Determination of mercury species using thermal desorption analysis in AAS

Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO,...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Coufalík, Pavel [verfasserIn] Zvěřina, Ondřej [verfasserIn] Komárek, Josef [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2013

Schlagwörter:	mercury speciation soil thermal desorption extraction

Übergeordnetes Werk:	Enthalten in: Chemical papers - Wien : Springer Vienna, 1947, 68(2013), 4 vom: 11. Sept., Seite 427-434
Übergeordnetes Werk:	volume:68 ; year:2013 ; number:4 ; day:11 ; month:09 ; pages:427-434

Links:	Volltext

DOI / URN:	10.2478/s11696-013-0471-0

Katalog-ID:	SPR021872716

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520			\|a Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils.
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700	1		\|a Komárek, Josef \|e verfasserin \|4 aut
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matchkey_str	article:13369075:2013----::eemntoomruypceuighradsrt
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allfields	10.2478/s11696-013-0471-0 doi (DE-627)SPR021872716 (SPR)s11696-013-0471-0-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Coufalík, Pavel verfasserin aut Determination of mercury species using thermal desorption analysis in AAS 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils. mercury (dpeaa)DE-He213 speciation (dpeaa)DE-He213 soil (dpeaa)DE-He213 thermal desorption (dpeaa)DE-He213 extraction (dpeaa)DE-He213 Zvěřina, Ondřej verfasserin aut Komárek, Josef verfasserin aut Enthalten in Chemical papers Wien : Springer Vienna, 1947 68(2013), 4 vom: 11. Sept., Seite 427-434 (DE-627)518347737 (DE-600)2252770-9 1336-9075 nnns volume:68 year:2013 number:4 day:11 month:09 pages:427-434 https://dx.doi.org/10.2478/s11696-013-0471-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 68 2013 4 11 09 427-434
spelling	10.2478/s11696-013-0471-0 doi (DE-627)SPR021872716 (SPR)s11696-013-0471-0-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Coufalík, Pavel verfasserin aut Determination of mercury species using thermal desorption analysis in AAS 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils. mercury (dpeaa)DE-He213 speciation (dpeaa)DE-He213 soil (dpeaa)DE-He213 thermal desorption (dpeaa)DE-He213 extraction (dpeaa)DE-He213 Zvěřina, Ondřej verfasserin aut Komárek, Josef verfasserin aut Enthalten in Chemical papers Wien : Springer Vienna, 1947 68(2013), 4 vom: 11. Sept., Seite 427-434 (DE-627)518347737 (DE-600)2252770-9 1336-9075 nnns volume:68 year:2013 number:4 day:11 month:09 pages:427-434 https://dx.doi.org/10.2478/s11696-013-0471-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 68 2013 4 11 09 427-434
allfields_unstemmed	10.2478/s11696-013-0471-0 doi (DE-627)SPR021872716 (SPR)s11696-013-0471-0-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Coufalík, Pavel verfasserin aut Determination of mercury species using thermal desorption analysis in AAS 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils. mercury (dpeaa)DE-He213 speciation (dpeaa)DE-He213 soil (dpeaa)DE-He213 thermal desorption (dpeaa)DE-He213 extraction (dpeaa)DE-He213 Zvěřina, Ondřej verfasserin aut Komárek, Josef verfasserin aut Enthalten in Chemical papers Wien : Springer Vienna, 1947 68(2013), 4 vom: 11. Sept., Seite 427-434 (DE-627)518347737 (DE-600)2252770-9 1336-9075 nnns volume:68 year:2013 number:4 day:11 month:09 pages:427-434 https://dx.doi.org/10.2478/s11696-013-0471-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 68 2013 4 11 09 427-434
allfieldsGer	10.2478/s11696-013-0471-0 doi (DE-627)SPR021872716 (SPR)s11696-013-0471-0-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Coufalík, Pavel verfasserin aut Determination of mercury species using thermal desorption analysis in AAS 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils. mercury (dpeaa)DE-He213 speciation (dpeaa)DE-He213 soil (dpeaa)DE-He213 thermal desorption (dpeaa)DE-He213 extraction (dpeaa)DE-He213 Zvěřina, Ondřej verfasserin aut Komárek, Josef verfasserin aut Enthalten in Chemical papers Wien : Springer Vienna, 1947 68(2013), 4 vom: 11. Sept., Seite 427-434 (DE-627)518347737 (DE-600)2252770-9 1336-9075 nnns volume:68 year:2013 number:4 day:11 month:09 pages:427-434 https://dx.doi.org/10.2478/s11696-013-0471-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 68 2013 4 11 09 427-434
allfieldsSound	10.2478/s11696-013-0471-0 doi (DE-627)SPR021872716 (SPR)s11696-013-0471-0-e DE-627 ger DE-627 rakwb eng 540 ASE 35.00 bkl Coufalík, Pavel verfasserin aut Determination of mercury species using thermal desorption analysis in AAS 2013 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils. mercury (dpeaa)DE-He213 speciation (dpeaa)DE-He213 soil (dpeaa)DE-He213 thermal desorption (dpeaa)DE-He213 extraction (dpeaa)DE-He213 Zvěřina, Ondřej verfasserin aut Komárek, Josef verfasserin aut Enthalten in Chemical papers Wien : Springer Vienna, 1947 68(2013), 4 vom: 11. Sept., Seite 427-434 (DE-627)518347737 (DE-600)2252770-9 1336-9075 nnns volume:68 year:2013 number:4 day:11 month:09 pages:427-434 https://dx.doi.org/10.2478/s11696-013-0471-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 ASE AR 68 2013 4 11 09 427-434
language	English
source	Enthalten in Chemical papers 68(2013), 4 vom: 11. Sept., Seite 427-434 volume:68 year:2013 number:4 day:11 month:09 pages:427-434
sourceStr	Enthalten in Chemical papers 68(2013), 4 vom: 11. Sept., Seite 427-434 volume:68 year:2013 number:4 day:11 month:09 pages:427-434
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	mercury speciation soil thermal desorption extraction
dewey-raw	540
isfreeaccess_bool	false
container_title	Chemical papers
authorswithroles_txt_mv	Coufalík, Pavel @@aut@@ Zvěřina, Ondřej @@aut@@ Komárek, Josef @@aut@@
publishDateDaySort_date	2013-09-11T00:00:00Z
hierarchy_top_id	518347737
dewey-sort	3540
id	SPR021872716
language_de	englisch
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Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. 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author	Coufalík, Pavel
spellingShingle	Coufalík, Pavel ddc 540 bkl 35.00 misc mercury misc speciation misc soil misc thermal desorption misc extraction Determination of mercury species using thermal desorption analysis in AAS
authorStr	Coufalík, Pavel
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topic_title	540 ASE 35.00 bkl Determination of mercury species using thermal desorption analysis in AAS mercury (dpeaa)DE-He213 speciation (dpeaa)DE-He213 soil (dpeaa)DE-He213 thermal desorption (dpeaa)DE-He213 extraction (dpeaa)DE-He213
topic	ddc 540 bkl 35.00 misc mercury misc speciation misc soil misc thermal desorption misc extraction
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title	Determination of mercury species using thermal desorption analysis in AAS
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title_full	Determination of mercury species using thermal desorption analysis in AAS
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author_browse	Coufalík, Pavel Zvěřina, Ondřej Komárek, Josef
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title_sort	determination of mercury species using thermal desorption analysis in aas
title_auth	Determination of mercury species using thermal desorption analysis in AAS
abstract	Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils.
abstractGer	Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils.
abstract_unstemmed	Abstract Analytical aspects of the determination of inorganic mercury (Hg) species by thermal desorption followed by atomic absorption spectrometry (AAS) detection were investigated in this work. Characteristic Hg release curves of the following species were observed: $ Hg^{0} $, $ HgCl_{2} $, HgO, $ HgSO_{4} $, HgS, and the Hg bound to humic acids. Particular attention was dedicated to the thermal stability and change of bond of $ Hg^{0} $ in the following matrices: sand, kaolinite, granite, peat, power plant ash, and soil. The bond of elemental Hg in environmental materials was described on basis of this experiment. Contaminated soil samples from two locations in the Czech Republic were investigated by thermal desorption analysis. Afterwards, the contents of volatile and plant-available Hg in the studied samples were determined. The determination of $ Hg^{0} $ using the thermal method was related to the results of liquid sequential extraction. The development of Hg speciation and the stability of Hg were assessed on basis of the data obtained. Thus, the analytical procedure used is a suitable tool for the study of inorganic Hg species in contaminated soils.
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container_issue	4
title_short	Determination of mercury species using thermal desorption analysis in AAS
url	https://dx.doi.org/10.2478/s11696-013-0471-0
remote_bool	true
author2	Zvěřina, Ondřej Komárek, Josef
author2Str	Zvěřina, Ondřej Komárek, Josef
ppnlink	518347737
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hochschulschrift_bool	false
doi_str	10.2478/s11696-013-0471-0
up_date	2024-07-04T00:48:34.956Z
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Determination of mercury species using thermal desorption analysis in AAS

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