Synthesis of highly monodisperse silica nanoparticles in the microreactor system
Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Su, Min [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2016 |
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| Schlagwörter: |
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| Anmerkung: |
© Korean Institute of Chemical Engineers, Seoul, Korea 2017 |
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| Übergeordnetes Werk: |
Enthalten in: The Korean journal of chemical engineering - Seoul : Inst., 1984, 34(2016), 2 vom: 09. Dez., Seite 484-494 |
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| Übergeordnetes Werk: |
volume:34 ; year:2016 ; number:2 ; day:09 ; month:12 ; pages:484-494 |
| Links: |
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| DOI / URN: |
10.1007/s11814-016-0297-x |
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SPR022518916 |
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| 520 | |a Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with different sizes (from 20 nm to 2 μm) and size distributions (which were characterized by PDI from 0.01 to 0.40) were controllably synthesized by varying the concentration of reactants and the operating parameters in this system. The long microchannel with small diameter demonstrated a good mixing efficiency, and which produced small and uniform silica particles. In addition, the introduction of inert gas into the system intensified the mixing, and the silica particles with decreased size and narrow distribution were obtained. It was clearly demonstrated that the high mixing efficiency in the microchannel led to small and uniform silica particles. Furthermore, a theoretical foundation for the synthesis of nanoparticles in microreactors was established after illustrating the relationship of mass transfer and reaction in the system. | ||
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| 650 | 4 | |a Monodispersity |7 (dpeaa)DE-He213 | |
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10.1007/s11814-016-0297-x doi (DE-627)SPR022518916 (SPR)s11814-016-0297-x-e DE-627 ger DE-627 rakwb eng Su, Min verfasserin aut Synthesis of highly monodisperse silica nanoparticles in the microreactor system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Korean Institute of Chemical Engineers, Seoul, Korea 2017 Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with different sizes (from 20 nm to 2 μm) and size distributions (which were characterized by PDI from 0.01 to 0.40) were controllably synthesized by varying the concentration of reactants and the operating parameters in this system. The long microchannel with small diameter demonstrated a good mixing efficiency, and which produced small and uniform silica particles. In addition, the introduction of inert gas into the system intensified the mixing, and the silica particles with decreased size and narrow distribution were obtained. It was clearly demonstrated that the high mixing efficiency in the microchannel led to small and uniform silica particles. Furthermore, a theoretical foundation for the synthesis of nanoparticles in microreactors was established after illustrating the relationship of mass transfer and reaction in the system. Nanoparticle (dpeaa)DE-He213 Silica (dpeaa)DE-He213 Silica Nanoparticle (dpeaa)DE-He213 Microreactor (dpeaa)DE-He213 Monodispersity (dpeaa)DE-He213 Enthalten in The Korean journal of chemical engineering Seoul : Inst., 1984 34(2016), 2 vom: 09. Dez., Seite 484-494 (DE-627)391337246 (DE-600)2152566-3 1975-7220 nnns volume:34 year:2016 number:2 day:09 month:12 pages:484-494 https://dx.doi.org/10.1007/s11814-016-0297-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 34 2016 2 09 12 484-494 |
| spelling |
10.1007/s11814-016-0297-x doi (DE-627)SPR022518916 (SPR)s11814-016-0297-x-e DE-627 ger DE-627 rakwb eng Su, Min verfasserin aut Synthesis of highly monodisperse silica nanoparticles in the microreactor system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Korean Institute of Chemical Engineers, Seoul, Korea 2017 Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with different sizes (from 20 nm to 2 μm) and size distributions (which were characterized by PDI from 0.01 to 0.40) were controllably synthesized by varying the concentration of reactants and the operating parameters in this system. The long microchannel with small diameter demonstrated a good mixing efficiency, and which produced small and uniform silica particles. In addition, the introduction of inert gas into the system intensified the mixing, and the silica particles with decreased size and narrow distribution were obtained. It was clearly demonstrated that the high mixing efficiency in the microchannel led to small and uniform silica particles. Furthermore, a theoretical foundation for the synthesis of nanoparticles in microreactors was established after illustrating the relationship of mass transfer and reaction in the system. Nanoparticle (dpeaa)DE-He213 Silica (dpeaa)DE-He213 Silica Nanoparticle (dpeaa)DE-He213 Microreactor (dpeaa)DE-He213 Monodispersity (dpeaa)DE-He213 Enthalten in The Korean journal of chemical engineering Seoul : Inst., 1984 34(2016), 2 vom: 09. Dez., Seite 484-494 (DE-627)391337246 (DE-600)2152566-3 1975-7220 nnns volume:34 year:2016 number:2 day:09 month:12 pages:484-494 https://dx.doi.org/10.1007/s11814-016-0297-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 34 2016 2 09 12 484-494 |
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10.1007/s11814-016-0297-x doi (DE-627)SPR022518916 (SPR)s11814-016-0297-x-e DE-627 ger DE-627 rakwb eng Su, Min verfasserin aut Synthesis of highly monodisperse silica nanoparticles in the microreactor system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Korean Institute of Chemical Engineers, Seoul, Korea 2017 Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with different sizes (from 20 nm to 2 μm) and size distributions (which were characterized by PDI from 0.01 to 0.40) were controllably synthesized by varying the concentration of reactants and the operating parameters in this system. The long microchannel with small diameter demonstrated a good mixing efficiency, and which produced small and uniform silica particles. In addition, the introduction of inert gas into the system intensified the mixing, and the silica particles with decreased size and narrow distribution were obtained. It was clearly demonstrated that the high mixing efficiency in the microchannel led to small and uniform silica particles. Furthermore, a theoretical foundation for the synthesis of nanoparticles in microreactors was established after illustrating the relationship of mass transfer and reaction in the system. Nanoparticle (dpeaa)DE-He213 Silica (dpeaa)DE-He213 Silica Nanoparticle (dpeaa)DE-He213 Microreactor (dpeaa)DE-He213 Monodispersity (dpeaa)DE-He213 Enthalten in The Korean journal of chemical engineering Seoul : Inst., 1984 34(2016), 2 vom: 09. Dez., Seite 484-494 (DE-627)391337246 (DE-600)2152566-3 1975-7220 nnns volume:34 year:2016 number:2 day:09 month:12 pages:484-494 https://dx.doi.org/10.1007/s11814-016-0297-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 34 2016 2 09 12 484-494 |
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10.1007/s11814-016-0297-x doi (DE-627)SPR022518916 (SPR)s11814-016-0297-x-e DE-627 ger DE-627 rakwb eng Su, Min verfasserin aut Synthesis of highly monodisperse silica nanoparticles in the microreactor system 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Korean Institute of Chemical Engineers, Seoul, Korea 2017 Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with different sizes (from 20 nm to 2 μm) and size distributions (which were characterized by PDI from 0.01 to 0.40) were controllably synthesized by varying the concentration of reactants and the operating parameters in this system. The long microchannel with small diameter demonstrated a good mixing efficiency, and which produced small and uniform silica particles. In addition, the introduction of inert gas into the system intensified the mixing, and the silica particles with decreased size and narrow distribution were obtained. It was clearly demonstrated that the high mixing efficiency in the microchannel led to small and uniform silica particles. Furthermore, a theoretical foundation for the synthesis of nanoparticles in microreactors was established after illustrating the relationship of mass transfer and reaction in the system. Nanoparticle (dpeaa)DE-He213 Silica (dpeaa)DE-He213 Silica Nanoparticle (dpeaa)DE-He213 Microreactor (dpeaa)DE-He213 Monodispersity (dpeaa)DE-He213 Enthalten in The Korean journal of chemical engineering Seoul : Inst., 1984 34(2016), 2 vom: 09. Dez., Seite 484-494 (DE-627)391337246 (DE-600)2152566-3 1975-7220 nnns volume:34 year:2016 number:2 day:09 month:12 pages:484-494 https://dx.doi.org/10.1007/s11814-016-0297-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 34 2016 2 09 12 484-494 |
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Su, Min |
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Su, Min misc Nanoparticle misc Silica misc Silica Nanoparticle misc Microreactor misc Monodispersity Synthesis of highly monodisperse silica nanoparticles in the microreactor system |
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Synthesis of highly monodisperse silica nanoparticles in the microreactor system Nanoparticle (dpeaa)DE-He213 Silica (dpeaa)DE-He213 Silica Nanoparticle (dpeaa)DE-He213 Microreactor (dpeaa)DE-He213 Monodispersity (dpeaa)DE-He213 |
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Synthesis of highly monodisperse silica nanoparticles in the microreactor system |
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synthesis of highly monodisperse silica nanoparticles in the microreactor system |
| title_auth |
Synthesis of highly monodisperse silica nanoparticles in the microreactor system |
| abstract |
Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with different sizes (from 20 nm to 2 μm) and size distributions (which were characterized by PDI from 0.01 to 0.40) were controllably synthesized by varying the concentration of reactants and the operating parameters in this system. The long microchannel with small diameter demonstrated a good mixing efficiency, and which produced small and uniform silica particles. In addition, the introduction of inert gas into the system intensified the mixing, and the silica particles with decreased size and narrow distribution were obtained. It was clearly demonstrated that the high mixing efficiency in the microchannel led to small and uniform silica particles. Furthermore, a theoretical foundation for the synthesis of nanoparticles in microreactors was established after illustrating the relationship of mass transfer and reaction in the system. © Korean Institute of Chemical Engineers, Seoul, Korea 2017 |
| abstractGer |
Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with different sizes (from 20 nm to 2 μm) and size distributions (which were characterized by PDI from 0.01 to 0.40) were controllably synthesized by varying the concentration of reactants and the operating parameters in this system. The long microchannel with small diameter demonstrated a good mixing efficiency, and which produced small and uniform silica particles. In addition, the introduction of inert gas into the system intensified the mixing, and the silica particles with decreased size and narrow distribution were obtained. It was clearly demonstrated that the high mixing efficiency in the microchannel led to small and uniform silica particles. Furthermore, a theoretical foundation for the synthesis of nanoparticles in microreactors was established after illustrating the relationship of mass transfer and reaction in the system. © Korean Institute of Chemical Engineers, Seoul, Korea 2017 |
| abstract_unstemmed |
Abstract To avoid a poor mixing rate and local inhomogeneities in batch reactor systems, and to shorten the length of microchannels in microreactor systems, a new combined micromixer/microreactor/batch reactor system was used for the synthesis of colloidal silica particles. The silica particles with different sizes (from 20 nm to 2 μm) and size distributions (which were characterized by PDI from 0.01 to 0.40) were controllably synthesized by varying the concentration of reactants and the operating parameters in this system. The long microchannel with small diameter demonstrated a good mixing efficiency, and which produced small and uniform silica particles. In addition, the introduction of inert gas into the system intensified the mixing, and the silica particles with decreased size and narrow distribution were obtained. It was clearly demonstrated that the high mixing efficiency in the microchannel led to small and uniform silica particles. Furthermore, a theoretical foundation for the synthesis of nanoparticles in microreactors was established after illustrating the relationship of mass transfer and reaction in the system. © Korean Institute of Chemical Engineers, Seoul, Korea 2017 |
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Synthesis of highly monodisperse silica nanoparticles in the microreactor system |
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