An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $
Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ra...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Zhao, Rui Rui [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2012 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer-Verlag 2012 |
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| Übergeordnetes Werk: |
Enthalten in: Ionics - Berlin : Springer, 1995, 19(2012), 4 vom: 06. Sept., Seite 581-588 |
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| Übergeordnetes Werk: |
volume:19 ; year:2012 ; number:4 ; day:06 ; month:09 ; pages:581-588 |
| Links: |
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| DOI / URN: |
10.1007/s11581-012-0799-4 |
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| Katalog-ID: |
SPR020852258 |
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| 100 | 1 | |a Zhao, Rui Rui |e verfasserin |4 aut | |
| 245 | 1 | 3 | |a An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ |
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| 520 | |a Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. | ||
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| 650 | 4 | |a Charging/discharging |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Zhu, Li Cai |4 aut | |
| 700 | 1 | |a Huang, Zhen Ze |4 aut | |
| 700 | 1 | |a Liang, Jing Zhi |4 aut | |
| 700 | 1 | |a Chen, Hong Yu |4 aut | |
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10.1007/s11581-012-0799-4 doi (DE-627)SPR020852258 (SPR)s11581-012-0799-4-e DE-627 ger DE-627 rakwb eng Zhao, Rui Rui verfasserin aut An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2012 Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. Cathodes (dpeaa)DE-He213 Batteries (dpeaa)DE-He213 Charging/discharging (dpeaa)DE-He213 Zhu, Li Cai aut Huang, Zhen Ze aut Liang, Jing Zhi aut Chen, Hong Yu aut Enthalten in Ionics Berlin : Springer, 1995 19(2012), 4 vom: 06. Sept., Seite 581-588 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:19 year:2012 number:4 day:06 month:09 pages:581-588 https://dx.doi.org/10.1007/s11581-012-0799-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 19 2012 4 06 09 581-588 |
| spelling |
10.1007/s11581-012-0799-4 doi (DE-627)SPR020852258 (SPR)s11581-012-0799-4-e DE-627 ger DE-627 rakwb eng Zhao, Rui Rui verfasserin aut An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2012 Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. Cathodes (dpeaa)DE-He213 Batteries (dpeaa)DE-He213 Charging/discharging (dpeaa)DE-He213 Zhu, Li Cai aut Huang, Zhen Ze aut Liang, Jing Zhi aut Chen, Hong Yu aut Enthalten in Ionics Berlin : Springer, 1995 19(2012), 4 vom: 06. Sept., Seite 581-588 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:19 year:2012 number:4 day:06 month:09 pages:581-588 https://dx.doi.org/10.1007/s11581-012-0799-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 19 2012 4 06 09 581-588 |
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10.1007/s11581-012-0799-4 doi (DE-627)SPR020852258 (SPR)s11581-012-0799-4-e DE-627 ger DE-627 rakwb eng Zhao, Rui Rui verfasserin aut An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2012 Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. Cathodes (dpeaa)DE-He213 Batteries (dpeaa)DE-He213 Charging/discharging (dpeaa)DE-He213 Zhu, Li Cai aut Huang, Zhen Ze aut Liang, Jing Zhi aut Chen, Hong Yu aut Enthalten in Ionics Berlin : Springer, 1995 19(2012), 4 vom: 06. Sept., Seite 581-588 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:19 year:2012 number:4 day:06 month:09 pages:581-588 https://dx.doi.org/10.1007/s11581-012-0799-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 19 2012 4 06 09 581-588 |
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10.1007/s11581-012-0799-4 doi (DE-627)SPR020852258 (SPR)s11581-012-0799-4-e DE-627 ger DE-627 rakwb eng Zhao, Rui Rui verfasserin aut An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2012 Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. Cathodes (dpeaa)DE-He213 Batteries (dpeaa)DE-He213 Charging/discharging (dpeaa)DE-He213 Zhu, Li Cai aut Huang, Zhen Ze aut Liang, Jing Zhi aut Chen, Hong Yu aut Enthalten in Ionics Berlin : Springer, 1995 19(2012), 4 vom: 06. Sept., Seite 581-588 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:19 year:2012 number:4 day:06 month:09 pages:581-588 https://dx.doi.org/10.1007/s11581-012-0799-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 19 2012 4 06 09 581-588 |
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10.1007/s11581-012-0799-4 doi (DE-627)SPR020852258 (SPR)s11581-012-0799-4-e DE-627 ger DE-627 rakwb eng Zhao, Rui Rui verfasserin aut An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer-Verlag 2012 Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. Cathodes (dpeaa)DE-He213 Batteries (dpeaa)DE-He213 Charging/discharging (dpeaa)DE-He213 Zhu, Li Cai aut Huang, Zhen Ze aut Liang, Jing Zhi aut Chen, Hong Yu aut Enthalten in Ionics Berlin : Springer, 1995 19(2012), 4 vom: 06. Sept., Seite 581-588 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:19 year:2012 number:4 day:06 month:09 pages:581-588 https://dx.doi.org/10.1007/s11581-012-0799-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 19 2012 4 06 09 581-588 |
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Zhao, Rui Rui @@aut@@ Zhu, Li Cai @@aut@@ Huang, Zhen Ze @@aut@@ Liang, Jing Zhi @@aut@@ Chen, Hong Yu @@aut@@ |
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Zhao, Rui Rui |
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Zhao, Rui Rui misc Cathodes misc Batteries misc Charging/discharging An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ |
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An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ Cathodes (dpeaa)DE-He213 Batteries (dpeaa)DE-He213 Charging/discharging (dpeaa)DE-He213 |
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An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ |
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An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ |
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Zhao, Rui Rui |
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Zhao, Rui Rui Zhu, Li Cai Huang, Zhen Ze Liang, Jing Zhi Chen, Hong Yu |
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10.1007/s11581-012-0799-4 |
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investigation on the performance of $ lifepo_{4} $/c derived from various $ fepo_{4} $ |
| title_auth |
An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ |
| abstract |
Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. © Springer-Verlag 2012 |
| abstractGer |
Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. © Springer-Verlag 2012 |
| abstract_unstemmed |
Abstract $ LiFePO_{4} $/C composites were synthesized by carbothermal reduction method using commercial $ FePO_{4} $ and Tween#80-assisted synthesized nano-$ FePO_{4} $ as starting materials, glucose as reducing agent, and also carbon source. The $ FePO_{4} $ intermediates were characterized by X-ray diffraction and scanning electron microscopy. A suitable mole ratio of Li to Fe was investigated, and the performances of samples synthesized under different temperatures were studied. It seems that the residual carbon content, which determine the electrochemical polarization of the cathode composites, greatly depend on the synthesis temperature when carbothermal reduction method was used. The electrochemical measurements showed that the discharge capacity first increase and then decrease with the rise of temperature. The optimal sample synthesized at 600 °C for 10 h using homemade $ FePO_{4} $ as iron source exhibit 142 mAh $ g^{−1} $ at 0.2 C and a capacity retention rate of 98.8 % after 50 cycles. © Springer-Verlag 2012 |
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4 |
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An investigation on the performance of $ LiFePO_{4} $/C derived from various $ FePO_{4} $ |
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https://dx.doi.org/10.1007/s11581-012-0799-4 |
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Zhu, Li Cai Huang, Zhen Ze Liang, Jing Zhi Chen, Hong Yu |
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Zhu, Li Cai Huang, Zhen Ze Liang, Jing Zhi Chen, Hong Yu |
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10.1007/s11581-012-0799-4 |
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2024-07-03T18:40:07.045Z |
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| score |
7.3978176 |