| 100 | 1 | |a Ivicheva, S. N. |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices |
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| 520 | |a Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. | ||
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| 650 | 4 | |a Opal Matrix |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Opal Matrice |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Polyhydric Alcohol |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Titanium Alkoxide |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Kargin, Yu. F. |4 aut | |
| 700 | 1 | |a Kutsev, S. V. |4 aut | |
| 700 | 1 | |a Ashmarin, A. A. |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Russian journal of inorganic chemistry |d Moscow : MAIK Nauka/Interperiodica Publ., 2006 |g 60(2015), 11 vom: 24. Okt., Seite 1317-1328 |w (DE-627)508334675 |w (DE-600)2223897-9 |x 1531-8613 |7 nnns |
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10.1134/S003602361511008X doi (DE-627)SPR020306482 (SPR)S003602361511008X-e DE-627 ger DE-627 rakwb eng Ivicheva, S. N. verfasserin aut Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. Bismuth (dpeaa)DE-He213 Opal Matrix (dpeaa)DE-He213 Opal Matrice (dpeaa)DE-He213 Polyhydric Alcohol (dpeaa)DE-He213 Titanium Alkoxide (dpeaa)DE-He213 Kargin, Yu. F. aut Kutsev, S. V. aut Ashmarin, A. A. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 60(2015), 11 vom: 24. Okt., Seite 1317-1328 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:60 year:2015 number:11 day:24 month:10 pages:1317-1328 https://dx.doi.org/10.1134/S003602361511008X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 60 2015 11 24 10 1317-1328 |
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10.1134/S003602361511008X doi (DE-627)SPR020306482 (SPR)S003602361511008X-e DE-627 ger DE-627 rakwb eng Ivicheva, S. N. verfasserin aut Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. Bismuth (dpeaa)DE-He213 Opal Matrix (dpeaa)DE-He213 Opal Matrice (dpeaa)DE-He213 Polyhydric Alcohol (dpeaa)DE-He213 Titanium Alkoxide (dpeaa)DE-He213 Kargin, Yu. F. aut Kutsev, S. V. aut Ashmarin, A. A. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 60(2015), 11 vom: 24. Okt., Seite 1317-1328 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:60 year:2015 number:11 day:24 month:10 pages:1317-1328 https://dx.doi.org/10.1134/S003602361511008X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 60 2015 11 24 10 1317-1328 |
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10.1134/S003602361511008X doi (DE-627)SPR020306482 (SPR)S003602361511008X-e DE-627 ger DE-627 rakwb eng Ivicheva, S. N. verfasserin aut Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. Bismuth (dpeaa)DE-He213 Opal Matrix (dpeaa)DE-He213 Opal Matrice (dpeaa)DE-He213 Polyhydric Alcohol (dpeaa)DE-He213 Titanium Alkoxide (dpeaa)DE-He213 Kargin, Yu. F. aut Kutsev, S. V. aut Ashmarin, A. A. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 60(2015), 11 vom: 24. Okt., Seite 1317-1328 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:60 year:2015 number:11 day:24 month:10 pages:1317-1328 https://dx.doi.org/10.1134/S003602361511008X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 60 2015 11 24 10 1317-1328 |
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10.1134/S003602361511008X doi (DE-627)SPR020306482 (SPR)S003602361511008X-e DE-627 ger DE-627 rakwb eng Ivicheva, S. N. verfasserin aut Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. Bismuth (dpeaa)DE-He213 Opal Matrix (dpeaa)DE-He213 Opal Matrice (dpeaa)DE-He213 Polyhydric Alcohol (dpeaa)DE-He213 Titanium Alkoxide (dpeaa)DE-He213 Kargin, Yu. F. aut Kutsev, S. V. aut Ashmarin, A. A. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 60(2015), 11 vom: 24. Okt., Seite 1317-1328 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:60 year:2015 number:11 day:24 month:10 pages:1317-1328 https://dx.doi.org/10.1134/S003602361511008X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 60 2015 11 24 10 1317-1328 |
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10.1134/S003602361511008X doi (DE-627)SPR020306482 (SPR)S003602361511008X-e DE-627 ger DE-627 rakwb eng Ivicheva, S. N. verfasserin aut Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. Bismuth (dpeaa)DE-He213 Opal Matrix (dpeaa)DE-He213 Opal Matrice (dpeaa)DE-He213 Polyhydric Alcohol (dpeaa)DE-He213 Titanium Alkoxide (dpeaa)DE-He213 Kargin, Yu. F. aut Kutsev, S. V. aut Ashmarin, A. A. aut Enthalten in Russian journal of inorganic chemistry Moscow : MAIK Nauka/Interperiodica Publ., 2006 60(2015), 11 vom: 24. Okt., Seite 1317-1328 (DE-627)508334675 (DE-600)2223897-9 1531-8613 nnns volume:60 year:2015 number:11 day:24 month:10 pages:1317-1328 https://dx.doi.org/10.1134/S003602361511008X lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 60 2015 11 24 10 1317-1328 |
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Enthalten in Russian journal of inorganic chemistry 60(2015), 11 vom: 24. Okt., Seite 1317-1328 volume:60 year:2015 number:11 day:24 month:10 pages:1317-1328 |
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Russian journal of inorganic chemistry |
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Ivicheva, S. N. @@aut@@ Kargin, Yu. F. @@aut@@ Kutsev, S. V. @@aut@@ Ashmarin, A. A. @@aut@@ |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR020306482</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230519144025.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">201006s2015 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1134/S003602361511008X</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR020306482</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)S003602361511008X-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Ivicheva, S. N.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Pleiades Publishing, Ltd. 2015</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Bismuth</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Opal Matrix</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Opal Matrice</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Polyhydric Alcohol</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Titanium Alkoxide</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Kargin, Yu. 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| author |
Ivicheva, S. N. |
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Ivicheva, S. N. misc Bismuth misc Opal Matrix misc Opal Matrice misc Polyhydric Alcohol misc Titanium Alkoxide Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices |
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Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices Bismuth (dpeaa)DE-He213 Opal Matrix (dpeaa)DE-He213 Opal Matrice (dpeaa)DE-He213 Polyhydric Alcohol (dpeaa)DE-He213 Titanium Alkoxide (dpeaa)DE-He213 |
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misc Bismuth misc Opal Matrix misc Opal Matrice misc Polyhydric Alcohol misc Titanium Alkoxide |
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misc Bismuth misc Opal Matrix misc Opal Matrice misc Polyhydric Alcohol misc Titanium Alkoxide |
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Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices |
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Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices |
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Ivicheva, S. N. |
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Ivicheva, S. N. |
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10.1134/S003602361511008X |
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synthesis of different bismuth titanates and ordered bi-ti-o nanocomposites based on opal matrices |
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Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices |
| abstract |
Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. © Pleiades Publishing, Ltd. 2015 |
| abstractGer |
Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. © Pleiades Publishing, Ltd. 2015 |
| abstract_unstemmed |
Abstract Bismuth titanates of different composition and 3D nanocomposites based on opal matrices and bismuth titanates of different structure types have been synthesized by sol–gel and alkoxide methods with the use of polyhydric alcohols. The suggested procedure for synthesis of bismuth titanates $ Bi_{12} %$ TiO_{20} $ with a sillenite structure and $ Bi_{2} %$ Ti_{2} %$ O_{7} $ with a pyrochlore structure and layered titanates $ Bi_{4} %$ Ti_{3} %$ O_{12} $ makes it possible to decrease the temperature of the onset of formation of a target product in powders and a 3D nanocomposite based on opal matrices and to reduce the synthesis time. It has been revealed that the aging of the initial sol has an effect on the phase composition of bismuth titanates. It has been found that formation of the bismuth dititanate phase with a pyrochlore structure in the pores of opal matrices (nanoreactors) becomes dominating whatever the $ Bi_{2} %$ O_{3} $/$ TiO_{2} $ ratio is (2 : 3 or 1 : 2), which is associated with the effect of the size factor on the stability of the forming phases. It has been shown that the existence range of metastable $ Bi_{2} %$ Ti_{2} %$ O_{7} $ and $ Bi_{2} %$ SiO_{5} $ forming as nanoparticles can be extended from 20 to 1000°C through confinement of the reaction zone of the sol–gel synthesis in the pores of the opal matrix. © Pleiades Publishing, Ltd. 2015 |
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11 |
| title_short |
Synthesis of different bismuth titanates and ordered Bi-Ti-O nanocomposites based on opal matrices |
| url |
https://dx.doi.org/10.1134/S003602361511008X |
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Kargin, Yu. F. Kutsev, S. V. Ashmarin, A. A. |
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| doi_str |
10.1134/S003602361511008X |
| up_date |
2024-07-03T15:13:09.460Z |
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| score |
7.4006166 |